Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4064902
Preview
Coordinates | 4064902.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H37 Ge O0.62 |
---|---|
Calculated formula | C30 H37 Ge O0.6232 |
Title of publication | Tethered Heavy Dicarbene Analogues: Synthesis and Structure of Ditetryldiyl Ethers (Ar′E)2(μ-O) (E = Ge, Sn; Ar′ = C6H3-2,6-(C6H3-2,6-iPr2)2) |
Authors of publication | Summerscales, Owen T.; Olmstead, Marilyn M.; Power, Philip P. |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 13 |
Pages of publication | 3468 |
a | 9.1539 ± 0.0003 Å |
b | 12.7546 ± 0.0005 Å |
c | 13.0263 ± 0.0005 Å |
α | 63.729 ± 0.002° |
β | 81.404 ± 0.002° |
γ | 69.289 ± 0.002° |
Cell volume | 1275.61 ± 0.09 Å3 |
Cell temperature | 90 ± 2 K |
Ambient diffraction temperature | 90 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0263 |
Residual factor for significantly intense reflections | 0.0249 |
Weighted residual factors for significantly intense reflections | 0.0619 |
Weighted residual factors for all reflections included in the refinement | 0.063 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.647 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064902.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.