Information card for entry 4065451

Structure parameters

• Formula: C21 H32 B2 N O5
• Calculated formula: C21 H32 B2 N O5
• Title of publication: Magnesium-Catalyzed Hydroboration of Pyridines
• Authors of publication: Arrowsmith, Merle; Hill, Michael S.; Hadlington, Terrance; Kociok-Köhn, Gabriele; Weetman, Catherine
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 21
• Pages of publication: 5556
• a: 10.2451 ± 0.0003 Å
• b: 11.5707 ± 0.0004 Å
• c: 19.7004 ± 0.0006 Å
• α: 90°
• β: 103.599 ± 0.002°
• γ: 90°
• Cell volume: 2269.87 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0865
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1323
• Weighted residual factors for all reflections included in the refinement: 0.1531
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No