#------------------------------------------------------------------------------
#$Date: 2016-02-13 13:50:18 +0100 (Sat 13 de Feb de 2016) $
#$Revision: 176428 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/99/1519910.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1519910
loop_
_publ_author_name
'James, Stuart L.'
'Lagunas, M. Cristina'
'Horton, Peter N.'
'Hursthouse, Michael B.'
_publ_section_title
;
 C48H28Au2Cl10OP2
;
_journal_name_full               'Crystal Structure Report Archive'
_journal_page_first              599
_journal_year                    2008
_chemical_formula_sum            'C48 H28 Au2 Cl10 O P2'
_chemical_formula_weight         1431.08
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                94.551(1)
_cell_angle_beta                 95.856(1)
_cell_angle_gamma                94.182(1)
_cell_formula_units_Z            2
_cell_length_a                   12.1958(1)
_cell_length_b                   13.3800(2)
_cell_length_c                   14.7281(2)
_cell_measurement_reflns_used    10776
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      2.910
_cell_volume                     2375.28(5)
_computing_cell_refinement
'DENZO (Otwinowski & Minor, 1997) & COLLECT (Hooft, R.W.W., 1998)'
_computing_data_collection       'COLLECT (Hooft, R.W.W., 1998)'
_computing_data_reduction
'DENZO (Otwinowski & Minor, 1997) & COLLECT (Hooft, R.W.W., 1998)'
_computing_molecular_graphics    'ORTEP3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997b)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997a)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 9.091
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type
'Bruker-Nonius Roper CCD camera on κ-goniostat'
_diffrn_measurement_method       'φ & ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Bruker-Nonius FR591 rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0529
_diffrn_reflns_av_sigmaI/netI    0.0454
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            51299
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    6.837
_exptl_absorpt_correction_T_max  0.7716
_exptl_absorpt_correction_T_min  0.3725
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS 2007/2 (Sheldrick, G.M., 2007)'
_exptl_crystal_colour            Colourless
_exptl_crystal_density_diffrn    2.001
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1364
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.04
_refine_diff_density_max         0.882
_refine_diff_density_min         -1.045
_refine_diff_density_rms         0.132
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.057
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     568
_refine_ls_number_reflns         10872
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.057
_refine_ls_R_factor_all          0.0363
_refine_ls_R_factor_gt           0.0277
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0010P)²+3.2631P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0535
_refine_ls_wR_factor_ref         0.0566
_reflns_number_gt                9327
_reflns_number_total             10872
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            eCrystal-599.cif
_cod_data_source_block           2008src0881
_cod_depositor_comments
;
Citation :
James, Stuart L. and Lagunas, M. Cristina and Horton, Peter N. and 
Hursthouse, Michael B. (2008) 
University of Southampton, Crystal Structure Report Archive. 
(doi:10.5258/ecrystals/599)

More at:
http://ecrystals.chem.soton.ac.uk/599/
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               1519910
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.709362(11) 0.475174(10) 0.298450(9) 0.01651(4) Uani 1 1 d . . .
Au2 Au 0.819959(11) -0.006435(10) 0.211049(10) 0.01798(4) Uani 1 1 d . . .
C1 C 0.5999(3) 0.2456(3) 0.3584(2) 0.0179(8) Uani 1 1 d . . .
C2 C 0.7003(3) 0.2030(3) 0.3746(2) 0.0185(8) Uani 1 1 d . . .
C3 C 0.7197(3) 0.1400(3) 0.4431(3) 0.0236(8) Uani 1 1 d . . .
H3 H 0.7891 0.1125 0.4532 0.028 Uiso 1 1 calc R . .
C4 C 0.6363(3) 0.1175(3) 0.4969(3) 0.0258(9) Uani 1 1 d . . .
H4 H 0.6488 0.0749 0.5449 0.031 Uiso 1 1 calc R . .
C5 C 0.5346(3) 0.1566(3) 0.4815(3) 0.0259(9) Uani 1 1 d . . .
H5 H 0.4774 0.1398 0.5182 0.031 Uiso 1 1 calc R . .
C6 C 0.5163(3) 0.2202(3) 0.4126(2) 0.0207(8) Uani 1 1 d . . .
H6 H 0.4463 0.2466 0.4021 0.025 Uiso 1 1 calc R . .
C7 C 0.9701(3) 0.2246(3) 0.3021(2) 0.0165(7) Uani 1 1 d . . .
C8 C 0.8844(3) 0.2576(3) 0.3500(2) 0.0169(8) Uani 1 1 d . . .
C9 C 0.9037(3) 0.3282(3) 0.4249(2) 0.0209(8) Uani 1 1 d . . .
H9 H 0.8440 0.3495 0.4562 0.025 Uiso 1 1 calc R . .
C10 C 1.0116(3) 0.3677(3) 0.4539(3) 0.0225(8) Uani 1 1 d . . .
H10 H 1.0262 0.4153 0.5059 0.027 Uiso 1 1 calc R . .
C11 C 1.0973(3) 0.3373(3) 0.4066(3) 0.0243(9) Uani 1 1 d . . .
H11 H 1.1706 0.3656 0.4254 0.029 Uiso 1 1 calc R . .
C12 C 1.0777(3) 0.2665(3) 0.3325(3) 0.0211(8) Uani 1 1 d . . .
H12 H 1.1379 0.2457 0.3015 0.025 Uiso 1 1 calc R . .
C13 C 0.4512(3) 0.3795(3) 0.2732(3) 0.0211(8) Uani 1 1 d . . .
C14 C 0.4340(3) 0.4491(3) 0.3448(3) 0.0280(9) Uani 1 1 d . . .
H14 H 0.4898 0.4648 0.3949 0.034 Uiso 1 1 calc R . .
C15 C 0.3360(4) 0.4954(3) 0.3433(3) 0.0373(11) Uani 1 1 d . . .
H15 H 0.3247 0.5428 0.3923 0.045 Uiso 1 1 calc R . .
C16 C 0.2550(4) 0.4729(4) 0.2710(4) 0.0425(13) Uani 1 1 d . . .
H16 H 0.1884 0.5057 0.2698 0.051 Uiso 1 1 calc R . .
C17 C 0.2700(3) 0.4027(3) 0.1996(4) 0.0409(12) Uani 1 1 d . . .
H17 H 0.2135 0.3869 0.1501 0.049 Uiso 1 1 calc R . .
C18 C 0.3682(3) 0.3555(3) 0.2010(3) 0.0281(9) Uani 1 1 d . . .
H18 H 0.3785 0.3069 0.1527 0.034 Uiso 1 1 calc R . .
C19 C 0.5893(3) 0.2604(3) 0.1634(2) 0.0172(8) Uani 1 1 d . . .
C20 C 0.5737(3) 0.1562(3) 0.1572(3) 0.0225(8) Uani 1 1 d . . .
H20 H 0.5597 0.1229 0.2100 0.027 Uiso 1 1 calc R . .
C21 C 0.5783(3) 0.1009(3) 0.0748(3) 0.0274(9) Uani 1 1 d . . .
H21 H 0.5691 0.0295 0.0711 0.033 Uiso 1 1 calc R . .
C22 C 0.5963(3) 0.1498(3) -0.0026(3) 0.0275(9) Uani 1 1 d . . .
H22 H 0.5979 0.1117 -0.0597 0.033 Uiso 1 1 calc R . .
C23 C 0.6121(3) 0.2535(3) 0.0025(3) 0.0230(8) Uani 1 1 d . . .
H23 H 0.6249 0.2866 -0.0506 0.028 Uiso 1 1 calc R . .
C24 C 0.6092(3) 0.3092(3) 0.0855(3) 0.0210(8) Uani 1 1 d . . .
H24 H 0.6207 0.3805 0.0895 0.025 Uiso 1 1 calc R . .
C25 C 1.0798(3) 0.0921(3) 0.1885(3) 0.0207(8) Uani 1 1 d . . .
C26 C 1.1241(3) 0.0260(3) 0.2487(3) 0.0322(10) Uani 1 1 d . . .
H26 H 1.0804 -0.0010 0.2922 0.039 Uiso 1 1 calc R . .
C27 C 1.2318(4) -0.0004(3) 0.2451(3) 0.0375(11) Uani 1 1 d . . .
H27 H 1.2618 -0.0447 0.2866 0.045 Uiso 1 1 calc R . .
C28 C 1.2950(3) 0.0375(3) 0.1816(3) 0.0328(10) Uani 1 1 d . . .
H28 H 1.3691 0.0205 0.1802 0.039 Uiso 1 1 calc R . .
C29 C 1.2505(3) 0.1004(3) 0.1197(3) 0.0320(10) Uani 1 1 d . . .
H29 H 1.2933 0.1244 0.0744 0.038 Uiso 1 1 calc R . .
C30 C 1.1432(3) 0.1284(3) 0.1239(3) 0.0262(9) Uani 1 1 d . . .
H30 H 1.1135 0.1726 0.0821 0.031 Uiso 1 1 calc R . .
C31 C 0.9086(3) 0.2021(3) 0.1069(2) 0.0185(8) Uani 1 1 d . . .
C32 C 0.8831(3) 0.1505(3) 0.0200(3) 0.0231(8) Uani 1 1 d . . .
H32 H 0.8752 0.0790 0.0136 0.028 Uiso 1 1 calc R . .
C33 C 0.8696(3) 0.2034(3) -0.0565(3) 0.0291(10) Uani 1 1 d . . .
H33 H 0.8539 0.1679 -0.1154 0.035 Uiso 1 1 calc R . .
C34 C 0.8784(3) 0.3071(3) -0.0487(3) 0.0294(10) Uani 1 1 d . . .
H34 H 0.8697 0.3428 -0.1019 0.035 Uiso 1 1 calc R . .
C35 C 0.9000(4) 0.3588(3) 0.0371(3) 0.0322(10) Uani 1 1 d . . .
H35 H 0.9046 0.4302 0.0430 0.039 Uiso 1 1 calc R . .
C36 C 0.9150(3) 0.3069(3) 0.1144(3) 0.0252(9) Uani 1 1 d . . .
H36 H 0.9297 0.3430 0.1731 0.030 Uiso 1 1 calc R . .
O1 O 0.77783(19) 0.22225(19) 0.31348(16) 0.0201(6) Uani 1 1 d . . .
P1 P 0.58838(7) 0.33522(7) 0.27156(7) 0.0165(2) Uani 1 1 d . . .
P2 P 0.94177(7) 0.13056(7) 0.20436(7) 0.0169(2) Uani 1 1 d . . .
C41 C 0.8032(3) 0.6108(3) 0.3311(2) 0.0167(7) Uani 1 1 d . . .
C42 C 0.7626(3) 0.6875(3) 0.3845(2) 0.0176(8) Uani 1 1 d . . .
C43 C 0.8238(3) 0.7782(3) 0.4141(2) 0.0203(8) Uani 1 1 d . . .
C44 C 0.9301(3) 0.7948(3) 0.3888(2) 0.0192(8) Uani 1 1 d . . .
C45 C 0.9729(3) 0.7204(3) 0.3343(2) 0.0190(8) Uani 1 1 d . . .
C46 C 0.9084(3) 0.6318(3) 0.3057(2) 0.0175(8) Uani 1 1 d . . .
Cl42 Cl 0.63174(8) 0.66781(7) 0.42092(7) 0.0261(2) Uani 1 1 d . . .
Cl43 Cl 0.77142(8) 0.86961(7) 0.48354(7) 0.0308(2) Uani 1 1 d . . .
Cl44 Cl 1.00868(8) 0.90351(7) 0.43018(7) 0.0292(2) Uani 1 1 d . . .
Cl45 Cl 1.10690(8) 0.73947(8) 0.30686(7) 0.0289(2) Uani 1 1 d . . .
Cl46 Cl 0.96354(8) 0.54017(7) 0.23722(7) 0.0270(2) Uani 1 1 d . . .
C51 C 0.7171(3) -0.1377(3) 0.1981(2) 0.0174(8) Uani 1 1 d . . .
C52 C 0.6139(3) -0.1493(3) 0.2315(2) 0.0183(8) Uani 1 1 d . . .
C53 C 0.5433(3) -0.2369(3) 0.2150(3) 0.0200(8) Uani 1 1 d . . .
C54 C 0.5759(3) -0.3186(3) 0.1628(3) 0.0208(8) Uani 1 1 d . . .
C55 C 0.6779(3) -0.3114(3) 0.1282(2) 0.0205(8) Uani 1 1 d . . .
C56 C 0.7460(3) -0.2227(3) 0.1473(2) 0.0192(8) Uani 1 1 d . . .
Cl52 Cl 0.57154(8) -0.04935(7) 0.29973(7) 0.0242(2) Uani 1 1 d . . .
Cl53 Cl 0.41574(7) -0.24522(7) 0.25685(7) 0.0263(2) Uani 1 1 d . . .
Cl54 Cl 0.49097(8) -0.42855(7) 0.14164(7) 0.0281(2) Uani 1 1 d . . .
Cl55 Cl 0.71712(9) -0.41209(7) 0.06146(7) 0.0320(2) Uani 1 1 d . . .
Cl56 Cl 0.87491(8) -0.21774(7) 0.10565(7) 0.0267(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C41 Au1 P1 172.58(10) . .
C51 Au2 P2 171.34(10) . .
C2 C1 C6 117.8(3) . .
C2 C1 P1 117.9(3) . .
C6 C1 P1 124.2(3) . .
C3 C2 O1 121.5(3) . .
C3 C2 C1 122.3(3) . .
O1 C2 C1 116.1(3) . .
C2 C3 C4 118.8(4) . .
C2 C3 H3 120.6 . .
C4 C3 H3 120.6 . .
C3 C4 C5 120.6(4) . .
C3 C4 H4 119.7 . .
C5 C4 H4 119.7 . .
C4 C5 C6 120.1(4) . .
C4 C5 H5 120.0 . .
C6 C5 H5 120.0 . .
C5 C6 C1 120.5(3) . .
C5 C6 H6 119.8 . .
C1 C6 H6 119.8 . .
C8 C7 C12 117.3(3) . .
C8 C7 P2 120.8(3) . .
C12 C7 P2 121.9(3) . .
C9 C8 O1 121.6(3) . .
C9 C8 C7 122.0(3) . .
O1 C8 C7 116.2(3) . .
C8 C9 C10 119.3(3) . .
C8 C9 H9 120.3 . .
C10 C9 H9 120.3 . .
C11 C10 C9 119.6(4) . .
C11 C10 H10 120.2 . .
C9 C10 H10 120.2 . .
C12 C11 C10 120.8(4) . .
C12 C11 H11 119.6 . .
C10 C11 H11 119.6 . .
C11 C12 C7 120.9(3) . .
C11 C12 H12 119.5 . .
C7 C12 H12 119.5 . .
C18 C13 C14 119.4(4) . .
C18 C13 P1 122.4(3) . .
C14 C13 P1 117.8(3) . .
C15 C14 C13 120.3(4) . .
C15 C14 H14 119.9 . .
C13 C14 H14 119.9 . .
C16 C15 C14 120.1(4) . .
C16 C15 H15 119.9 . .
C14 C15 H15 119.9 . .
C15 C16 C17 120.4(4) . .
C15 C16 H16 119.8 . .
C17 C16 H16 119.8 . .
C16 C17 C18 119.6(4) . .
C16 C17 H17 120.2 . .
C18 C17 H17 120.2 . .
C17 C18 C13 120.1(4) . .
C17 C18 H18 120.0 . .
C13 C18 H18 120.0 . .
C20 C19 C24 119.7(3) . .
C20 C19 P1 121.4(3) . .
C24 C19 P1 118.9(3) . .
C21 C20 C19 120.3(4) . .
C21 C20 H20 119.9 . .
C19 C20 H20 119.9 . .
C20 C21 C22 119.8(4) . .
C20 C21 H21 120.1 . .
C22 C21 H21 120.1 . .
C23 C22 C21 120.5(4) . .
C23 C22 H22 119.8 . .
C21 C22 H22 119.8 . .
C22 C23 C24 119.8(4) . .
C22 C23 H23 120.1 . .
C24 C23 H23 120.1 . .
C23 C24 C19 119.9(3) . .
C23 C24 H24 120.0 . .
C19 C24 H24 120.0 . .
C30 C25 C26 119.3(4) . .
C30 C25 P2 123.5(3) . .
C26 C25 P2 117.2(3) . .
C27 C26 C25 120.2(4) . .
C27 C26 H26 119.9 . .
C25 C26 H26 119.9 . .
C28 C27 C26 120.2(4) . .
C28 C27 H27 119.9 . .
C26 C27 H27 119.9 . .
C27 C28 C29 120.0(4) . .
C27 C28 H28 120.0 . .
C29 C28 H28 120.0 . .
C28 C29 C30 120.1(4) . .
C28 C29 H29 119.9 . .
C30 C29 H29 119.9 . .
C25 C30 C29 120.2(4) . .
C25 C30 H30 119.9 . .
C29 C30 H30 119.9 . .
C36 C31 C32 118.7(3) . .
C36 C31 P2 122.4(3) . .
C32 C31 P2 118.8(3) . .
C33 C32 C31 120.0(4) . .
C33 C32 H32 120.0 . .
C31 C32 H32 120.0 . .
C34 C33 C32 121.0(4) . .
C34 C33 H33 119.5 . .
C32 C33 H33 119.5 . .
C33 C34 C35 119.4(4) . .
C33 C34 H34 120.3 . .
C35 C34 H34 120.3 . .
C34 C35 C36 120.3(4) . .
C34 C35 H35 119.8 . .
C36 C35 H35 119.8 . .
C35 C36 C31 120.5(4) . .
C35 C36 H36 119.7 . .
C31 C36 H36 119.7 . .
C8 O1 C2 117.7(3) . .
C19 P1 C13 107.09(17) . .
C19 P1 C1 104.95(16) . .
C13 P1 C1 105.90(16) . .
C19 P1 Au1 116.94(12) . .
C13 P1 Au1 106.00(12) . .
C1 P1 Au1 115.21(12) . .
C31 P2 C7 104.80(16) . .
C31 P2 C25 103.53(17) . .
C7 P2 C25 102.14(16) . .
C31 P2 Au2 113.76(12) . .
C7 P2 Au2 119.91(11) . .
C25 P2 Au2 110.91(12) . .
C46 C41 C42 115.6(3) . .
C46 C41 Au1 124.6(3) . .
C42 C41 Au1 119.8(3) . .
C43 C42 C41 123.1(3) . .
C43 C42 Cl42 117.9(3) . .
C41 C42 Cl42 119.0(3) . .
C42 C43 C44 119.2(3) . .
C42 C43 Cl43 121.3(3) . .
C44 C43 Cl43 119.4(3) . .
C43 C44 C45 119.4(3) . .
C43 C44 Cl44 119.4(3) . .
C45 C44 Cl44 121.1(3) . .
C46 C45 C44 119.3(3) . .
C46 C45 Cl45 121.5(3) . .
C44 C45 Cl45 119.1(3) . .
C45 C46 C41 123.4(3) . .
C45 C46 Cl46 118.5(3) . .
C41 C46 Cl46 118.1(3) . .
C56 C51 C52 114.6(3) . .
C56 C51 Au2 119.6(3) . .
C52 C51 Au2 125.7(3) . .
C53 C52 C51 123.7(3) . .
C53 C52 Cl52 117.7(3) . .
C51 C52 Cl52 118.5(3) . .
C54 C53 C52 119.1(3) . .
C54 C53 Cl53 119.6(3) . .
C52 C53 Cl53 121.3(3) . .
C53 C54 C55 119.6(3) . .
C53 C54 Cl54 120.4(3) . .
C55 C54 Cl54 120.1(3) . .
C56 C55 C54 119.3(3) . .
C56 C55 Cl55 121.2(3) . .
C54 C55 Cl55 119.6(3) . .
C55 C56 C51 123.7(3) . .
C55 C56 Cl56 117.9(3) . .
C51 C56 Cl56 118.4(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Au1 C41 2.068(3) .
Au1 P1 2.2805(9) .
Au2 C51 2.067(3) .
Au2 P2 2.2887(9) .
C1 C2 1.395(5) .
C1 C6 1.397(5) .
C1 P1 1.823(4) .
C2 C3 1.379(5) .
C2 O1 1.395(4) .
C3 C4 1.383(5) .
C3 H3 0.9500 .
C4 C5 1.385(5) .
C4 H4 0.9500 .
C5 C6 1.387(5) .
C5 H5 0.9500 .
C6 H6 0.9500 .
C7 C8 1.397(5) .
C7 C12 1.404(5) .
C7 P2 1.822(4) .
C8 C9 1.384(5) .
C8 O1 1.389(4) .
C9 C10 1.394(5) .
C9 H9 0.9500 .
C10 C11 1.381(5) .
C10 H10 0.9500 .
C11 C12 1.377(5) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C18 1.392(5) .
C13 C14 1.393(5) .
C13 P1 1.817(4) .
C14 C15 1.385(5) .
C14 H14 0.9500 .
C15 C16 1.375(7) .
C15 H15 0.9500 .
C16 C17 1.389(7) .
C16 H16 0.9500 .
C17 C18 1.392(6) .
C17 H17 0.9500 .
C18 H18 0.9500 .
C19 C20 1.388(5) .
C19 C24 1.397(5) .
C19 P1 1.814(4) .
C20 C21 1.379(5) .
C20 H20 0.9500 .
C21 C22 1.389(5) .
C21 H21 0.9500 .
C22 C23 1.383(5) .
C22 H22 0.9500 .
C23 C24 1.385(5) .
C23 H23 0.9500 .
C24 H24 0.9500 .
C25 C30 1.382(5) .
C25 C26 1.398(5) .
C25 P2 1.828(4) .
C26 C27 1.389(6) .
C26 H26 0.9500 .
C27 C28 1.375(6) .
C27 H27 0.9500 .
C28 C29 1.386(6) .
C28 H28 0.9500 .
C29 C30 1.394(5) .
C29 H29 0.9500 .
C30 H30 0.9500 .
C31 C36 1.394(5) .
C31 C32 1.400(5) .
C31 P2 1.815(4) .
C32 C33 1.379(5) .
C32 H32 0.9500 .
C33 C34 1.378(6) .
C33 H33 0.9500 .
C34 C35 1.383(6) .
C34 H34 0.9500 .
C35 C36 1.383(5) .
C35 H35 0.9500 .
C36 H36 0.9500 .
C41 C46 1.389(5) .
C41 C42 1.394(5) .
C42 C43 1.392(5) .
C42 Cl42 1.744(4) .
C43 C44 1.392(5) .
C43 Cl43 1.732(4) .
C44 C45 1.394(5) .
C44 Cl44 1.715(4) .
C45 C46 1.385(5) .
C45 Cl45 1.729(4) .
C46 Cl46 1.742(4) .
C51 C56 1.398(5) .
C51 C52 1.400(5) .
C52 C53 1.392(5) .
C52 Cl52 1.749(4) .
C53 C54 1.391(5) .
C53 Cl53 1.731(4) .
C54 C55 1.391(5) .
C54 Cl54 1.724(4) .
C55 C56 1.391(5) .
C55 Cl55 1.730(4) .
C56 Cl56 1.743(4) .
