#------------------------------------------------------------------------------
#$Date: 2025-07-06 16:11:03 +0200 (Sun 06 de Jul de 2025) $
#$Revision: 300591 $
#$URL: svn://www.crystallography.net/cod/cif/1/57/42/1574220.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1574220
loop_
_publ_author_name
'Kemp, Kingsley Christian'
'Altundal, Ömer F.'
'Jo, Donghui'
'Huang, Weidong'
'Wang, Qiang'
'Deng, Feng'
'Sastre, German'
'Hong, Suk Bong'
_publ_section_title
;
 The role of structural defects in the fluoride-mediated synthesis of
 aluminosilicate zeolites
;
_journal_issue                   17
_journal_name_full               'Chemical Science'
_journal_page_first              7579
_journal_page_last               7589
_journal_paper_doi               10.1039/D5SC00899A
_journal_volume                  16
_journal_year                    2025
_chemical_formula_sum            'C4 N0.5 O10 Si5'
_chemical_formula_weight         355.47
_chemical_name_common            'As-made PST-21 (134TMP)'
_chemical_name_systematic        zeolite
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_date             2024-06-23T23:58
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
;
2024-06-29 deposited with the CCDC.	2025-03-25 downloaded from the CCDC.
;
_cell_angle_alpha                90.0
_cell_angle_beta                 93.013(22)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.3494(15)
_cell_length_b                   11.9607(34)
_cell_length_c                   11.0756(31)
_cell_measurement_temperature    298
_cell_volume                     1236.8(5)
_computing_structure_refinement  GSAS
_diffrn_ambient_temperature      298
_diffrn_radiation_polarisn_ratio 0.95
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.7
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id                     2024-06-23T23:58|PWO|Jo|PAL_2D
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.025
_pd_meas_2theta_range_max        40.9875
_pd_meas_2theta_range_min        2.9875
_pd_meas_number_of_points        1521
_pd_phase_name                   PWO
_pd_proc_2theta_range_inc        0.025
_pd_proc_2theta_range_max        40.94405
_pd_proc_2theta_range_min        2.94405
_pd_proc_info_datetime           2024-06-23T23:58:46
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 14 terms.
 Shifted Chebyshev function of 1st kind
      1:    2614.28     2:   -897.075     3:   -42.5785     4:    172.057    
      5:   -274.523     6:   -38.9368     7:    562.107     8:   -474.324    
      9:    171.497    10:    47.7374    11:   -246.064    12:    132.104    
     13:    23.4931    14:   -88.0879    
;
_pd_proc_ls_peak_cutoff          0.00500
_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  21 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 #1(GU)   =    0.000 #2(GV)   = -127.509 #3(GW)   =   21.747
 #4(GP)   =    2.297 #5(LX)   =   11.561 #6(ptec) =     0.97
 #7(trns) =     0.00 #8(shft) =   0.0000 #9(sfec) =     0.00
 #10(S/L) =   0.0110 #11(H/L) =   0.0110 #12(eta) =   0.0000
 #13(S400 ) =  5.2E-02 #14(S040 ) =  0.0E+00 #15(S004 ) =  0.0E+00
 #16(S220 ) =  6.9E-01 #17(S202 ) =  1.6E-01 #18(S022 ) =  1.7E+00
 #19(S301 ) =  2.0E-02 #20(S103 ) =  4.4E-02 #21(S121 ) = -7.1E-01
 Peak tails are ignored  where the intensity is below 0.0050 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0352
_pd_proc_ls_prof_wR_expected     0.0162
_pd_proc_ls_prof_wR_factor       0.0451
_pd_proc_number_of_points        1521
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   3.60
_refine_ls_matrix_type           full
_refine_ls_number_parameters     81
_refine_ls_number_restraints     50
_refine_ls_R_Fsqd_factor         0.06588
_refine_ls_shift/su_max          0.02
_refine_ls_shift/su_mean         0.00
_reflns_d_resolution_high        1.001
_reflns_d_resolution_low         9.336
_reflns_limit_h_max              9
_reflns_limit_h_min              0
_reflns_limit_k_max              12
_reflns_limit_k_min              0
_reflns_limit_l_max              11
_reflns_limit_l_min              -11
_reflns_number_total             1288
_cod_data_source_file            d5sc00899a2.cif
_cod_data_source_block           PWO_publ
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_geom_angle_publ_flag' value 'N' was changed to 'n' in
accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26 (12 times).

data item '_geom_bond_publ_flag' value 'N' was changed to 'n' in
accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26 (29 times).

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 1574220--1574221.cif.
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C4 N0.50 O10 Si5'
_cod_database_code               1574220
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y+1/2,-z+1/2
-1 -x,-y,-z
-2 +x,-y+1/2,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Si Si1 0.1587(8) 0.4044(7) 0.2222(7) 1.0 Uiso 0.01 4
Si Si2 0.0865(8) 0.8273(6) 0.4677(7) 1.0 Uiso 0.01 4
Si Si3 0.1436(8) 0.1646(7) 0.3260(7) 1.0 Uiso 0.01 4
Si Si4 0.3259(8) 0.4888(7) 0.0016(8) 1.0 Uiso 0.01 4
Si Si5 0.0462(9) 0.5772(6) 0.3904(7) 1.0 Uiso 0.01 4
O O1 0.1533(7) 0.5092(5) 0.3100(6) 1.0 Uiso 0.01 4
O O2 0.0084(6) 0.3834(7) 0.1438(5) 1.0 Uiso 0.01 4
O O3 0.1943(9) 0.2912(4) 0.2991(7) 1.0 Uiso 0.01 4
O O4 0.2835(7) 0.4275(7) 0.1266(5) 1.0 Uiso 0.01 4
O O5 0.7629(6) 0.3953(5) 0.0107(9) 1.0 Uiso 0.01 4
O O6 0.0066(6) 0.1650(8) 0.4123(5) 1.0 Uiso 0.01 4
O O7 0.1134(9) 0.6960(4) 0.4378(8) 1.0 Uiso 0.01 4
O O8 0.2717(7) 0.0937(5) 0.3911(6) 1.0 Uiso 0.01 4
O O9 0.0940(7) 0.1071(7) 0.1981(5) 1.0 Uiso 0.01 4
O O10 0.5 0.0 0.5 1.0 Uiso 0.01 2
O O11 0.0 0.0 0.0 1.0 Uiso 0.01 2
N N1 0.573(6) 0.389(5) 0.402(5) 0.5 Uiso 0.01 4
C C2 0.569(6) 0.501(5) 0.375(5) 0.5 Uiso 0.01 4
C C3 0.513(6) 0.579(5) 0.455(5) 0.5 Uiso 0.01 4
C C4 0.460(6) 0.540(5) 0.564(5) 0.5 Uiso 0.01 4
C C5 0.464(6) 0.425(6) 0.589(5) 0.5 Uiso 0.01 4
C C6 0.521(6) 0.351(5) 0.507(6) 0.5 Uiso 0.01 4
C Cm1 0.633(7) 0.312(6) 0.316(7) 0.5 Uiso 0.01 4
C Cm3 0.513(7) 0.701(5) 0.421(7) 0.5 Uiso 0.01 4
C Cm4 0.398(7) 0.617(7) 0.656(6) 0.5 Uiso 0.01 4
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Si 20.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100
81.6937 1.14070 International_Tables_Vol_C
O 40.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
N 2.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630
0.58260 -11.529 International_Tables_Vol_C
C 16.0 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 N1 C6 120.5375(35) 1_555 . 1_555 n
C2 N1 Cm1 118.904(15) 1_555 . 1_555 n
C6 N1 Cm1 120.559(18) 1_555 . 1_555 n
N1 C2 C3 121.160(15) 1_555 . 1_555 n
C2 C3 C4 118.785(18) 1_555 . 1_555 n
C2 C3 Cm3 119.020(16) 1_555 . 1_555 n
C4 C3 Cm3 122.1949(26) 1_555 . 1_555 n
C3 C4 C5 118.794(4) 1_555 . 1_555 n
C3 C4 Cm4 123.141(18) 1_555 . 1_555 n
C5 C4 Cm4 118.064(15) 1_555 . 1_555 n
C4 C5 C6 120.174(15) 1_555 . 1_555 n
N1 C6 C5 120.547(18) 1_555 . 1_555 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Si1 O1 1.589(10) . 1_555 n
Si1 O2 1.632(10) . 1_555 n
Si1 O3 1.624(10) . 1_555 n
Si1 O4 1.639(10) . 1_555 n
Si2 O2 1.627(10) . 2_555 n
Si2 O5 1.633(9) . 2_655 n
Si2 O6 1.629(10) . -1_566 n
Si2 O7 1.627(9) . 1_555 n
Si3 O3 1.620(10) . 1_555 n
Si3 O6 1.637(10) . 1_555 n
Si3 O8 1.607(10) . 1_555 n
Si3 O9 1.621(10) . 1_555 n
Si4 O4 1.634(10) . 1_555 n
Si4 O5 1.617(10) . -1_665 n
Si4 O8 1.632(10) . -2_554 n
Si4 O10 1.635(7) . 2_655 n
Si5 O1 1.597(10) . 1_555 n
Si5 O7 1.630(9) . 1_555 n
Si5 O9 1.634(10) . 2_555 n
Si5 O11 1.602(8) . 2_555 n
N1 C2 1.3636(4) . 1_555 n
N1 C6 1.36352(33) . 1_555 n
N1 Cm1 1.46479(29) . 1_555 n
C2 C3 1.40385(27) . 1_555 n
C3 C4 1.41447(35) . 1_555 n
C3 Cm3 1.5045(4) . 1_555 n
C4 C5 1.4006(4) . 1_555 n
C4 Cm4 1.50905(30) . 1_555 n
C5 C6 1.39421(27) . 1_555 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
3853.0 0.0 3986.61938 .
3847.0 0.0002599 3954.73682 3954.68677
3834.0 0.0002608 3923.30688 3923.25952
3826.0 0.0002614 3892.31177 3892.26733
3817.0 0.0002620 3861.73657 3861.69507
3799.0 0.0002632 3831.56616 3831.52734
3793.0 0.0002636 3801.78589 3801.74976
3779.0 0.0002646 3772.38354 3772.34985
3774.0 0.0002650 3743.34570 3743.31421
3755.0 0.0002663 3714.66089 3714.63159
3755.0 0.0002663 3686.31812 3686.29102
3747.0 0.0002669 3658.30713 3658.28198
3735.0 0.0002677 3630.61865 3630.59521
3727.0 0.0002683 3603.24292 3603.22144
3716.0 0.0002691 3576.17139 3576.15186
3709.0 0.0002696 3549.39771 3549.37964
3698.0 0.0002704 3522.91309 3680.30347
3698.0 0.0002704 3496.71240 3663.11963
3690.0 0.0002710 3470.78882 3647.00903
3679.0 0.0002718 3445.13623 3632.06226
3669.0 0.0002726 3419.75122 3618.38721
3657.0 0.0002734 3394.62769 3606.10791
3646.0 0.0002743 3369.76221 3595.37085
3638.0 0.0002749 3345.15137 3586.35059
3636.0 0.0002750 3320.79102 3579.25122
3637.0 0.0002750 3296.67993 3574.31836
3636.0 0.0002750 3272.81445 3571.84229
3645.0 0.0002743 3249.19287 3572.17480
3654.0 0.0002737 3225.81348 3575.73950
3678.0 0.0002719 3202.67505 3583.05298
3688.0 0.0002711 3179.77637 3594.74854
3715.0 0.0002692 3157.11719 3611.60986
3726.0 0.0002684 3134.69678 3634.61401
3745.0 0.0002670 3112.51465 3664.99243
3762.0 0.0002658 3090.57202 3704.31885
3794.0 0.0002636 3068.86816 3754.63062
3846.0 0.0002600 3047.40405 3818.64111
3914.0 0.0002555 3026.18091 3900.10742
4015.0 0.0002491 3005.19946 4004.55103
4141.0 0.0002415 2984.46069 4140.65039
4309.0 0.0002321 2963.96704 4322.75146
4523.0 0.0002211 2943.71924 4574.81738
4801.0 0.0002083 2923.71899 4968.38428
5245.0 0.0001907 2903.96899 5498.44385
5869.0 0.0001704 2884.47046 6277.76611
6838.0 0.0001462 2865.22632 7409.23145
8223.0 0.0001216 2846.23901 9004.82324
10287.0 0.0000972 2827.51001 11147.99805
12896.0 0.0000775 2809.04272 13809.90430
16201.0 0.0000617 2790.83936 16778.28711
19928.0 0.0000502 2772.90308 19793.30273
23068.0 0.0000434 2755.23657 22690.79102
25098.0 0.0000398 2737.84229 24994.34766
24834.0 0.0000403 2720.72314 25614.04102
22797.0 0.0000439 2703.88232 23769.39648
19195.0 0.0000521 2687.32300 20159.66797
15350.0 0.0000651 2671.04858 16130.57910
12016.0 0.0000832 2655.06104 12559.25781
9339.0 0.0001071 2639.36401 9761.90137
7537.0 0.0001327 2623.96069 7744.21094
6228.0 0.0001606 2608.85400 6372.58643
5378.0 0.0001859 2594.04736 5472.21045
4817.0 0.0002076 2579.54321 4884.80811
4475.0 0.0002235 2565.34521 4493.92334
4234.0 0.0002362 2551.45630 4226.15576
4070.0 0.0002457 2537.87915 4040.85083
3965.0 0.0002522 2524.61743 3918.34326
3908.0 0.0002559 2511.67358 3851.27002
3897.0 0.0002566 2499.05054 3839.31714
3922.0 0.0002550 2486.75146 3886.07495
4004.0 0.0002498 2474.77905 3996.65430
4143.0 0.0002414 2463.13623 4175.19238
4337.0 0.0002306 2451.82520 4421.82910
4588.0 0.0002180 2440.84912 4729.12939
4886.0 0.0002047 2430.21069 5078.60303
5221.0 0.0001915 2419.91187 5439.28516
5513.0 0.0001814 2409.95581 5770.32617
5761.0 0.0001736 2400.34448 6025.34473
5853.0 0.0001709 2391.07983 6155.44824
5788.0 0.0001728 2382.16479 6119.52930
5574.0 0.0001794 2373.60132 5908.10498
5245.0 0.0001907 2365.39160 5556.97412
4892.0 0.0002044 2357.53687 5129.14600
4522.0 0.0002211 2350.03955 4687.61182
4225.0 0.0002367 2342.90137 4271.72803
3966.0 0.0002521 2336.12402 3909.55859
3782.0 0.0002644 2329.70947 3613.48511
3642.0 0.0002746 2323.65820 3386.62769
3557.0 0.0002811 2317.97266 3226.70337
3500.0 0.0002857 2312.65332 2976.00195
3467.0 0.0002884 2307.70190 2946.30127
3454.0 0.0002895 2303.11938 2974.90649
3463.0 0.0002888 2298.90625 3064.03979
3489.0 0.0002866 2295.06421 3216.67041
3523.0 0.0002838 2291.59326 3432.09106
3564.0 0.0002806 2288.49438 3699.24658
3607.0 0.0002772 2285.76807 3991.09351
3639.0 0.0002748 2283.41479 4266.85254
3653.0 0.0002737 2281.43457 4477.73389
3646.0 0.0002743 2279.82813 4564.67139
3612.0 0.0002769 2278.59497 4478.51807
3552.0 0.0002815 2277.73560 4231.94043
3484.0 0.0002870 2277.24927 3899.14795
3400.0 0.0002941 2277.13647 3557.55811
3318.0 0.0003014 2277.39624 3254.41870
3237.0 0.0003089 2278.02808 3009.38013
3165.0 0.0003160 2279.03223 2824.76758
3100.0 0.0003226 2280.40674 2693.27295
3039.0 0.0003291 2282.15186 2603.41406
2990.0 0.0003344 2284.26611 2543.40161
2953.0 0.0003386 2286.74854 2503.39258
2916.0 0.0003429 2289.59790 2480.22534
2881.0 0.0003471 2292.81323 2461.55054
2852.0 0.0003506 2296.39307 2471.25488
2830.0 0.000353 2300.33594 2463.17456
2810.0 0.000356 2304.63989 2426.13550
2796.0 0.000358 2309.30347 2425.18555
2789.0 0.000359 2314.32520 2426.23511
2780.0 0.000360 2319.70264 2429.07715
2774.0 0.000360 2325.43433 2433.58789
2768.0 0.000361 2331.51758 2439.71777
2766.0 0.000362 2337.95044 2447.49463
2760.0 0.000362 2344.73071 2457.04224
2758.0 0.000363 2351.85620 2468.61108
2760.0 0.000362 2359.32373 2482.62524
2769.0 0.000361 2367.13110 2499.72974
2772.0 0.000361 2375.27539 2520.83691
2781.0 0.000360 2383.75391 2547.14551
2793.0 0.000358 2392.56372 2580.10059
2807.0 0.000356 2401.70215 2621.27661
2824.0 0.000354 2411.16577 2672.16162
2854.0 0.0003504 2420.95142 2733.83862
2892.0 0.0003458 2431.05591 2806.60059
2929.0 0.0003414 2441.47607 2889.51782
2969.0 0.0003368 2452.20801 2993.07178
3012.0 0.0003320 2463.24854 3087.69580
3055.0 0.0003273 2474.59375 3180.13843
3085.0 0.0003241 2486.24048 3264.71167
3117.0 0.0003208 2498.18481 3337.78906
3154.0 0.0003171 2510.42261 3401.20532
3189.0 0.0003136 2522.95020 3465.72974
3253.0 0.0003074 2535.76343 3551.81421
3377.0 0.0002961 2548.85840 3686.17236
3616.0 0.0002765 2562.23120 3899.78857
3985.0 0.0002509 2575.87720 4222.85303
4488.0 0.0002228 2589.79248 4665.52393
5221.0 0.0001915 2603.97241 5239.25439
6053.0 0.0001652 2618.41284 5870.54883
6856.0 0.0001459 2633.10913 6444.08984
7271.0 0.0001375 2648.05713 6819.49854
7147.0 0.0001399 2663.25195 6827.04541
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2136.0 0.000468 1847.79285 2172.85449
2124.0 0.000471 1845.02087 2164.41992
2113.0 0.000473 1842.25122 2156.76733
2102.0 0.000476 1839.48462 2149.98291
2093.0 0.000478 1836.72034 2144.04785
2085.0 0.000480 1833.95947 2138.99365
2078.0 0.000481 1831.20142 2134.84937
2072.0 0.000483 1828.44702 2131.65454
2070.0 0.000483 1825.69690 2129.62036
2073.0 0.000482 1822.95068 2129.17480
2076.0 0.000482 1820.20935 2130.70825
2080.0 0.000481 1817.47241 2134.81250
2085.0 0.000480 1814.74109 2141.70239
2092.0 0.000478 1812.01575 2152.11499
2100.0 0.000476 1809.29639 2164.26587
2107.0 0.000475 1806.58398 2174.87378
2110.0 0.000474 1803.87842 2179.47485
2115.0 0.000473 1801.18054 2175.25757
2119.0 0.000472 1798.49133 2164.57471
2121.0 0.000471 1795.81055 2151.78516
2124.0 0.000471 1793.13953 2140.25854
2128.0 0.000470 1790.47827 2130.57056
2134.0 0.000469 1787.82751 2122.09204
2136.0 0.000468 1785.18872 2114.05933
2136.0 0.000468 1782.56140 2105.80664
2132.0 0.000469 1779.94751 2097.48486
2128.0 0.000470 1777.34656 2089.22388
2120.0 0.000472 1774.75989 2081.61060
2111.0 0.000474 1772.18896 2075.23608
2103.0 0.000476 1769.63342 2070.47583
2096.0 0.000477 1767.09509 2067.70947
2092.0 0.000478 1764.57410 2066.87036
2090.0 0.000478 1762.07178 2067.75806
2090.0 0.000478 1759.58936 2070.74097
2091.0 0.000478 1757.12695 2075.13989
2095.0 0.000477 1754.68665 2080.49316
2100.0 0.000476 1752.26831 2086.32227
2106.0 0.000475 1749.87354 2091.92310
2111.0 0.000474 1747.50378 2097.39966
2116.0 0.000473 1745.15930 2102.31763
2121.0 0.000471 1742.84204 2106.40430
2122.0 0.000471 1740.55237 2109.57129
2120.0 0.000472 1738.29199 2110.99146
2116.0 0.000473 1736.06201 2110.84595
2110.0 0.000474 1733.86340 2109.22974
2102.0 0.000476 1731.69775 2106.33179
2091.0 0.000478 1729.56592 2102.56738
2080.0 0.000481 1727.46924 2098.25635
2070.0 0.000483 1725.40942 2093.62646
2062.0 0.000485 1723.38721 2088.80786
2055.0 0.000487 1721.40454 2083.93530
2051.0 0.000488 1719.46216 2079.11377
2048.0 0.000488 1717.56165 2074.34912
2047.0 0.000489 1715.70483 2069.73926
2048.0 0.000488 1713.89246 2065.18042
2048.0 0.000488 1712.12646 2060.54492
2049.0 0.000488 1710.40771 2056.26880
2053.0 0.000487 1708.73804 2052.03442
2054.0 0.000487 1707.11902 2047.80347
2054.0 0.000487 1705.55164 2043.60217
2054.0 0.000487 1704.03796 2039.48096
2052.0 0.000487 1702.57886 2035.48059
2048.0 0.000488 1701.17603 2031.64294
2045.0 0.000489 1699.83130 2028.05493
2040.0 0.000490 1698.54565 2024.83691
2037.0 0.000491 1697.32080 2022.09985
2035.0 0.000491 1696.15820 2019.92371
2033.0 0.000492 1695.05920 2018.36328
2032.0 0.000492 1694.02563 2017.68323
2032.0 0.000492 1693.05859 2017.75159
2034.0 0.000492 1692.15979 2018.61292
2037.0 0.000491 1691.33032 2020.25696
2042.0 0.000490 1690.57202 2022.47754
2047.0 0.000489 1689.88599 2025.47815
2051.0 0.000488 1689.27380 2028.90356
2053.0 0.000487 1688.73669 2032.44336
2053.0 0.000487 1688.27612 2035.90491
2054.0 0.000487 1687.89331 2039.10022
2054.0 0.000487 1687.58960 2041.90845
2055.0 0.000487 1687.36633 2044.36694
2055.0 0.000487 1687.22449 2046.43408
2056.0 0.000486 1687.16541 2048.32373
2057.0 0.000486 1687.19019 2050.23608
2059.0 0.000486 1687.29993 2052.26807
2064.0 0.000484 1687.49573 2054.61621
2068.0 0.000484 1687.77832 2057.28174
2077.0 0.000481 1688.14893 2060.41772
2087.0 0.000479 1688.60828 2063.77441
2099.0 0.000476 1689.15710 2067.51587
2113.0 0.000473 1689.79626 2071.17261
2129.0 0.000470 1690.52625 2074.72388
2146.0 0.000466 1691.34778 2078.01685
2160.0 0.000463 1692.26135 2080.96802
2173.0 0.000460 1693.26721 2083.21338
2184.0 0.000458 1694.36584 2084.81445
2190.0 0.000457 1695.55725 2085.75366
2190.0 0.000457 1696.84192 2086.09497
2186.0 0.000457 1698.21960 2085.94653
2180.0 0.000459 1699.68994 2085.43213
2171.0 0.000461 1701.25317 2084.66992
2161.0 0.000463 1702.90845 2083.70508
2151.0 0.000465 1704.65588 2082.72729
2140.0 0.000467 1706.49463 2081.54785
2133.0 0.000469 1708.42334 2080.33594
2126.0 0.000470 1710.44189 2079.09302
2118.0 0.000472 1712.54871 2077.82593
2113.0 0.000473 1714.74292 2076.49438
2108.0 0.000474 1717.02307 2075.07056
2103.0 0.000476 1719.38696 2073.57397
2098.0 0.000477 1721.83374 2071.93286
2092.0 0.000478 1724.36047 2070.11670
2086.0 0.000479 1726.96594 2068.11084
2083.0 0.000480 1729.64746 2065.98267
2078.0 0.000481 1732.40186 2063.79053
2073.0 0.000482 1735.22717 2060.90161
2068.0 0.000484 1738.11963 2058.78540
2062.0 0.000485 1741.07654 2056.95801
2055.0 0.000487 1744.09424 2055.29370
2047.0 0.000489 1747.16833 2053.91113
2042.0 0.000490 1750.29565 2052.81738
2034.0 0.000492 1753.47083 2051.95654
2028.0 0.000493 1756.69031 2051.28491
2023.0 0.000494 1759.94873 2050.68018
2018.0 0.000496 1763.24011 2049.67114
2013.0 0.000497 1766.56006 2048.40234
2010.0 0.000498 1769.90149 2047.02441
2008.0 0.000498 1773.25940 2045.68176
2009.0 0.000498 1776.62646 2044.65747
2011.0 0.000497 1779.99524 2044.12036
2015.0 0.000496 1783.35950 2044.15918
2018.0 0.000496 1786.71045 2044.79175
2019.0 0.000495 1790.04089 2046.03613
2021.0 0.000495 1793.34180 2047.99072
2024.0 0.000494 1796.60364 2050.51001
2025.0 0.000494 1799.81812 2053.63306
2026.0 0.000494 1802.97412 2057.28223
2026.0 0.000494 1806.06238 2061.33643
2028.0 0.000493 1809.07166 2065.63696
2030.0 0.000493 1811.98987 2070.05542
2032.0 0.000492 1814.80640 2074.38745
2034.0 0.000492 1817.50781 2078.54321
2038.0 0.000491 1820.08191 2082.37695
2043.0 0.000489 1822.51489 2085.81763
2046.0 0.000489 1824.79236 2088.80786
2049.0 0.000488 1826.90027 2091.32422
2053.0 0.000487 1828.82263 2093.38940
2056.0 0.000486 1830.54419 2095.08569
2062.0 0.000485 1832.04810 2096.53564
2067.0 0.000484 1833.31689 2097.87988
2072.0 0.000483 1834.33301 2099.23535
2075.0 0.000482 1835.07751 2100.78711
2078.0 0.000481 1835.53149 2102.57617
2081.0 0.000481 1835.67444 2104.76099
2081.0 0.000481 1835.48572 2107.35205
2080.0 0.000481 1834.94360 2110.37524
2078.0 0.000481 1834.02588 2113.38965
2077.0 0.000481 1832.70898 2117.07983
2079.0 0.000481 1830.96887 2120.84570
2080.0 0.000481 1828.78101 2124.39844
2083.0 0.000480 1826.11865 2127.35327
2086.0 0.000479 1822.95618 2129.23706
2092.0 0.000478 1819.26465 2129.52832
2097.0 0.000477 1815.01599 2127.76807
2100.0 0.000476 1810.18115 2123.71924
2100.0 0.000476 1804.72803 2117.42065
2101.0 0.000476 1798.62671 2109.14673
2101.0 0.000476 1791.84229 2099.23633
2100.0 0.000476 1784.34204 2088.02490
2099.0 0.000476 1776.09216 2075.80054
2096.0 0.000477 1767.05396 2062.80542
2092.0 0.000478 1757.19299 2049.24292
2087.0 0.000479 1746.46777 2035.25452
2083.0 0.000480 1734.83997 2020.92249
2078.0 0.000481 1722.27039 2006.27319
2072.0 0.000483 1708.71326 1991.29419
2065.0 0.000484 1694.12891 1975.98633
2059.0 0.000486 1678.46802 1960.43286
2055.0 0.000487 1661.68628 1944.86487
2052.0 . . .
