Information card for entry 4078490

Structure parameters

• Formula: C37 H62 B2 N12 Si U
• Calculated formula: C37 H62 B2 N12 Si U
• Title of publication: Use of Alkylsodium Reagents for the Synthesis of Trivalent Uranium Alkyl Complexes
• Authors of publication: Matson, Ellen M.; Forrest, William P.; Fanwick, Phillip E.; Bart, Suzanne C.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 12
• Pages of publication: 4467
• a: 12.6822 ± 0.0008 Å
• b: 13.1029 ± 0.001 Å
• c: 14.4609 ± 0.001 Å
• α: 78.889 ± 0.005°
• β: 66.013 ± 0.005°
• γ: 84.836 ± 0.004°
• Cell volume: 2154.2 ± 0.3 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for significantly intense reflections: 0.129
• Weighted residual factors for all reflections included in the refinement: 0.138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CU-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No