Information card for entry 4079488

Structure parameters

• Formula: C47 H55 F3 N6 O5 Rh S
• Calculated formula: C46 H58 N6 O2 Rh
• Title of publication: Synthesis and Characterization of Cationic Rhodium Peroxo Complexes
• Authors of publication: Cipot-Wechsler, Judy; Covelli, Danielle; Praetorius, Jeremy M.; Hearns, Nigel; Zenkina, Olena V.; Keske, Eric C.; Wang, Ruiyao; Kennepohl, Pierre; Crudden, Cathleen M.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 21
• Pages of publication: 7306
• a: 32.344 ± 0.003 Å
• b: 8.6387 ± 0.0008 Å
• c: 33.322 ± 0.003 Å
• α: 90°
• β: 95.251 ± 0.002°
• γ: 90°
• Cell volume: 9271.4 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0927
• Weighted residual factors for significantly intense reflections: 0.2139
• Weighted residual factors for all reflections included in the refinement: 0.216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No