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Information card for entry 4083782
Preview
Coordinates | 4083782.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H18 Br2 Cl0.25 N4 Pd |
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Calculated formula | C16.873 H17.873 Br2 Cl0.254 N3.873 Pd |
Title of publication | Palladium(II) Complexes Bearing an Indazole-Derived N-Heterocyclic Carbene and Phosphine Coligands as Catalysts for the Sonogashira Coupling and the Hydroamination of Alkynes |
Authors of publication | Bernhammer, Jan C.; Chong, Ning Xi; Jothibasu, Ramasamy; Zhou, Binbin; Huynh, Han Vinh |
Journal of publication | Organometallics |
Year of publication | 2014 |
Pages of publication | 140627160434001 |
a | 13.4325 ± 0.0006 Å |
b | 10.2745 ± 0.0004 Å |
c | 13.8594 ± 0.0006 Å |
α | 90° |
β | 98.377 ± 0.002° |
γ | 90° |
Cell volume | 1892.36 ± 0.14 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0372 |
Residual factor for significantly intense reflections | 0.0291 |
Weighted residual factors for significantly intense reflections | 0.0663 |
Weighted residual factors for all reflections included in the refinement | 0.0693 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4083782.html
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