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Information card for entry 4083736
Preview
Coordinates | 4083736.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H28 N4 O8 Pd2 |
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Calculated formula | C28 H28 N4 O8 Pd2 |
SMILES | [Pd]123([n]4c(OC)cccc4c4c1ccc(OC)n4)[Pd]1([n]4c(OC)cccc4c4c1ccc(OC)n4)([O]=C(O2)C)OC(=[O]3)C |
Title of publication | Synthesis and Characterization of Palladium(II) and Platinum(II) Adducts and Cyclometalated Complexes of 6,6′-Dimethoxy-2,2′-bipyridine: C(sp3)‒H and C(sp2)‒H Bond Activations |
Authors of publication | Cocco, Fabio; Zucca, Antonio; Stoccoro, Sergio; Serratrice, Maria; Guerri, Annalisa; Cinellu, Maria A. |
Journal of publication | Organometallics |
Year of publication | 2014 |
Pages of publication | 140624160931008 |
a | 10.729 ± 0.0005 Å |
b | 13.9982 ± 0.0008 Å |
c | 20.103 ± 0.001 Å |
α | 90° |
β | 103.084 ± 0.006° |
γ | 90° |
Cell volume | 2940.8 ± 0.3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0566 |
Residual factor for significantly intense reflections | 0.0368 |
Weighted residual factors for significantly intense reflections | 0.078 |
Weighted residual factors for all reflections included in the refinement | 0.0923 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4083736.html
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