Information card for entry 4065471

Structure parameters

• Chemical name: N,N'-(3,7-Diallyl-3,7-diaza-bicyclo[3.3.1]nonane(N,N'-Diallyl-bispidine))- di-acetylacetonato-nickel(II)
• Formula: C23 H36 N2 Ni O4
• Calculated formula: C23 H36 N2 Ni O4
• Title of publication: Synthesis and Coordination Chemistry ofN,N-Diallylbispidine
• Authors of publication: Cui, Huiling; Goddard, Richard; Pörschke, Klaus-Richard
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 22
• Pages of publication: 6241
• a: 11.4068 ± 0.001 Å
• b: 12.8159 ± 0.0012 Å
• c: 16.1676 ± 0.0015 Å
• α: 90°
• β: 99.213 ± 0.002°
• γ: 90°
• Cell volume: 2333 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0751
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No