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Information card for entry 4064873
Preview
Coordinates | 4064873.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H37 Cl N2 O Si |
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Calculated formula | C25 H37 Cl N2 O Si |
SMILES | C1(c2ccccc2)=[N](C(C)(C)C)[Si]2(C3(C4CC5CC(C4)CC3C5)O2)(Cl)N1C(C)(C)C |
Title of publication | Reactions of StableN-Heterocyclic Silylenes with Ketones and 3,5-Di-tert-butyl-o-benzoquinone |
Authors of publication | Azhakar, Ramachandran; Ghadwal, Rajendra S.; Roesky, Herbert W.; Hey, Jakob; Stalke, Dietmar |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 14 |
Pages of publication | 3853 |
a | 15.4914 ± 0.0014 Å |
b | 11.6071 ± 0.001 Å |
c | 13.5417 ± 0.0012 Å |
α | 90° |
β | 104.728 ± 0.002° |
γ | 90° |
Cell volume | 2354.9 ± 0.4 Å3 |
Cell temperature | 90 ± 2 K |
Ambient diffraction temperature | 90 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0403 |
Residual factor for significantly intense reflections | 0.0366 |
Weighted residual factors for significantly intense reflections | 0.0942 |
Weighted residual factors for all reflections included in the refinement | 0.0964 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.122 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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