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Information card for entry 4064418
Preview
Coordinates | 4064418.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Acetonitrile-dibromo-(9,9-dimethyl-4,5-bis(diphenylphosphino)-9-silaxanthene-P,P')-nitrosyl-rhenium(I) dichloromethane solvate |
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Formula | C42 H39 Br2 Cl4 N2 O2 P2 Re Si |
Calculated formula | C42 H39 Br2 Cl4 N2 O2 P2 Re Si |
Title of publication | Rhenium Nitrosyl Complexes Bearing Large-Bite-Angle Diphosphines |
Authors of publication | Dudle, Balz; Rajesh, Kunjanpillai; Blacque, Olivier; Berke, Heinz |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 11 |
Pages of publication | 2986 |
a | 11.2933 ± 0.0002 Å |
b | 27.3351 ± 0.0004 Å |
c | 14.7027 ± 0.0002 Å |
α | 90° |
β | 92.782 ± 0.002° |
γ | 90° |
Cell volume | 4533.43 ± 0.12 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 9 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.061 |
Residual factor for significantly intense reflections | 0.032 |
Weighted residual factors for significantly intense reflections | 0.047 |
Weighted residual factors for all reflections included in the refinement | 0.05 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.85 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064418.html
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