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Information card for entry 4064421
Preview
Coordinates | 4064421.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | Chloro-dihydrido-(1,1'-bis(diisopropylphosphino)ferrocene-P,P')-nitrosyl-trichlorosilyl-rhenium(I) |
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Formula | C22 H38 Cl4 Fe N O P2 Re Si |
Calculated formula | C22 H38 Cl4 Fe N O P2 Re Si |
Title of publication | Rhenium Nitrosyl Complexes Bearing Large-Bite-Angle Diphosphines |
Authors of publication | Dudle, Balz; Rajesh, Kunjanpillai; Blacque, Olivier; Berke, Heinz |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 11 |
Pages of publication | 2986 |
a | 8.8694 ± 0.0001 Å |
b | 9.7012 ± 0.0002 Å |
c | 17.26 ± 0.0003 Å |
α | 79.778 ± 0.002° |
β | 82.725 ± 0.001° |
γ | 84.055 ± 0.001° |
Cell volume | 1444.77 ± 0.04 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0237 |
Residual factor for significantly intense reflections | 0.0203 |
Weighted residual factors for significantly intense reflections | 0.0463 |
Weighted residual factors for all reflections included in the refinement | 0.047 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064421.html
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