Information card for entry 4065466

Structure parameters

• Formula: C23 H30 Ge N2
• Calculated formula: C23 H30 Ge N2
• SMILES: [GeH]1[N](=C(C)C=C(N1c1c(cc(cc1C)C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Synthesis, Characterization, and Reactivity of an N-Heterocyclic Germanium(II) Hydride: Reversible Hydrogermylation of a Phosphaalkyne
• Authors of publication: Choong, Sam L.; Woodul, William D.; Schenk, Christian; Stasch, Andreas; Richards, Anne F.; Jones, Cameron
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 20
• Pages of publication: 5543
• a: 7.193 ± 0.0014 Å
• b: 24.351 ± 0.005 Å
• c: 12.147 ± 0.002 Å
• α: 90°
• β: 99.41 ± 0.03°
• γ: 90°
• Cell volume: 2099 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0944
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1116
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No