Crystallography Open Database

Information card for entry 1100876

Preview

Coordinates	1100876.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H30 Cl Os P
Calculated formula	C22 H30 Cl Os P
Title of publication	Ene-Type Reactions between an α-Alkenylphosphine and Terminal Alkynes Promoted by Osmium-Cyclopentadienyl Fragments
Authors of publication	Baya, Miguel; Buil, María L.; Esteruelas, Miguel A.; Oñate, Enrique
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	9
Pages of publication	2030 - 2038
a	12.3343 ± 0.001 Å
b	12.6118 ± 0.001 Å
c	13.4358 ± 0.0011 Å
α	90°
β	95.913 ± 0.002°
γ	90°
Cell volume	2078.9 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0576
Residual factor for significantly intense reflections	0.0297
Weighted residual factors for significantly intense reflections	0.0365
Weighted residual factors for all reflections included in the refinement	0.0402
Goodness-of-fit parameter for all reflections included in the refinement	0.655
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	4060292
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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