Information card for entry 1549272

Structure parameters

• Formula: C H7.89 N O7.45 P V
• Calculated formula: C H7.89 N O7.445 P V
• Title of publication: Synthesis, crystal structure of the ammonium vanadyl oxalatophosphite and its controlled conversion into catalytic vanadyl phosphates
• Authors of publication: C. Kouvatas; V. Alonzo; T. Bataille; L. Le Polles; C. Roiland; G. Louarn; E. Le Fur
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2017
• Journal volume: 253
• Pages of publication: 73 - 77
• a: 6.3844 ± 0.0004 Å
• b: 7.2278 ± 0.0004 Å
• c: 9.2965 ± 0.0005 Å
• α: 67.26 ± 0.004°
• β: 72.927 ± 0.004°
• γ: 85.848 ± 0.003°
• Cell volume: 377.8 ± 0.04 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.1064
• Weighted residual factors for all reflections included in the refinement: 0.1114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No