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Information card for entry 4064903
Preview
Coordinates | 4064903.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H70 Cl6 O9 P S4 V |
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Calculated formula | C65 H68 Cl4 O9 P S4 V |
Title of publication | Ethylene Polymerization Catalysis by Vanadium-Based Systems Bearing Sulfur-Bridged Calixarenes |
Authors of publication | Redshaw, Carl; Clowes, Lucy; Hughes, David L.; Elsegood, Mark R. J.; Yamato, Takehiko |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 21 |
Pages of publication | 5620 |
a | 11.7107 ± 0.0002 Å |
b | 14.4377 ± 0.0004 Å |
c | 22.2159 ± 0.0005 Å |
α | 89.098 ± 0.002° |
β | 77.16 ± 0.002° |
γ | 75.928 ± 0.002° |
Cell volume | 3549.43 ± 0.15 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 140 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1121 |
Residual factor for significantly intense reflections | 0.0649 |
Weighted residual factors for significantly intense reflections | 0.1592 |
Weighted residual factors for all reflections included in the refinement | 0.1725 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.968 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064903.html
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