Information card for entry 4077548

Structure parameters

• Formula: C27 H39 N3 Si2 W
• Calculated formula: C27 H39 N3 Si2 W
• Title of publication: Synthesis of d2Tungsten Arene Complexes and Their Reaction with Diphenylacetylene
• Authors of publication: Mills, R. C.; Abboud, K. A.; Boncella, J. M.
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 16
• Pages of publication: 2953
• a: 12.1874 ± 0.0005 Å
• b: 15.6037 ± 0.0007 Å
• c: 14.5968 ± 0.0006 Å
• α: 90°
• β: 94.317 ± 0.001°
• γ: 90°
• Cell volume: 2768 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0798
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0553
• Weighted residual factors for all reflections included in the refinement: 0.0642
• Goodness-of-fit parameter for all reflections included in the refinement: 0.961
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No