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Information card for entry 4065295
Preview
Coordinates | 4065295.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H34 Cl3 O2 P2 Rh |
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Calculated formula | C41 H34 Cl3 O2 P2 Rh |
Title of publication | Mechanistic Study of Rhodium/xantphos-Catalyzed Methanol Carbonylation |
Authors of publication | Williams, Gary L.; Parks, Christopher M.; Smith, C. Robert; Adams, Harry; Haynes, Anthony; Meijer, Anthony J. H. M.; Sunley, Glenn J.; Gaemers, Sander |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 22 |
Pages of publication | 6166 |
a | 11.952 ± 0.013 Å |
b | 18.106 ± 0.02 Å |
c | 17.351 ± 0.019 Å |
α | 90° |
β | 95.47 ± 0.018° |
γ | 90° |
Cell volume | 3738 ± 7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0524 |
Residual factor for significantly intense reflections | 0.0342 |
Weighted residual factors for significantly intense reflections | 0.0763 |
Weighted residual factors for all reflections included in the refinement | 0.0838 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065295.html
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Users of the data should acknowledge the original authors of the
structural data.