Information card for entry 4064901

Structure parameters

• Formula: C88 H106 O1.63 Sn2
• Calculated formula: C88 H106 O1.64 Sn2.02
• Title of publication: Tethered Heavy Dicarbene Analogues: Synthesis and Structure of Ditetryldiyl Ethers (Ar′E)2(μ-O) (E = Ge, Sn; Ar′ = C6H3-2,6-(C6H3-2,6-iPr2)2)
• Authors of publication: Summerscales, Owen T.; Olmstead, Marilyn M.; Power, Philip P.
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 13
• Pages of publication: 3468
• a: 11.9117 ± 0.0008 Å
• b: 13.3946 ± 0.0004 Å
• c: 13.7183 ± 0.0005 Å
• α: 111.263 ± 0.002°
• β: 103.04 ± 0.002°
• γ: 102.296 ± 0.002°
• Cell volume: 1879.52 ± 0.16 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0274
• Residual factor for significantly intense reflections: 0.0239
• Weighted residual factors for significantly intense reflections: 0.0614
• Weighted residual factors for all reflections included in the refinement: 0.0633
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No