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Information card for entry 4064373
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Coordinates | 4064373.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Lithium[2-(1,3-bis-(2',6'-dimethylphenyl)[1,3,2]diazaphospholenyl-3- diphenylphosphino-1-cyanoethanide]dichloropalladium(II) |
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Formula | C41 H45 Cl2 Li N6 P2 Pd |
Calculated formula | C41 H45 Cl2 Li N6 P2 Pd |
Title of publication | Synthesis and Characterization of an Unsymmetrical 1,2-Diphosphinoethanide Complex |
Authors of publication | Förster, Daniela; Nieger, Martin; Gudat, Dietrich |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 9 |
Pages of publication | 2628 |
a | 10.471 ± 0.001 Å |
b | 14.436 ± 0.001 Å |
c | 15.933 ± 0.002 Å |
α | 107.57 ± 0.01° |
β | 102.66 ± 0.01° |
γ | 109.74 ± 0.01° |
Cell volume | 2018 ± 0.5 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1169 |
Residual factor for significantly intense reflections | 0.0696 |
Weighted residual factors for significantly intense reflections | 0.1637 |
Weighted residual factors for all reflections included in the refinement | 0.1911 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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