Information card for entry 4064389

Structure parameters

• Formula: C40 H32 Cl4 Ni O3 P2
• Calculated formula: C40 H32 Cl4 Ni O3 P2
• Title of publication: Oxidative Addition of a Diphosphine Anhydride to Iron(0) and Nickel(0): A Simple Approach to Installing Four Ligands
• Authors of publication: Ringenberg, Mark R.; Gray, Danielle L.; Rauchfuss, Thomas B.
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 10
• Pages of publication: 2885
• a: 9.2924 ± 0.0007 Å
• b: 12.4785 ± 0.001 Å
• c: 17.5116 ± 0.0014 Å
• α: 88.217 ± 0.005°
• β: 75.154 ± 0.004°
• γ: 70.221 ± 0.004°
• Cell volume: 1843.5 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0795
• Weighted residual factors for all reflections included in the refinement: 0.085
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No