Information card for entry 2005088

Structure parameters

• Chemical name: bis(1,4,7,10–tetraoxacyclododecane)lithium(1+) bis[(1,2,3,3a,7a–η)–4,5,6,7–tetrahydro–4,7–methanoindenido] lithate(1-)
• Formula: C36 H54 Li2 O8
• Calculated formula: C36 H54 Li2 O8
• Title of publication: Two Derivatives of Lithium Isodicyclopentadienide: [(1,2,3,3a,7a-η)-4,5,6,7-Tetrahydro-4,7-methanoindenido](<i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'-tetramethylethylenediamine)lithium and Bis(1,4,7,10-tetraoxacyclododecane)lithium(1+) Bis[(1,2,3,3a,7a-η)-4,5,6,7-tetrahydro-4,7-methanoindenido]lithate(1–)
• Authors of publication: Gallucci, J. C.; Sivik, M. R.; Paquette, L. A.; Zaegel, F.; Meunier, P.; Gautheron, B.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 7
• Pages of publication: 1673 - 1679
• a: 11.818 ± 0.001 Å
• b: 16.129 ± 0.002 Å
• c: 9.871 ± 0.001 Å
• α: 107.05 ± 0.01°
• β: 108.23 ± 0.01°
• γ: 88.7 ± 0.01°
• Cell volume: 1703.6 ± 0.3 ų
• Cell temperature: 203 K
• Ambient diffraction temperature: 203 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for all reflections: 0.056
• Weighted residual factors for significantly intense reflections: 0.0555
• Goodness-of-fit parameter for all reflections: 1.706
• Goodness-of-fit parameter for significantly intense reflections: 1.706
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No