Crystallography Open Database

Information card for entry 4121358

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Coordinates	4121358.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H56 O2 P2 Ru Si2
Calculated formula	C34 H56 O2 P2 Ru Si2
Title of publication	Reversible Insertion of Carbenes into Ruthenium-Silicon Bonds
Authors of publication	María J. Bernal; Olga Torres; Marta Martín; Eduardo Sola
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	19008 - 19015
a	11.4424 ± 0.0005 Å
b	18.9456 ± 0.0008 Å
c	33.3086 ± 0.0015 Å
α	90°
β	93.922 ± 0.001°
γ	90°
Cell volume	7203.8 ± 0.5 Å³
Cell temperature	100 ± 0.2 K
Ambient diffraction temperature	100 ± 0.2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0344
Residual factor for significantly intense reflections	0.0305
Weighted residual factors for significantly intense reflections	0.0705
Weighted residual factors for all reflections included in the refinement	0.0726
Goodness-of-fit parameter for all reflections included in the refinement	1.101
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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