Crystallography Open Database

Information card for entry 4065288

Preview

Coordinates	4065288.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H69 Cl N2 P2 Rh
Calculated formula	C43 H66 Cl N2 P2 Rh
Title of publication	Synthesis of Rhodium(I) Complexes Bearing Bidentate NH,NR-NHC/Phosphine Ligands
Authors of publication	Naziruddin, Abbas Raja; Hepp, Alexander; Pape, Tania; Hahn, F. Ekkehardt
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	21
Pages of publication	5859
a	9.5232 ± 0.0005 Å
b	10.4892 ± 0.0006 Å
c	21.0399 ± 0.0012 Å
α	86.62 ± 0.001°
β	86.903 ± 0.001°
γ	79.1 ± 0.001°
Cell volume	2058.2 ± 0.2 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0915
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.1247
Weighted residual factors for all reflections included in the refinement	0.1419
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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