Crystallography Open Database

Information card for entry 4065432

Preview

Coordinates	4065432.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H60 Br4 Cu4 O4 P4
Calculated formula	C72 H60 Br4 Cu4 O4 P4
Title of publication	Novel Phosphinite and Phosphonite Copper(I) Complexes: Efficient Catalysts for Click Azide‒Alkyne Cycloaddition Reactions
Authors of publication	Lal, Steven; McNally, Jayne; White, Andrew J. P.; Díez-González, Silvia
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	22
Pages of publication	6225
a	17.3739 ± 0.0004 Å
b	20.9402 ± 0.0004 Å
c	19.1287 ± 0.0003 Å
α	90°
β	97.8271 ± 0.0017°
γ	90°
Cell volume	6894.4 ± 0.2 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.077
Residual factor for significantly intense reflections	0.0311
Weighted residual factors for significantly intense reflections	0.052
Weighted residual factors for all reflections included in the refinement	0.0559
Goodness-of-fit parameter for all reflections included in the refinement	0.868
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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