#------------------------------------------------------------------------------
#$Date: 2016-03-22 22:19:23 +0100 (mar 22 de mar de 2016) $
#$Revision: 179055 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/17/4301727.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4301727
loop_
_publ_author_name
'Liam P. Spencer'
'Ping Yang'
'Brian L. Scott'
'Enrique R. Batista'
'James M. Boncella'
_publ_section_title
;
Uranium(VI) Bis(imido) Chalcogenate Complexes: Synthesis and Density
Functional Theory Analysis
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2693
_journal_page_last               2700
_journal_paper_doi               10.1021/ic802212m
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C64 H74 N2 O4 P2 U'
_chemical_formula_weight         1235.22
_chemical_name_systematic
; 

 ? 

;
_space_group_IT_number           69
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-F 2 2'
_symmetry_space_group_name_H-M   'F m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.516(2)
_cell_length_b                   17.417(4)
_cell_length_c                   19.897(3)
_cell_measurement_temperature    120(1)
_cell_volume                     5723.6(17)
_computing_cell_refinement       'SAINT+, v. 7.06 (Bruker AXS, 2001)'
_computing_data_collection       'APEX II, v. 1.08 (Bruker AXS, 2003)'
_computing_data_reduction        'SAINT+, v. 7.06 (Bruker AXS, 2001)'
_computing_molecular_graphics    'SHELXTL, v. 6.10, (Bruker AXS, 2000)'
_computing_publication_material  'SHELXTL, v. 6.10, (Bruker AXS, 2000)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(1)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.953
_diffrn_measurement_device_type  'Bruker D8 with APEXII CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0533
_diffrn_reflns_av_sigmaI/netI    0.0317
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            16034
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         28.35
_diffrn_reflns_theta_min         1.98
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.940
_exptl_absorpt_correction_T_max  0.7192
_exptl_absorpt_correction_T_min  0.6836
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS 2.03 (Sheldrick, 2001)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.433
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'multifaceted block'
_exptl_crystal_F_000             2504
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.440
_refine_diff_density_min         -0.900
_refine_diff_density_rms         0.120
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.099
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     249
_refine_ls_number_reflns         1871
_refine_ls_number_restraints     22
_refine_ls_restrained_S_all      1.146
_refine_ls_R_factor_all          0.0279
_refine_ls_R_factor_gt           0.0279
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0571P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0714
_refine_ls_wR_factor_ref         0.0714
_reflns_number_gt                1871
_reflns_number_total             1871
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic802212m_si_001_1.cif
_cod_data_source_block           apx456d
_cod_original_cell_volume        5723.5(16)
_cod_database_code               4301727
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'-x, y+1/2, -z+1/2'
'x, -y+1/2, -z+1/2'
'x+1/2, y, z+1/2'
'-x+1/2, -y, z+1/2'
'-x+1/2, y, -z+1/2'
'x+1/2, -y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, -z'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x, -y+1/2, -z+1/2'
'x, y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'
'-x, y+1/2, z+1/2'
'-x+1/2, -y, -z+1/2'
'x+1/2, y, -z+1/2'
'x+1/2, -y, z+1/2'
'-x+1/2, y, z+1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z'
'x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.0000 0.5000 0.0000 0.01154(11) Uani 1 8 d S . .
P1 P 0.08386(14) 0.5000 0.17846(11) 0.0235(5) Uani 0.50 2 d SP . .
O1 O 0.0510(5) 0.4797(4) 0.1082(4) 0.0158(18) Uani 0.25 1 d P . .
N1 N 0.0000 0.6070(4) 0.0000 0.0415(17) Uani 1 4 d S . .
O2 O -0.1263(4) 0.5000 0.0447(3) 0.0300(15) Uani 0.50 2 d SP . .
C1 C 0.0000 0.6888(5) 0.0000 0.068(4) Uani 1 4 d SD . .
C2 C -0.0675(7) 0.7178(8) -0.0462(6) 0.058(3) Uani 0.38 1 d PDU . .
C3 C 0.0217(7) 0.7267(7) 0.0604(5) 0.058(3) Uani 0.38 1 d PDU . .
C5 C -0.1834(4) 0.4591(4) 0.0644(4) 0.016(2) Uani 0.25 1 d PG . .
C6 C -0.1567(4) 0.3892(5) 0.0898(5) 0.024(3) Uani 0.25 1 d PG . .
C7 C -0.2120(6) 0.3312(4) 0.1037(5) 0.035(3) Uani 0.25 1 d PG . .
C8 C -0.2941(5) 0.3431(5) 0.0922(5) 0.031(3) Uani 0.25 1 d PG . .
C9 C -0.3208(4) 0.4130(6) 0.0668(5) 0.028(3) Uani 0.25 1 d PG . .
C10 C -0.2655(5) 0.4710(4) 0.0529(4) 0.023(3) Uani 0.25 1 d PGD . .
C11 C 0.0123(6) 0.4572(5) 0.2290(4) 0.019(3) Uani 0.25 1 d PG . .
C12 C 0.0300(5) 0.4390(6) 0.2954(4) 0.031(3) Uani 0.25 1 d PG . .
C13 C -0.0251(5) 0.3975(6) 0.3337(3) 0.038(4) Uani 0.25 1 d PG . .
C14 C -0.0981(5) 0.3742(6) 0.3055(4) 0.030(3) Uani 0.25 1 d PG . .
C15 C -0.1159(5) 0.3924(7) 0.2391(4) 0.029(4) Uani 0.25 1 d PG . .
C16 C -0.0607(6) 0.4339(6) 0.2009(3) 0.023(3) Uani 0.25 1 d PG . .
C23 C 0.1023(5) 0.5990(4) 0.2197(5) 0.016(3) Uani 0.25 1 d PG . .
C24 C 0.0386(4) 0.6363(5) 0.2517(5) 0.033(3) Uani 0.25 1 d PG . .
C25 C 0.0484(5) 0.7111(5) 0.2747(5) 0.046(4) Uani 0.25 1 d PG . .
C26 C 0.1219(5) 0.7486(4) 0.2657(4) 0.030(4) Uani 0.25 1 d PG . .
C27 C 0.1856(4) 0.7113(4) 0.2338(4) 0.026(3) Uani 0.25 1 d PG . .
C28 C 0.1758(4) 0.6366(4) 0.2107(4) 0.020(2) Uani 0.25 1 d PG . .
C17 C 0.1765(4) 0.4549(4) 0.1762(4) 0.016(2) Uani 0.25 1 d PG . .
C18 C 0.1937(5) 0.4140(5) 0.1180(3) 0.023(2) Uani 0.25 1 d PG . .
C19 C 0.2632(5) 0.3691(5) 0.1144(4) 0.028(3) Uani 0.25 1 d PG . .
C20 C 0.3155(4) 0.3653(5) 0.1691(5) 0.029(3) Uani 0.25 1 d PG . .
C21 C 0.2983(5) 0.4062(5) 0.2273(4) 0.028(3) Uani 0.25 1 d PG . .
C22 C 0.2288(5) 0.4511(5) 0.2309(3) 0.022(2) Uani 0.25 1 d PG . .
C10A C -0.2996(9) 0.5488(8) 0.0313(7) 0.028(3) Uani 0.25 1 d PD . .
C10B C -0.2649(10) 0.5773(9) -0.0370(6) 0.031(3) Uani 0.25 1 d PD . .
C10C C -0.2818(10) 0.6073(9) 0.0856(6) 0.029(3) Uani 0.25 1 d PD . .
C10D C -0.3935(7) 0.5468(10) 0.0213(8) 0.044(4) Uani 0.25 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 U1 N1 180.0 17_565 . ?
N1 U1 O2 89.999(1) 17_565 18 ?
N1 U1 O2 90.000(1) . 18 ?
N1 U1 O2 89.998(1) 17_565 . ?
N1 U1 O2 90.000(1) . . ?
O2 U1 O2 46.1(3) 18 . ?
N1 U1 O2 90.0 17_565 17_565 ?
N1 U1 O2 90.000(1) . 17_565 ?
O2 U1 O2 133.9(3) 18 17_565 ?
O2 U1 O2 180.0 . 17_565 ?
N1 U1 O2 90.001(1) 17_565 2_565 ?
N1 U1 O2 90.000(1) . 2_565 ?
O2 U1 O2 180.0 18 2_565 ?
O2 U1 O2 133.9(3) . 2_565 ?
O2 U1 O2 46.1(3) 17_565 2_565 ?
N1 U1 O1 81.30(17) 17_565 20 ?
N1 U1 O1 98.69(17) . 20 ?
O2 U1 O1 91.7(3) 18 20 ?
O2 U1 O1 46.2(2) . 20 ?
O2 U1 O1 133.8(2) 17_565 20 ?
O2 U1 O1 88.3(3) 2_565 20 ?
N1 U1 O1 98.69(17) 17_565 2_565 ?
N1 U1 O1 81.30(17) . 2_565 ?
O2 U1 O1 91.7(3) 18 2_565 ?
O2 U1 O1 46.2(2) . 2_565 ?
O2 U1 O1 133.8(2) 17_565 2_565 ?
O2 U1 O1 88.3(3) 2_565 2_565 ?
O1 U1 O1 17.4(3) 20 2_565 ?
N1 U1 O1 98.70(17) 17_565 19_565 ?
N1 U1 O1 81.30(17) . 19_565 ?
O2 U1 O1 133.8(2) 18 19_565 ?
O2 U1 O1 88.3(3) . 19_565 ?
O2 U1 O1 91.7(3) 17_565 19_565 ?
O2 U1 O1 46.2(2) 2_565 19_565 ?
O1 U1 O1 46.0(4) 20 19_565 ?
O1 U1 O1 42.2(4) 2_565 19_565 ?
N1 U1 O1 81.30(17) 17_565 . ?
N1 U1 O1 98.70(17) . . ?
O2 U1 O1 133.8(2) 18 . ?
O2 U1 O1 88.3(3) . . ?
O2 U1 O1 91.7(3) 17_565 . ?
O2 U1 O1 46.2(2) 2_565 . ?
O1 U1 O1 42.2(4) 20 . ?
O1 U1 O1 46.0(4) 2_565 . ?
O1 U1 O1 17.4(3) 19_565 . ?
N1 U1 O1 81.31(17) 17_565 3 ?
N1 U1 O1 98.69(17) . 3 ?
O2 U1 O1 46.2(2) 18 3 ?
O2 U1 O1 91.7(3) . 3 ?
O2 U1 O1 88.3(3) 17_565 3 ?
O2 U1 O1 133.8(2) 2_565 3 ?
O1 U1 O1 134.0(4) 20 3 ?
O1 U1 O1 137.8(4) 2_565 3 ?
O1 U1 O1 179.998(1) 19_565 3 ?
O1 U1 O1 162.6(3) . 3 ?
N1 U1 O1 98.70(17) 17_565 17_565 ?
N1 U1 O1 81.30(17) . 17_565 ?
O2 U1 O1 46.2(2) 18 17_565 ?
O2 U1 O1 91.7(3) . 17_565 ?
O2 U1 O1 88.3(3) 17_565 17_565 ?
O2 U1 O1 133.8(2) 2_565 17_565 ?
O1 U1 O1 137.8(4) 20 17_565 ?
O1 U1 O1 134.0(4) 2_565 17_565 ?
O1 U1 O1 162.6(3) 19_565 17_565 ?
O1 U1 O1 180.0(3) . 17_565 ?
O1 U1 O1 17.4(3) 3 17_565 ?
C16 P1 C16 125.9(12) 2_565 20 ?
C16 P1 O1 114.4(8) 2_565 . ?
C16 P1 O1 90.2(5) 20 . ?
C16 P1 O1 90.2(8) 2_565 19_565 ?
C16 P1 O1 114.4(4) 20 19_565 ?
O1 P1 O1 26.5(5) . 19_565 ?
C16 P1 C17 82.3(8) 2_565 19_565 ?
C16 P1 C17 132.7(5) 20 19_565 ?
O1 P1 C17 113.3(4) . 19_565 ?
O1 P1 C17 100.7(4) 19_565 19_565 ?
C16 P1 C17 132.7(8) 2_565 . ?
C16 P1 C17 82.3(6) 20 . ?
O1 P1 C17 100.7(4) . . ?
O1 P1 C17 113.3(4) 19_565 . ?
C17 P1 C17 54.3(5) 19_565 . ?
C16 P1 C11 37.8(8) 2_565 19_565 ?
C16 P1 C11 88.9(8) 20 19_565 ?
O1 P1 C11 112.8(4) . 19_565 ?
O1 P1 C11 100.9(4) 19_565 19_565 ?
C17 P1 C11 115.4(4) 19_565 19_565 ?
C17 P1 C11 145.4(4) . 19_565 ?
C16 P1 C11 88.9(9) 2_565 . ?
C16 P1 C11 37.8(6) 20 . ?
O1 P1 C11 100.9(4) . . ?
O1 P1 C11 112.8(4) 19_565 . ?
C17 P1 C11 145.4(4) 19_565 . ?
C17 P1 C11 115.4(4) . . ?
C11 P1 C11 51.2(6) 19_565 . ?
C16 P1 C23 134.0(8) 2_565 19_565 ?
C16 P1 C23 26.6(5) 20 19_565 ?
O1 P1 C23 103.6(4) . 19_565 ?
O1 P1 C23 130.2(4) 19_565 19_565 ?
C17 P1 C23 106.1(4) 19_565 19_565 ?
C17 P1 C23 57.6(4) . 19_565 ?
C11 P1 C23 104.2(4) 19_565 19_565 ?
C11 P1 C23 58.3(4) . 19_565 ?
C16 P1 C23 26.6(7) 2_565 . ?
C16 P1 C23 134.0(6) 20 . ?
O1 P1 C23 130.2(4) . . ?
O1 P1 C23 103.6(4) 19_565 . ?
C17 P1 C23 57.6(4) 19_565 . ?
C17 P1 C23 106.1(4) . . ?
C11 P1 C23 58.3(4) 19_565 . ?
C11 P1 C23 104.2(4) . . ?
C23 P1 C23 126.2(6) 19_565 . ?
C16 P1 C11 85.6(9) 2_565 20 ?
C16 P1 C11 42.9(4) 20 20 ?
O1 P1 C11 95.2(4) . 20 ?
O1 P1 C11 105.0(4) 19_565 20 ?
C17 P1 C11 151.6(4) 19_565 20 ?
C17 P1 C11 122.9(3) . 20 ?
C11 P1 C11 47.9(5) 19_565 20 ?
C11 P1 C11 8.4(4) . 20 ?
C23 P1 C11 65.4(3) 19_565 20 ?
C23 P1 C11 103.9(4) . 20 ?
C16 P1 C11 42.9(7) 2_565 2_565 ?
C16 P1 C11 85.7(8) 20 2_565 ?
O1 P1 C11 105.0(4) . 2_565 ?
O1 P1 C11 95.2(4) 19_565 2_565 ?
C17 P1 C11 122.9(3) 19_565 2_565 ?
C17 P1 C11 151.6(4) . 2_565 ?
C11 P1 C11 8.4(4) 19_565 2_565 ?
C11 P1 C11 47.9(5) . 2_565 ?
C23 P1 C11 103.9(4) 19_565 2_565 ?
C23 P1 C11 65.4(3) . 2_565 ?
C11 P1 C11 43.2(5) 20 2_565 ?
O1 O1 P1 76.7(3) 19_565 . ?
O1 O1 O1 90.000(2) 19_565 20 ?
P1 O1 O1 110.6(3) . 20 ?
O1 O1 O2 78.7(2) 19_565 2_565 ?
P1 O1 O2 110.3(5) . 2_565 ?
O1 O1 O2 133.5(3) 20 2_565 ?
O1 O1 U1 81.30(17) 19_565 . ?
P1 O1 U1 158.0(4) . . ?
O1 O1 U1 68.90(19) 20 . ?
O2 O1 U1 64.8(3) 2_565 . ?
C1 N1 U1 180.000(1) . . ?
C5 O2 C5 69.8(8) . 19_565 ?
C5 O2 O2 108.4(5) . 18 ?
C5 O2 O2 108.4(5) 19_565 18 ?
C5 O2 O1 100.9(6) . 20 ?
C5 O2 O1 114.3(6) 19_565 20 ?
O2 O2 O1 134.3(3) 18 20 ?
C5 O2 O1 114.3(6) . 2_565 ?
C5 O2 O1 100.9(6) 19_565 2_565 ?
O2 O2 O1 134.3(3) 18 2_565 ?
O1 O2 O1 22.5(4) 20 2_565 ?
C5 O2 U1 145.1(4) . . ?
C5 O2 U1 145.1(4) 19_565 . ?
O2 O2 U1 66.93(17) 18 . ?
O1 O2 U1 69.0(3) 20 . ?
O1 O2 U1 69.0(3) 2_565 . ?
C3 C1 C3 29.3(10) 18 3 ?
C3 C1 C3 116.1(11) 18 . ?
C3 C1 C3 124.5(11) 3 . ?
C3 C1 C3 124.5(11) 18 20 ?
C3 C1 C3 116.1(11) 3 20 ?
C3 C1 C3 29.3(10) . 20 ?
C3 C1 N1 117.7(6) 18 . ?
C3 C1 N1 117.7(6) 3 . ?
C3 C1 N1 117.7(6) . . ?
C3 C1 N1 117.7(6) 20 . ?
C3 C1 C2 32.1(6) 18 20 ?
C3 C1 C2 61.4(8) 3 20 ?
C3 C1 C2 99.9(8) . 20 ?
C3 C1 C2 122.7(7) 20 20 ?
N1 C1 C2 109.3(6) . 20 ?
C3 C1 C2 99.9(8) 18 3 ?
C3 C1 C2 122.7(7) 3 3 ?
C3 C1 C2 32.1(6) . 3 ?
C3 C1 C2 61.4(8) 20 3 ?
N1 C1 C2 109.3(6) . 3 ?
C2 C1 C2 73.8(10) 20 3 ?
C3 C1 C2 61.4(8) 18 . ?
C3 C1 C2 32.1(6) 3 . ?
C3 C1 C2 122.7(7) . . ?
C3 C1 C2 99.9(8) 20 . ?
N1 C1 C2 109.3(6) . . ?
C2 C1 C2 93.5(11) 20 . ?
C2 C1 C2 141.5(12) 3 . ?
C3 C1 C2 122.7(7) 18 18 ?
C3 C1 C2 99.9(8) 3 18 ?
C3 C1 C2 61.4(8) . 18 ?
C3 C1 C2 32.1(7) 20 18 ?
N1 C1 C2 109.3(6) . 18 ?
C2 C1 C2 141.5(12) 20 18 ?
C2 C1 C2 93.5(11) 3 18 ?
C2 C1 C2 73.8(10) . 18 ?
C3 C2 C3 10.7(6) 3 18 ?
C3 C2 C1 66.3(9) 3 . ?
C3 C2 C1 55.6(6) 18 . ?
C3 C2 C2 110.1(12) 3 18 ?
C3 C2 C2 100.8(6) 18 18 ?
C1 C2 C2 53.1(5) . 18 ?
C3 C3 C2 157.0(10) 20 3 ?
C3 C3 C1 75.4(5) 20 . ?
C2 C3 C1 81.6(10) 3 . ?
C3 C3 C2 12.3(5) 20 18 ?
C2 C3 C2 144.6(15) 3 18 ?
C1 C3 C2 63.0(6) . 18 ?
O2 C5 C18 133.2(10) . 20 ?
O2 C5 C6 112.1(6) . . ?
C18 C5 C6 40.1(11) 20 . ?
O2 C5 C10 126.9(6) . . ?
C18 C5 C10 95.5(6) 20 . ?
C6 C5 C10 120.0 . . ?
O2 C5 C5 55.1(4) . 19_565 ?
C18 C5 C5 126.1(14) 20 19_565 ?
C6 C5 C5 151.1(3) . 19_565 ?
C10 C5 C5 81.4(3) . 19_565 ?
O2 C5 C10B 139.7(9) . 4_565 ?
C18 C5 C10B 86.1(11) 20 4_565 ?
C6 C5 C10B 92.6(7) . 4_565 ?
C10 C5 C10B 34.4(7) . 4_565 ?
C5 C5 C10B 113.5(7) 19_565 4_565 ?
O2 C5 C10 98.1(7) . 19_565 ?
C18 C5 C10 113.3(8) 20 19_565 ?
C6 C5 C10 149.4(3) . 19_565 ?
C10 C5 C10 33.0(3) . 19_565 ?
C5 C5 C10 48.5(3) 19_565 19_565 ?
C10B C5 C10 66.1(7) 4_565 19_565 ?
O2 C5 C10C 173.3(8) . 19_565 ?
C18 C5 C10C 53.1(9) 20 19_565 ?
C6 C5 C10C 71.4(4) . 19_565 ?
C10 C5 C10C 48.8(4) . 19_565 ?
C5 C5 C10C 124.6(5) 19_565 19_565 ?
C10B C5 C10C 33.6(7) 4_565 19_565 ?
C10 C5 C10C 79.3(5) 19_565 19_565 ?
O2 C5 C10A 130.6(7) . 19_565 ?
C18 C5 C10A 95.7(8) 20 19_565 ?
C6 C5 C10A 111.0(5) . 19_565 ?
C10 C5 C10A 15.5(5) . 19_565 ?
C5 C5 C10A 93.9(5) 19_565 19_565 ?
C10B C5 C10A 19.9(6) 4_565 19_565 ?
C10 C5 C10A 46.2(4) 19_565 19_565 ?
C10C C5 C10A 43.7(5) 19_565 19_565 ?
C18 C6 C5 67(2) 20 . ?
C18 C6 C7 78(2) 20 . ?
C5 C6 C7 120.0 . . ?
C18 C6 C19 46.4(7) 20 20 ?
C5 C6 C19 87.7(13) . 20 ?
C7 C6 C19 35.8(13) . 20 ?
C19 C7 C6 96(2) 20 . ?
C19 C7 C8 35.8(19) 20 . ?
C6 C7 C8 120.0 . . ?
C19 C7 C18 63(2) 20 20 ?
C6 C7 C18 37.5(7) . 20 ?
C8 C7 C18 94.9(6) . 20 ?
C19 C7 C10C 25(2) 20 19_565 ?
C6 C7 C10C 86.7(6) . 19_565 ?
C8 C7 C10C 33.7(6) . 19_565 ?
C18 C7 C10C 63.2(10) 20 19_565 ?
C19 C8 C10C 53(3) 20 19_565 ?
C19 C8 C9 85(3) 20 . ?
C10C C8 C9 34.5(11) 19_565 . ?
C19 C8 C7 51.8(18) 20 . ?
C10C C8 C7 86.9(11) 19_565 . ?
C9 C8 C7 120.0 . . ?
C19 C8 C20 59(2) 20 20 ?
C10C C8 C20 88(2) 19_565 20 ?
C9 C8 C20 93.8(16) . 20 ?
C7 C8 C20 95.3(6) . 20 ?
C19 C8 C10B 75(3) 20 4_565 ?
C10C C8 C10B 28.9(11) 19_565 4_565 ?
C9 C8 C10B 37.2(6) . 4_565 ?
C7 C8 C10B 87.4(6) . 4_565 ?
C20 C8 C10B 116.3(18) 20 4_565 ?
C10C C9 C10A 108.7(14) 19_565 19_565 ?
C10C C9 C10B 70.0(14) 19_565 4_565 ?
C10A C9 C10B 41.7(9) 19_565 4_565 ?
C10C C9 C10 83.6(11) 19_565 . ?
C10A C9 C10 34.1(9) 19_565 . ?
C10B C9 C10 40.2(9) 4_565 . ?
C10C C9 C8 37.9(12) 19_565 . ?
C10A C9 C8 134.9(10) 19_565 . ?
C10B C9 C8 93.7(9) 4_565 . ?
C10 C9 C8 120.0 . . ?
C10C C9 C19 13.7(14) 19_565 20 ?
C10A C9 C19 121.9(14) 19_565 20 ?
C10B C9 C19 83.7(13) 4_565 20 ?
C10 C9 C19 94.4(12) . 20 ?
C8 C9 C19 31.6(15) . 20 ?
C10C C9 C10D 173.7(15) 19_565 19_565 ?
C10A C9 C10D 66.4(9) 19_565 19_565 ?
C10B C9 C10D 104.2(10) 4_565 19_565 ?
C10 C9 C10D 93.5(7) . 19_565 ?
C8 C9 C10D 142.9(8) . 19_565 ?
C19 C9 C10D 171.6(13) 20 19_565 ?
C10A C10 C10B 53.6(12) 19_565 4_565 ?
C10A C10 C10 115.9(12) 19_565 19_565 ?
C10B C10 C10 159.3(9) 4_565 19_565 ?
C10A C10 C9 47.2(12) 19_565 . ?
C10B C10 C9 52.9(11) 4_565 . ?
C10 C10 C9 136.6 19_565 . ?
C10A C10 C5 136.2(14) 19_565 . ?
C10B C10 C5 84.7(11) 4_565 . ?
C10 C10 C5 98.6 19_565 . ?
C9 C10 C5 120.0 . . ?
C10A C10 C10A 88.3(16) 19_565 . ?
C10B C10 C10A 137.2(13) 4_565 . ?
C10 C10 C10A 27.6(8) 19_565 . ?
C9 C10 C10A 117.2(7) . . ?
C5 C10 C10A 122.5(7) . . ?
C10A C10 C10C 73.6(12) 19_565 19_565 ?
C10B C10 C10C 47.1(11) 4_565 19_565 ?
C10 C10 C10C 152.7(6) 19_565 19_565 ?
C9 C10 C10C 32.3(6) . 19_565 ?
C5 C10 C10C 88.2(6) . 19_565 ?
C10A C10 C10C 147.3(10) . 19_565 ?
C10A C10 C10A 35.4(11) 19_565 4_565 ?
C10B C10 C10A 59.8(9) 4_565 4_565 ?
C10 C10 C10A 101.0(6) 19_565 4_565 ?
C9 C10 C10A 80.9(6) . 4_565 ?
C5 C10 C10A 115.4(7) . 4_565 ?
C10A C10 C10A 78.0(9) . 4_565 ?
C10C C10 C10A 99.8(9) 19_565 4_565 ?
C10A C10 C5 152.3(12) 19_565 19_565 ?
C10B C10 C5 131.0(12) 4_565 19_565 ?
C10 C10 C5 48.5(4) 19_565 19_565 ?
C9 C10 C5 160.5(3) . 19_565 ?
C5 C10 C5 50.1(4) . 19_565 ?
C10A C10 C5 73.7(7) . 19_565 ?
C10C C10 C5 131.8(7) 19_565 19_565 ?
C10A C10 C5 118.2(6) 4_565 19_565 ?
C10A C10 C10B 110.0(14) 19_565 18 ?
C10B C10 C10B 149.6(14) 4_565 18 ?
C10 C10 C10B 9.7(7) 19_565 18 ?
C9 C10 C10B 138.9(7) . 18 ?
C5 C10 C10B 99.8(7) . 18 ?
C10A C10 C10B 23.2(6) . 18 ?
C10C C10 C10B 161.5(9) 19_565 18 ?
C10A C10 C10B 91.9(8) 4_565 18 ?
C5 C10 C10B 50.5(6) 19_565 18 ?
C10A C10 C10B 47.4(12) 19_565 19_565 ?
C10B C10 C10B 44.2(10) 4_565 19_565 ?
C10 C10 C10B 115.2(6) 19_565 19_565 ?
C9 C10 C10B 82.8(5) . 19_565 ?
C5 C10 C10B 94.6(6) . 19_565 ?
C10A C10 C10B 97.1(9) . 19_565 ?
C10C C10 C10B 90.4(7) 19_565 19_565 ?
C10A C10 C10B 22.8(5) 4_565 19_565 ?
C5 C10 C10B 113.0(6) 19_565 19_565 ?
C10B C10 C10B 105.4(7) 18 19_565 ?
C10A C10 C18 123.7(15) 19_565 20 ?
C10B C10 C18 76.1(14) 4_565 20 ?
C10 C10 C18 119.5(10) 19_565 20 ?
C9 C10 C18 84.3(8) . 20 ?
C5 C10 C18 41.2(6) . 20 ?
C10A C10 C18 146.4(12) . 20 ?
C10C C10 C18 52.7(10) 19_565 20 ?
C10A C10 C18 133.4(11) 4_565 20 ?
C5 C10 C18 79.2(8) 19_565 20 ?
C10B C10 C18 126.2(11) 18 20 ?
C10B C10 C18 111.7(11) 19_565 20 ?
C11 C11 C16 139.1(7) 20 20 ?
C11 C11 C12 102.2(3) 20 . ?
C16 C11 C12 104.8(5) 20 . ?
C11 C11 C16 29.9(3) 20 . ?
C16 C11 C16 109.3(8) 20 . ?
C12 C11 C16 120.0 . . ?
C11 C11 C11 90.0 20 19_565 ?
C16 C11 C11 112.6(5) 20 19_565 ?
C12 C11 C11 103.2(3) . 19_565 ?
C16 C11 C11 107.0(4) . 19_565 ?
C11 C11 C12 62.8(6) 20 20 ?
C16 C11 C12 136.4(5) 20 20 ?
C12 C11 C12 39.4(5) . 20 ?
C16 C11 C12 83.8(5) . 20 ?
C11 C11 C12 102.0(3) 19_565 20 ?
C11 C11 C11 74.8(7) 20 2_565 ?
C16 C11 C11 124.7(9) 20 2_565 ?
C12 C11 C11 106.0(4) . 2_565 ?
C16 C11 C11 93.1(8) . 2_565 ?
C11 C11 C11 15.2(7) 19_565 2_565 ?
C12 C11 C11 94.6(7) 20 2_565 ?
C11 C11 P1 133.4(3) 20 . ?
C16 C11 P1 48.5(8) 20 . ?
C12 C11 P1 120.6(5) . . ?
C16 C11 P1 119.1(5) . . ?
C11 C11 P1 64.4(3) 19_565 . ?
C12 C11 P1 155.4(7) 20 . ?
C11 C11 P1 76.3(5) 2_565 . ?
C11 C11 C24 104.4(10) 20 19_565 ?
C16 C11 C24 65.8(9) 20 19_565 ?
C12 C11 C24 59.3(11) . 19_565 ?
C16 C11 C24 92.7(11) . 19_565 ?
C11 C11 C24 159.0(12) 19_565 19_565 ?
C12 C11 C24 72.4(9) 20 19_565 ?
C11 C11 C24 165.1(10) 2_565 19_565 ?
P1 C11 C24 112.5(10) . 19_565 ?
C11 C11 C23 146.1(4) 20 19_565 ?
C16 C11 C23 26.7(4) 20 19_565 ?
C12 C11 C23 78.4(5) . 19_565 ?
C16 C11 C23 121.2(6) . 19_565 ?
C11 C11 C23 123.2(4) 19_565 19_565 ?
C12 C11 C23 110.9(6) 20 19_565 ?
C11 C11 C23 138.3(9) 2_565 19_565 ?
P1 C11 C23 66.8(4) . 19_565 ?
C24 C11 C23 46.3(8) 19_565 19_565 ?
C11 C11 C24 63.6(9) 20 2_565 ?
C16 C11 C24 97.6(12) 20 2_565 ?
C12 C11 C24 70.8(10) . 2_565 ?
C16 C11 C24 57.2(9) . 2_565 ?
C11 C11 C24 149.7(11) 19_565 2_565 ?
C12 C11 C24 53.9(11) 20 2_565 ?
C11 C11 C24 135.7(13) 2_565 2_565 ?
P1 C11 C24 144.9(12) . 2_565 ?
C24 C11 C24 40.9(18) 19_565 2_565 ?
C23 C11 C24 85.5(12) 19_565 2_565 ?
C11 C11 P1 38.25(19) 20 2_565 ?
C16 C11 P1 118.1(5) 20 2_565 ?
C12 C11 P1 136.3(4) . 2_565 ?
C16 C11 P1 39.3(4) . 2_565 ?
C11 C11 P1 68.4(2) 19_565 2_565 ?
C12 C11 P1 98.5(7) 20 2_565 ?
C11 C11 P1 55.8(5) 2_565 2_565 ?
P1 C11 P1 95.1(3) . 2_565 ?
C24 C11 P1 131.9(12) 19_565 2_565 ?
C23 C11 P1 143.3(6) 19_565 2_565 ?
C24 C11 P1 95.0(9) 2_565 2_565 ?
C12 C12 C13 85.6(10) 20 20 ?
C12 C12 C11 77.8 20 . ?
C13 C12 C11 145.8(5) 20 . ?
C12 C12 C13 49.0 20 . ?
C13 C12 C13 36.6(10) 20 . ?
C11 C12 C13 120.0 . . ?
C12 C12 C11 62.8(7) 20 20 ?
C13 C12 C11 137.1(10) 20 20 ?
C11 C12 C11 15.0(7) . 20 ?
C13 C12 C11 106.3(6) . 20 ?
C12 C12 C24 95.1(11) 20 19_565 ?
C13 C12 C24 80.5(10) 20 19_565 ?
C11 C12 C24 71.6(11) . 19_565 ?
C13 C12 C24 85.9(10) . 19_565 ?
C11 C12 C24 74.7(11) 20 19_565 ?
C12 C12 C14 134.4(4) 20 20 ?
C13 C12 C14 58.7(6) 20 20 ?
C11 C12 C14 115.26(6) . 20 ?
C13 C12 C14 91.4(4) . 20 ?
C11 C12 C14 125.0(4) 20 20 ?
C24 C12 C14 54.7(11) 19_565 20 ?
C12 C12 C24 54.3(10) 20 2_565 ?
C13 C12 C24 79.3(10) 20 2_565 ?
C11 C12 C24 66.7(9) . 2_565 ?
C13 C12 C24 60.7(10) . 2_565 ?
C11 C12 C24 59.0(9) 20 2_565 ?
C24 C12 C24 41(2) 19_565 2_565 ?
C14 C12 C24 89.4(8) 20 2_565 ?
C12 C12 C16 105.1(6) 20 20 ?
C13 C12 C16 133.3(3) 20 20 ?
C11 C12 C16 31.6(5) . 20 ?
C13 C12 C16 132.4(4) . 20 ?
C11 C12 C16 45.10(19) 20 20 ?
C24 C12 C16 53.7(10) 19_565 20 ?
C14 C12 C16 84.6(5) 20 20 ?
C24 C12 C16 71.8(11) 2_565 20 ?
C12 C12 C15 135.7(3) 20 20 ?
C13 C12 C15 100.5(7) 20 20 ?
C11 C12 C15 73.0(2) . 20 ?
C13 C12 C15 124.44(15) . 20 ?
C11 C12 C15 85.6(4) 20 20 ?
C24 C12 C15 44.3(10) 19_565 20 ?
C14 C12 C15 44.1(3) 20 20 ?
C24 C12 C15 83.5(11) 2_565 20 ?
C16 C12 C15 41.4(3) 20 20 ?
C12 C12 C23 125.9(5) 20 19_565 ?
C13 C12 C23 110.9(6) 20 19_565 ?
C11 C12 C23 59.6(5) . 19_565 ?
C13 C12 C23 128.4(5) . 19_565 ?
C11 C12 C23 72.2(4) 20 19_565 ?
C24 C12 C23 43.0(9) 19_565 19_565 ?
C14 C12 C23 56.8(5) 20 19_565 ?
C24 C12 C23 77.8(13) 2_565 19_565 ?
C16 C12 C23 28.1(3) 20 19_565 ?
C15 C12 C23 13.4(4) 20 19_565 ?
C13 C13 C12 94.4(9) 20 20 ?
C13 C13 C12 49.0 20 . ?
C12 C13 C12 45.4(9) 20 . ?
C13 C13 C14 150.1 20 . ?
C12 C13 C14 80.9(8) 20 . ?
C12 C13 C14 120.0 . . ?
C13 C13 C24 97.3(10) 20 2_565 ?
C12 C13 C24 63.1(6) 20 2_565 ?
C12 C13 C24 75.4(7) . 2_565 ?
C14 C13 C24 54.2(10) . 2_565 ?
C13 C13 C24 58.8(9) 20 19_565 ?
C12 C13 C24 70.0(7) 20 19_565 ?
C12 C13 C24 51.0(6) . 19_565 ?
C14 C13 C24 92.3(9) . 19_565 ?
C24 C13 C24 38.5(18) 2_565 19_565 ?
C15 C14 C13 120.0 . . ?
C15 C14 C24 58.4(11) . 2_565 ?
C13 C14 C24 75.5(9) . 2_565 ?
C15 C14 C20 98.1(12) . 26_455 ?
C13 C14 C20 135.1(12) . 26_455 ?
C24 C14 C20 149.3(16) 2_565 26_455 ?
C15 C14 C12 82.50(18) . 20 ?
C13 C14 C12 40.3(3) . 20 ?
C24 C14 C12 61.8(6) 2_565 20 ?
C20 C14 C12 140.3(17) 26_455 20 ?
C15 C14 C23 10.1(4) . 2_565 ?
C13 C14 C23 110.2(4) . 2_565 ?
C24 C14 C23 49.8(10) 2_565 2_565 ?
C20 C14 C23 108.1(13) 26_455 2_565 ?
C12 C14 C23 73.9(3) 20 2_565 ?
C15 C14 C25 87.8(13) . 2_565 ?
C13 C14 C25 89.0(9) . 2_565 ?
C24 C14 C25 49.0(13) 2_565 2_565 ?
C20 C14 C25 117.1(18) 26_455 2_565 ?
C12 C14 C25 102.6(10) 20 2_565 ?
C23 C14 C25 84.7(15) 2_565 2_565 ?
C15 C14 C21 54.6(12) . 26_455 ?
C13 C14 C21 145.8(13) . 26_455 ?
C24 C14 C21 112.8(16) 2_565 26_455 ?
C20 C14 C21 46.0(5) 26_455 26_455 ?
C12 C14 C21 112.2(12) 20 26_455 ?
C23 C14 C21 63.9(12) 2_565 26_455 ?
C25 C14 C21 122.1(16) 2_565 26_455 ?
C23 C15 C28 98(3) 2_565 2_565 ?
C23 C15 C16 22.1(16) 2_565 . ?
C28 C15 C16 118.9(17) 2_565 . ?
C23 C15 C14 138.6(14) 2_565 . ?
C28 C15 C14 120.4(16) 2_565 . ?
C16 C15 C14 120.0 . . ?
C23 C15 C24 80(2) 2_565 2_565 ?
C28 C15 C24 132(3) 2_565 2_565 ?
C16 C15 C24 71.6(10) . 2_565 ?
C14 C15 C24 63.5(15) . 2_565 ?
C23 C15 C21 136(2) 2_565 26_455 ?
C28 C15 C21 63(2) 2_565 26_455 ?
C16 C15 C21 137.6(15) . 26_455 ?
C14 C15 C21 79.8(12) . 26_455 ?
C24 C15 C21 142.9(19) 2_565 26_455 ?
C23 C15 C17 62.6(15) 2_565 20 ?
C28 C15 C17 61.6(13) 2_565 20 ?
C16 C15 C17 72.1(5) . 20 ?
C14 C15 C17 148.3(6) . 20 ?
C24 C15 C17 142.3(14) 2_565 20 ?
C21 C15 C17 74.0(13) 26_455 20 ?
C23 C15 C12 89.5(16) 2_565 20 ?
C28 C15 C12 172(2) 2_565 20 ?
C16 C15 C12 68.1(2) . 20 ?
C14 C15 C12 53.45(13) . 20 ?
C24 C15 C12 52.4(11) 2_565 20 ?
C21 C15 C12 109.8(12) 26_455 20 ?
C17 C15 C12 120.3(6) 20 20 ?
C23 C15 P1 36.8(17) 2_565 2_565 ?
C28 C15 P1 106.0(14) 2_565 2_565 ?
C16 C15 P1 30.1(4) . 2_565 ?
C14 C15 P1 129.7(4) . 2_565 ?
C24 C15 P1 100.1(9) 2_565 2_565 ?
C21 C15 P1 107.7(15) 26_455 2_565 ?
C17 C15 P1 47.1(3) 20 2_565 ?
C12 C15 P1 78.3(4) 20 2_565 ?
C23 C16 C11 123.9(8) 2_565 20 ?
C23 C16 P1 116.8(11) 2_565 2_565 ?
C11 C16 P1 93.7(6) 20 2_565 ?
C23 C16 C15 10.5(8) 2_565 . ?
C11 C16 C15 113.9(5) 20 . ?
P1 C16 C15 117.3(7) 2_565 . ?
C23 C16 C11 129.1(7) 2_565 . ?
C11 C16 C11 11.0(7) 20 . ?
P1 C16 C11 97.8(7) 2_565 . ?
C15 C16 C11 120.0 . . ?
C23 C16 C24 58.3(8) 2_565 2_565 ?
C11 C16 C24 77.9(7) 20 2_565 ?
P1 C16 C24 161.7(14) 2_565 2_565 ?
C15 C16 C24 54.3(11) . 2_565 ?
C11 C16 C24 77.0(7) . 2_565 ?
C23 C16 C12 80.7(7) 2_565 20 ?
C11 C16 C12 43.5(4) 20 20 ?
P1 C16 C12 111.6(6) 2_565 20 ?
C15 C16 C12 70.5(4) . 20 ?
C11 C16 C12 51.1(4) . 20 ?
C24 C16 C12 51.5(10) 2_565 20 ?
C23 C16 C16 135.0(8) 2_565 20 ?
C11 C16 C16 40.9(7) 20 20 ?
P1 C16 C16 107.2(7) 2_565 20 ?
C15 C16 C16 131.0 . 20 ?
C11 C16 C16 29.9 . 20 ?
C24 C16 C16 77.0(10) 2_565 20 ?
C12 C16 C16 74.9(5) 20 20 ?
C23 C16 C17 61.8(7) 2_565 20 ?
C11 C16 C17 141.2(8) 20 20 ?
P1 C16 C17 58.1(4) 2_565 20 ?
C15 C16 C17 66.7(5) . 20 ?
C11 C16 C17 150.6(6) . 20 ?
C24 C16 C17 120.2(10) 2_565 20 ?
C12 C16 C17 118.3(6) 20 20 ?
C16 C16 C17 162.3(5) 20 20 ?
C15 C23 C16 147(3) 2_565 2_565 ?
C15 C23 C24 81(3) 2_565 . ?
C16 C23 C24 85.3(13) 2_565 . ?
C15 C23 C28 63(2) 2_565 . ?
C16 C23 C28 147.8(13) 2_565 . ?
C24 C23 C28 120.0 . . ?
C15 C23 C14 31(2) 2_565 2_565 ?
C16 C23 C14 120.0(16) 2_565 2_565 ?
C24 C23 C14 53.6(10) . 2_565 ?
C28 C23 C14 91.9(6) . 2_565 ?
C15 C23 C17 104(3) 2_565 19_565 ?
C16 C23 C17 89.3(13) 2_565 19_565 ?
C24 C23 C17 174.5(4) . 19_565 ?
C28 C23 C17 65.3(4) . 19_565 ?
C14 C23 C17 129.6(10) 2_565 19_565 ?
C15 C23 C11 119(3) 2_565 19_565 ?
C16 C23 C11 29.4(10) 2_565 19_565 ?
C24 C23 C11 65.1(5) . 19_565 ?
C28 C23 C11 174.7(5) . 19_565 ?
C14 C23 C11 90.7(7) 2_565 19_565 ?
C17 C23 C11 109.6(4) 19_565 19_565 ?
C15 C23 P1 135(3) 2_565 . ?
C16 C23 P1 36.6(12) 2_565 . ?
C24 C23 P1 119.4(4) . . ?
C28 C23 P1 120.1(4) . . ?
C14 C23 P1 129.6(6) 2_565 . ?
C17 C23 P1 55.1(3) 19_565 . ?
C11 C23 P1 54.9(3) 19_565 . ?
C15 C23 C21 34(3) 2_565 25_565 ?
C16 C23 C21 140.8(14) 2_565 25_565 ?
C24 C23 C21 114.3(5) . 25_565 ?
C28 C23 C21 50.0(7) . 25_565 ?
C14 C23 C21 61.6(10) 2_565 25_565 ?
C17 C23 C21 69.9(5) 19_565 25_565 ?
C11 C23 C21 128.0(9) 19_565 25_565 ?
P1 C23 C21 108.6(5) . 25_565 ?
C15 C23 C12 77(3) 2_565 19_565 ?
C16 C23 C12 71.2(9) 2_565 19_565 ?
C24 C23 C12 50.9(5) . 19_565 ?
C28 C23 C12 139.5(8) . 19_565 ?
C14 C23 C12 49.3(8) 2_565 19_565 ?
C17 C23 C12 126.5(6) 19_565 19_565 ?
C11 C23 C12 42.0(5) 19_565 19_565 ?
P1 C23 C12 86.1(5) . 19_565 ?
C21 C23 C12 94.4(10) 25_565 19_565 ?
C24 C24 C23 139.2 20 . ?
C24 C24 C25 96.7 20 . ?
C23 C24 C25 120.0 . . ?
C24 C24 C15 156.4(5) 20 2_565 ?
C23 C24 C15 19.5(8) . 2_565 ?
C25 C24 C15 106.7(4) . 2_565 ?
C24 C24 C14 132.2(9) 20 2_565 ?
C23 C24 C14 76.6(11) . 2_565 ?
C25 C24 C14 78.3(8) . 2_565 ?
C15 C24 C14 58.1(11) 2_565 2_565 ?
C24 C24 C12 84.9(9) 20 19_565 ?
C23 C24 C12 86.1(7) . 19_565 ?
C25 C24 C12 127.3(8) . 19_565 ?
C15 C24 C12 83.3(9) 2_565 19_565 ?
C14 C24 C12 63.5(10) 2_565 19_565 ?
C24 C24 C16 103.0(7) 20 2_565 ?
C23 C24 C16 36.4(7) . 2_565 ?
C25 C24 C16 151.9(7) . 2_565 ?
C15 C24 C16 54.1(8) 2_565 2_565 ?
C14 C24 C16 102.1(14) 2_565 2_565 ?
C12 C24 C16 74.9(5) 19_565 2_565 ?
C24 C24 C13 82.7(9) 20 2_565 ?
C23 C24 C13 111.5(9) . 2_565 ?
C25 C24 C13 91.3(7) . 2_565 ?
C15 C24 C13 99.4(15) 2_565 2_565 ?
C14 C24 C13 50.3(8) 2_565 2_565 ?
C12 C24 C13 36.4(3) 19_565 2_565 ?
C16 C24 C13 110.8(8) 2_565 2_565 ?
C24 C24 C11 75.6(6) 20 19_565 ?
C23 C24 C11 68.6(5) . 19_565 ?
C25 C24 C11 171.4(5) . 19_565 ?
C15 C24 C11 81.2(6) 2_565 19_565 ?
C14 C24 C11 103.9(8) 2_565 19_565 ?
C12 C24 C11 49.1(5) 19_565 19_565 ?
C16 C24 C11 36.4(7) 2_565 19_565 ?
C13 C24 C11 84.0(6) 2_565 19_565 ?
C24 C24 C11 63.6(5) 20 2_565 ?
C23 C24 C11 79.9(5) . 2_565 ?
C25 C24 C11 159.9(5) . 2_565 ?
C15 C24 C11 93.2(7) 2_565 2_565 ?
C14 C24 C11 111.4(8) 2_565 2_565 ?
C12 C24 C11 51.4(7) 19_565 2_565 ?
C16 C24 C11 45.9(4) 2_565 2_565 ?
C13 C24 C11 82.8(6) 2_565 2_565 ?
C11 C24 C11 12.0(6) 19_565 2_565 ?
C24 C24 C12 54.3(7) 20 2_565 ?
C23 C24 C12 109.4(6) . 2_565 ?
C25 C24 C12 123.6(7) . 2_565 ?
C15 C24 C12 111.9(10) 2_565 2_565 ?
C14 C24 C12 88.8(8) 2_565 2_565 ?
C12 C24 C12 30.6(11) 19_565 2_565 ?
C16 C24 C12 84.4(6) 2_565 2_565 ?
C13 C24 C12 43.9(4) 2_565 2_565 ?
C11 C24 C12 48.6(5) 19_565 2_565 ?
C11 C24 C12 42.6(4) 2_565 2_565 ?
C24 C24 C25 43.9(3) 20 20 ?
C23 C24 C25 162.93(10) . 20 ?
C25 C24 C25 52.8(3) . 20 ?
C15 C24 C25 159.4(5) 2_565 20 ?
C14 C24 C25 113.4(11) 2_565 20 ?
C12 C24 C25 110.6(7) 19_565 20 ?
C16 C24 C25 142.7(8) 2_565 20 ?
C13 C24 C25 85.1(9) 2_565 20 ?
C11 C24 C25 119.3(6) 19_565 20 ?
C11 C24 C25 107.3(6) 2_565 20 ?
C12 C24 C25 85.3(7) 2_565 20 ?
C26 C25 C24 120.0 . . ?
C26 C25 C25 150.8 . 20 ?
C24 C25 C25 83.3 . 20 ?
C26 C25 C26 22.5(6) . 8_565 ?
C24 C25 C26 109.3(5) . 8_565 ?
C25 C25 C26 138.6(4) 20 8_565 ?
C26 C25 C25 62.88(17) . 8_565 ?
C24 C25 C25 124.4(9) . 8_565 ?
C25 C25 C25 90.0 20 8_565 ?
C26 C25 C25 49.9(5) 8_565 8_565 ?
C26 C25 C14 91.9(6) . 2_565 ?
C24 C25 C14 52.7(7) . 2_565 ?
C25 C25 C14 117.1(6) 20 2_565 ?
C26 C25 C14 100.7(7) 8_565 2_565 ?
C25 C25 C14 150.0(8) 8_565 2_565 ?
C26 C25 C24 155.2(2) . 20 ?
C24 C25 C24 39.4(3) . 20 ?
C25 C25 C24 43.9(3) 20 20 ?
C26 C25 C24 135.3(6) 8_565 20 ?
C25 C25 C24 113.2(6) 8_565 20 ?
C14 C25 C24 82.4(6) 2_565 20 ?
C26 C26 C27 87.9(13) 8_565 8_565 ?
C26 C26 C25 99.5(5) 8_565 . ?
C27 C26 C25 170.6(9) 8_565 . ?
C26 C26 C27 65.2(6) 8_565 . ?
C27 C26 C27 68.4(6) 8_565 . ?
C25 C26 C27 120.0 . . ?
C26 C26 C25 58.0(9) 8_565 8_565 ?
C27 C26 C25 112.9(12) 8_565 8_565 ?
C25 C26 C25 67.2(5) . 8_565 ?
C27 C26 C25 122.9(9) . 8_565 ?
C26 C27 C26 26.9(8) 8_565 . ?
C26 C27 C28 115.1(5) 8_565 . ?
C26 C27 C28 120.0 . . ?
C26 C27 C27 59.9(5) 8_565 8_565 ?
C26 C27 C27 51.8(3) . 8_565 ?
C28 C27 C27 170.9(7) . 8_565 ?
C15 C28 C27 108.8(9) 2_565 . ?
C15 C28 C23 19.6(10) 2_565 . ?
C27 C28 C23 120.0 . . ?
C15 C28 C21 69.8(14) 2_565 25_565 ?
C27 C28 C21 99.3(5) . 25_565 ?
C23 C28 C21 84.9(9) . 25_565 ?
C15 C28 C17 79.2(10) 2_565 19_565 ?
C27 C28 C17 171.9(5) . 19_565 ?
C23 C28 C17 68.0(5) . 19_565 ?
C21 C28 C17 82.4(6) 25_565 19_565 ?
C15 C28 C22 86.7(13) 2_565 19_565 ?
C27 C28 C22 131.5(7) . 19_565 ?
C23 C28 C22 89.9(6) . 19_565 ?
C21 C28 C22 42.3(7) 25_565 19_565 ?
C17 C28 C22 46.2(4) 19_565 19_565 ?
C18 C17 C22 120.0 . . ?
C18 C17 C17 120.9(3) . 19_565 ?
C22 C17 C17 92.8(3) . 19_565 ?
C18 C17 P1 115.9(5) . . ?
C22 C17 P1 123.7(5) . . ?
C17 C17 P1 62.9(3) 19_565 . ?
C18 C17 C28 81.9(10) . 19_565 ?
C22 C17 C28 69.5(10) . 19_565 ?
C17 C17 C28 156.7(10) 19_565 19_565 ?
P1 C17 C28 113.7(9) . 19_565 ?
C18 C17 C23 106.0(5) . 19_565 ?
C22 C17 C23 91.3(5) . 19_565 ?
C17 C17 C23 122.1(3) 19_565 19_565 ?
P1 C17 C23 67.3(3) . 19_565 ?
C28 C17 C23 46.7(8) 19_565 19_565 ?
C18 C17 C15 110.8(7) . 20 ?
C22 C17 C15 77.8(5) . 20 ?
C17 C17 C15 124.2(6) 19_565 20 ?
P1 C17 C15 77.3(5) . 20 ?
C28 C17 C15 39.2(10) 19_565 20 ?
C23 C17 C15 13.7(4) 19_565 20 ?
C18 C17 C16 107.7(5) . 20 ?
C22 C17 C16 113.1(5) . 20 ?
C17 C17 C16 100.5(4) 19_565 20 ?
P1 C17 C16 39.6(4) . 20 ?
C28 C17 C16 74.3(10) 19_565 20 ?
C23 C17 C16 28.9(4) 19_565 20 ?
C15 C17 C16 41.2(2) 20 20 ?
C6 C18 C5 73.1(17) 20 20 ?
C6 C18 C19 104.5(17) 20 . ?
C5 C18 C19 113.2(6) 20 . ?
C6 C18 C17 127.1(17) 20 . ?
C5 C18 C17 109.7(7) 20 . ?
C19 C18 C17 120.0 . . ?
C6 C18 C7 64.9(19) 20 20 ?
C5 C18 C7 116.1(17) 20 20 ?
C19 C18 C7 44.2(5) . 20 ?
C17 C18 C7 133.8(16) . 20 ?
C6 C18 C10C 103.9(17) 20 2_565 ?
C5 C18 C10C 86.1(7) 20 2_565 ?
C19 C18 C10C 28.0(6) . 2_565 ?
C17 C18 C10C 128.9(6) . 2_565 ?
C7 C18 C10C 61.8(8) 20 2_565 ?
C6 C18 C10B 86.3(18) 20 17_565 ?
C5 C18 C10B 52.2(6) 20 17_565 ?
C19 C18 C10B 61.1(6) . 17_565 ?
C17 C18 C10B 138.8(7) . 17_565 ?
C7 C18 C10B 78.6(13) 20 17_565 ?
C10C C18 C10B 34.5(7) 2_565 17_565 ?
C6 C18 C10 103(3) 20 20 ?
C5 C18 C10 43.3(8) 20 20 ?
C19 C18 C10 76.0(8) . 20 ?
C17 C18 C10 113.7(14) . 20 ?
C7 C18 C10 103.5(19) 20 20 ?
C10C C18 C10 48.3(9) 2_565 20 ?
C10B C18 C10 25.8(14) 17_565 20 ?
C10C C19 C8 69(3) 2_565 20 ?
C10C C19 C7 119(2) 2_565 20 ?
C8 C19 C7 92(4) 20 20 ?
C10C C19 C18 93.9(15) 2_565 . ?
C8 C19 C18 149(3) 20 . ?
C7 C19 C18 73.2(18) 20 . ?
C10C C19 C20 111.2(14) 2_565 . ?
C8 C19 C20 90(3) 20 . ?
C7 C19 C20 127(2) 20 . ?
C18 C19 C20 120.0 . . ?
C10C C19 C9 14.8(16) 2_565 20 ?
C8 C19 C9 64(2) 20 20 ?
C7 C19 C9 131(4) 20 20 ?
C18 C19 C9 105.2(12) . 20 ?
C20 C19 C9 96.9(14) . 20 ?
C10C C19 C10B 23.0(13) 2_565 17_565 ?
C8 C19 C10B 79(3) 20 17_565 ?
C7 C19 C10B 99(2) 20 17_565 ?
C18 C19 C10B 76.5(6) . 17_565 ?
C20 C19 C10B 133.2(7) . 17_565 ?
C9 C19 C10B 37.8(12) 20 17_565 ?
C10C C19 C6 94.7(16) 2_565 20 ?
C8 C19 C6 124(4) 20 20 ?
C7 C19 C6 48.0(9) 20 20 ?
C18 C19 C6 29.1(11) . 20 ?
C20 C19 C6 143.4(12) . 20 ?
C9 C19 C6 109.2(19) 20 20 ?
C10B C19 C6 72.1(11) 17_565 20 ?
C21 C20 C19 120.0 . . ?
C21 C20 C14 82.1(15) . 26 ?
C19 C20 C14 146.9(17) . 26 ?
C21 C20 C8 150.1(11) . 20 ?
C19 C20 C8 30.2(10) . 20 ?
C14 C20 C8 123.0(16) 26 20 ?
C21 C20 C10C 124.4(6) . 2_565 ?
C19 C20 C10C 23.3(6) . 2_565 ?
C14 C20 C10C 124.4(18) 26 2_565 ?
C8 C20 C10C 29.6(15) 20 2_565 ?
C22 C21 C20 165.4(6) 11 . ?
C22 C21 C22 46.1(7) 11 . ?
C20 C21 C22 120.0 . . ?
C22 C21 C28 82.1(12) 11 25_565 ?
C20 C21 C28 111.8(11) . 25_565 ?
C22 C21 C28 118.2(12) . 25_565 ?
C22 C21 C15 97.8(14) 11 26 ?
C20 C21 C15 95.2(13) . 26 ?
C22 C21 C15 143.3(14) . 26 ?
C28 C21 C15 47.4(19) 25_565 26 ?
C22 C21 C21 49.3(6) 11 11 ?
C20 C21 C21 126.1(4) . 11 ?
C22 C21 C21 42.0(3) . 11 ?
C28 C21 C21 81.0(12) 25_565 11 ?
C15 C21 C21 124.7(14) 26 11 ?
C22 C21 C14 138.0(13) 11 26 ?
C20 C21 C14 52.0(10) . 26 ?
C22 C21 C14 156.8(14) . 26 ?
C28 C21 C14 83.1(17) 25_565 26 ?
C15 C21 C14 45.6(4) 26 26 ?
C21 C21 C14 161.0(15) 11 26 ?
C22 C21 C23 88.3(6) 11 25_565 ?
C20 C21 C23 104.7(5) . 25_565 ?
C22 C21 C23 133.8(5) . 25_565 ?
C28 C21 C23 45.1(13) 25_565 25_565 ?
C15 C21 C23 9.6(13) 26 25_565 ?
C21 C21 C23 117.7(5) 11 25_565 ?
C14 C21 C23 54.5(10) 26 25_565 ?
C22 C22 C21 75.4(7) 11 11 ?
C22 C22 C21 58.6(9) 11 . ?
C21 C22 C21 88.7(8) 11 . ?
C22 C22 C17 175.0(10) 11 . ?
C21 C22 C17 109.6(10) 11 . ?
C21 C22 C17 120.0 . . ?
C22 C22 C22 90.0 11 19_565 ?
C21 C22 C22 129.6(4) 11 19_565 ?
C21 C22 C22 124.2 . 19_565 ?
C17 C22 C22 87.2 . 19_565 ?
C22 C22 C28 119.5(9) 11 19_565 ?
C21 C22 C28 55.6(10) 11 19_565 ?
C21 C22 C28 85.1(8) . 19_565 ?
C17 C22 C28 64.3(9) . 19_565 ?
C22 C22 C28 147.7(9) 19_565 19_565 ?
C22 C22 C22 58.7(9) 11 25_565 ?
C21 C22 C22 114.4(11) 11 25_565 ?
C21 C22 C22 102.1(8) . 25_565 ?
C17 C22 C22 118.4(9) . 25_565 ?
C22 C22 C22 31.3(9) 19_565 25_565 ?
C28 C22 C22 168.0(12) 19_565 25_565 ?
C10B C10A C10 70.6(18) 18 19_565 ?
C10B C10A C9 74.6(17) 18 19_565 ?
C10 C10A C9 98.7(19) 19_565 19_565 ?
C10B C10A C10A 98.5(17) 18 18 ?
C10 C10A C10A 123.1(13) 19_565 18 ?
C9 C10A C10A 133.2(13) 19_565 18 ?
C10B C10A C10C 46.7(16) 18 . ?
C10 C10A C10C 76.5(13) 19_565 . ?
C9 C10A C10C 31.1(11) 19_565 . ?
C10A C10A C10C 135.5(8) 18 . ?
C10B C10A C10 104.9(19) 18 . ?
C10 C10A C10 36.5(9) 19_565 . ?
C9 C10A C10 120.3(17) 19_565 . ?
C10A C10A C10 106.3(6) 18 . ?
C10C C10A C10 109.0(11) . . ?
C10B C10A C10B 69.3(19) 18 . ?
C10 C10A C10B 110.7(17) 19_565 . ?
C9 C10A C10B 121.1(15) 19_565 . ?
C10A C10A C10B 29.1(6) 18 . ?
C10C C10A C10B 109.7(10) . . ?
C10 C10A C10B 113.1(11) . . ?
C10B C10A C10D 141(2) 18 . ?
C10 C10A C10D 140.3(18) 19_565 . ?
C9 C10A C10D 76.4(12) 19_565 . ?
C10A C10A C10D 82.7(8) 18 . ?
C10C C10A C10D 107.3(11) . . ?
C10 C10A C10D 112.5(11) . . ?
C10B C10A C10D 105.1(11) . . ?
C10B C10A C10A 130.4(16) 18 19_565 ?
C10 C10A C10A 64.1(12) 19_565 19_565 ?
C9 C10A C10A 130.2(11) 19_565 19_565 ?
C10A C10A C10A 90.000(2) 18 19_565 ?
C10C C10A C10A 132.3(8) . 19_565 ?
C10 C10A C10A 27.6(6) . 19_565 ?
C10B C10A C10A 108.6(7) . 19_565 ?
C10D C10A C10A 88.8(8) . 19_565 ?
C10B C10A C10 91.6(19) 18 4_565 ?
C10 C10A C10 101.6(16) 19_565 4_565 ?
C9 C10A C10 150.0(18) 19_565 4_565 ?
C10A C10A C10 21.5(7) 18 4_565 ?
C10C C10A C10 137.0(12) . 4_565 ?
C10 C10A C10 88.7(8) . 4_565 ?
C10B C10A C10 29.9(8) . 4_565 ?
C10D C10A C10 100.8(11) . 4_565 ?
C10A C10A C10 79.0(6) 19_565 4_565 ?
C10B C10A C10D 136(2) 18 18 ?
C10 C10A C10D 152.9(16) 19_565 18 ?
C9 C10A C10D 96.5(13) 19_565 18 ?
C10A C10A C10D 56.0(6) 18 18 ?
C10C C10A C10D 124.9(11) . 18 ?
C10 C10A C10D 116.5(10) . 18 ?
C10B C10A C10D 79.7(9) . 18 ?
C10D C10A C10D 26.7(10) . 18 ?
C10A C10A C10D 89.0(7) 19_565 18 ?
C10 C10A C10D 74.6(9) 4_565 18 ?
C10B C10A C5 44.8(15) 18 19_565 ?
C10 C10A C5 28.2(9) 19_565 19_565 ?
C9 C10A C5 98.2(13) 19_565 19_565 ?
C10A C10A C5 108.9(4) 18 19_565 ?
C10C C10A C5 68.4(8) . 19_565 ?
C10 C10A C5 60.1(6) . 19_565 ?
C10B C10A C5 87.5(8) . 19_565 ?
C10D C10A C5 167.3(11) . 19_565 ?
C10A C10A C5 86.1(5) 19_565 19_565 ?
C10 C10A C5 89.6(8) 4_565 19_565 ?
C10D C10A C5 164.2(9) 18 19_565 ?
C10A C10B C10 55.8(18) 18 4_565 ?
C10A C10B C9 63.7(16) 18 4_565 ?
C10 C10B C9 87(2) 4_565 4_565 ?
C10A C10B C10C 104(2) 18 18 ?
C10 C10B C10C 97.4(16) 4_565 18 ?
C9 C10B C10C 43.1(10) 4_565 18 ?
C10A C10B C10B 81.5(17) 18 18 ?
C10 C10B C10B 110.7(10) 4_565 18 ?
C9 C10B C10B 122.3(11) 4_565 18 ?
C10C C10B C10B 148.5(11) 18 18 ?
C10A C10B C10A 52.4(17) 18 . ?
C10 C10B C10A 90.3(13) 4_565 . ?
C9 C10B C10A 102.1(13) 4_565 . ?
C10C C10B C10A 143.3(16) 18 . ?
C10B C10B C10A 29.1(7) 18 . ?
C10A C10B C5 115.3(19) 18 4_565 ?
C10 C10B C5 60.9(12) 4_565 4_565 ?
C9 C10B C5 125.7(16) 4_565 4_565 ?
C10C C10B C5 95.7(12) 18 4_565 ?
C10B C10B C5 110.1(6) 18 4_565 ?
C10A C10B C5 119.1(11) . 4_565 ?
C10A C10B C19 118(2) 18 17_565 ?
C10 C10B C19 100.6(19) 4_565 17_565 ?
C9 C10B C19 58.5(14) 4_565 17_565 ?
C10C C10B C19 15.4(14) 18 17_565 ?
C10B C10B C19 148.8(16) 18 17_565 ?
C10A C10B C19 156.6(16) . 17_565 ?
C5 C10B C19 84.2(13) 4_565 17_565 ?
C10A C10B C8 112(2) 18 4_565 ?
C10 C10B C8 119.6(19) 4_565 4_565 ?
C9 C10B C8 49.1(8) 4_565 4_565 ?
C10C C10B C8 22.4(13) 18 4_565 ?
C10B C10B C8 126.8(10) 18 4_565 ?
C10A C10B C8 131.9(14) . 4_565 ?
C5 C10B C8 108.6(13) 4_565 4_565 ?
C19 C10B C8 25.8(16) 17_565 4_565 ?
C10A C10B C10 51.9(16) 18 18 ?
C10 C10B C10 10.9(6) 4_565 18 ?
C9 C10B C10 93.2(17) 4_565 18 ?
C10C C10B C10 108.0(13) 18 18 ?
C10B C10B C10 99.7(5) 18 18 ?
C10A C10B C10 80.3(8) . 18 ?
C5 C10B C10 63.4(7) 4_565 18 ?
C19 C10B C10 111.5(17) 17_565 18 ?
C8 C10B C10 130.0(15) 4_565 18 ?
C10A C10B C10 65.7(16) 18 19_565 ?
C10 C10B C10 85.5(12) 4_565 19_565 ?
C9 C10B C10 123.0(14) 4_565 19_565 ?
C10C C10B C10 165.2(15) 18 19_565 ?
C10B C10B C10 25.2(5) 18 19_565 ?
C10A C10B C10 21.9(6) . 19_565 ?
C5 C10B C10 98.4(8) 4_565 19_565 ?
C19 C10B C10 173.9(18) 17_565 19_565 ?
C8 C10B C10 149.6(12) 4_565 19_565 ?
C10 C10B C10 74.6(7) 18 19_565 ?
C10A C10B C18 127(2) 18 17_565 ?
C10 C10B C18 78.1(17) 4_565 17_565 ?
C9 C10B C18 92.7(12) 4_565 17_565 ?
C10C C10B C18 54.7(11) 18 17_565 ?
C10B C10B C18 143.7(7) 18 17_565 ?
C10A C10B C18 160.8(13) . 17_565 ?
C5 C10B C18 41.7(7) 4_565 17_565 ?
C19 C10B C18 42.5(11) 17_565 17_565 ?
C8 C10B C18 67.3(12) 4_565 17_565 ?
C10 C10B C18 86.7(15) 18 17_565 ?
C10 C10B C18 139.8(10) 19_565 17_565 ?
C19 C10C C9 151(3) 2_565 19_565 ?
C19 C10C C8 58(3) 2_565 19_565 ?
C9 C10C C8 108(3) 19_565 19_565 ?
C19 C10C C10B 142(2) 2_565 18 ?
C9 C10C C10B 66.9(16) 19_565 18 ?
C8 C10C C10B 129(2) 19_565 18 ?
C19 C10C C10A 166(2) 2_565 . ?
C9 C10C C10A 40.2(14) 19_565 . ?
C8 C10C C10A 135(2) 19_565 . ?
C10B C10C C10A 29.4(9) 18 . ?
C19 C10C C10 136(2) 2_565 19_565 ?
C9 C10C C10 64.1(11) 19_565 19_565 ?
C8 C10C C10 163(2) 19_565 19_565 ?
C10B C10C C10 35.5(10) 18 19_565 ?
C10A C10C C10 29.9(7) . 19_565 ?
C19 C10C C7 36(3) 2_565 19_565 ?
C9 C10C C7 161(2) 19_565 19_565 ?
C8 C10C C7 59.4(12) 19_565 19_565 ?
C10B C10C C7 108.7(16) 18 19_565 ?
C10A C10C C7 138.2(13) . 19_565 ?
C10 C10C C7 124.0(14) 19_565 19_565 ?
C19 C10C C18 58.1(16) 2_565 2_565 ?
C9 C10C C18 141(2) 19_565 2_565 ?
C8 C10C C18 111(2) 19_565 2_565 ?
C10B C10C C18 90.7(17) 18 2_565 ?
C10A C10C C18 107.5(16) . 2_565 ?
C10 C10C C18 79.0(16) 19_565 2_565 ?
C7 C10C C18 55.0(15) 19_565 2_565 ?
C19 C10C C20 45.6(18) 2_565 2_565 ?
C9 C10C C20 107(2) 19_565 2_565 ?
C8 C10C C20 63(2) 19_565 2_565 ?
C10B C10C C20 168(2) 18 2_565 ?
C10A C10C C20 140.4(19) . 2_565 ?
C10 C10C C20 132.5(18) 19_565 2_565 ?
C7 C10C C20 80.8(18) 19_565 2_565 ?
C18 C10C C20 88.4(18) 2_565 2_565 ?
C19 C10C C5 98.0(15) 2_565 19_565 ?
C9 C10C C5 106.6(15) 19_565 19_565 ?
C8 C10C C5 139(2) 19_565 19_565 ?
C10B C10C C5 50.7(10) 18 19_565 ?
C10A C10C C5 68.0(8) . 19_565 ?
C10 C10C C5 43.0(5) 19_565 19_565 ?
C7 C10C C5 81.6(10) 19_565 19_565 ?
C18 C10C C5 40.8(13) 2_565 19_565 ?
C20 C10C C5 125.6(11) 2_565 19_565 ?
C10D C10D C10A 97.3(8) 18 . ?
C10D C10D C10D 90.001(2) 18 19_565 ?
C10A C10D C10D 91.2(8) . 19_565 ?
C10D C10D C9 123.1(8) 18 19_565 ?
C10A C10D C9 37.2(8) . 19_565 ?
C10D C10D C9 114.9(8) 19_565 19_565 ?
C10D C10D C10D 62.6(10) 18 4_565 ?
C10A C10D C10D 94.5(8) . 4_565 ?
C10D C10D C10D 27.4(10) 19_565 4_565 ?
C9 C10D C10D 128.8(9) 19_565 4_565 ?
C10D C10D C10A 56.0(6) 18 18 ?
C10A C10D C10A 41.4(9) . 18 ?
C10D C10D C10A 91.0(7) 19_565 18 ?
C9 C10D C10A 72.5(8) 19_565 18 ?
C10D C10D C10A 76.0(8) 4_565 18 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 N1 1.863(6) 17_565 ?
U1 N1 1.863(6) . ?
U1 O2 2.268(7) 18 ?
U1 O2 2.268(7) . ?
U1 O2 2.268(7) 17_565 ?
U1 O2 2.268(7) 2_565 ?
U1 O1 2.339(8) 20 ?
U1 O1 2.339(8) 2_565 ?
U1 O1 2.339(8) 19_565 ?
U1 O1 2.339(8) . ?
U1 O1 2.339(8) 3 ?
U1 O1 2.339(8) 17_565 ?
P1 C16 1.292(15) 2_565 ?
P1 C16 1.292(13) 20 ?
P1 O1 1.541(8) . ?
P1 O1 1.541(8) 19_565 ?
P1 C17 1.720(6) 19_565 ?
P1 C17 1.720(6) . ?
P1 C11 1.722(7) 19_565 ?
P1 C11 1.722(7) . ?
P1 C23 1.934(6) 19_565 ?
P1 C23 1.934(6) . ?
P1 C11 2.022(10) 20 ?
P1 C11 2.022(10) 2_565 ?
O1 O1 0.707(14) 19_565 ?
O1 O1 1.684(16) 20 ?
O1 O2 1.809(10) 2_565 ?
N1 C1 1.426(10) . ?
O2 C5 1.245(8) . ?
O2 C5 1.245(8) 19_565 ?
O2 O2 1.777(13) 18 ?
O2 O1 1.809(10) 20 ?
O2 O1 1.809(10) 2_565 ?
C1 C3 1.416(8) 18 ?
C1 C3 1.416(8) 3 ?
C1 C3 1.416(8) . ?
C1 C3 1.416(8) 20 ?
C1 C2 1.530(8) 20 ?
C1 C2 1.530(8) 3 ?
C1 C2 1.530(8) . ?
C1 C2 1.530(8) 18 ?
C2 C3 0.822(17) 3 ?
C2 C3 1.507(19) 18 ?
C2 C2 1.84(2) 18 ?
C3 C3 0.72(2) 20 ?
C3 C2 0.822(17) 3 ?
C3 C2 1.507(19) 18 ?
C5 C18 1.34(4) 20 ?
C5 C6 1.3900 . ?
C5 C10 1.3900 . ?
C5 C5 1.425(14) 19_565 ?
C5 C10B 1.584(16) 4_565 ?
C5 C10 1.836(10) 19_565 ?
C5 C10C 2.038(16) 19_565 ?
C5 C10A 2.033(15) 19_565 ?
C6 C18 0.93(2) 20 ?
C6 C7 1.3900 . ?
C6 C19 1.859(16) 20 ?
C7 C19 1.09(2) 20 ?
C7 C8 1.3900 . ?
C7 C18 1.50(4) 20 ?
C7 C10C 1.613(16) 19_565 ?
C8 C19 0.81(3) 20 ?
C8 C10C 0.897(16) 19_565 ?
C8 C9 1.3900 . ?
C8 C20 1.62(4) 20 ?
C8 C10B 1.834(16) 4_565 ?
C9 C10C 0.825(16) 19_565 ?
C9 C10A 1.032(16) 19_565 ?
C9 C10B 1.111(17) 4_565 ?
C9 C10 1.3900 . ?
C9 C19 1.55(4) 20 ?
C9 C10D 1.659(15) 19_565 ?
C10 C10A 0.787(16) 19_565 ?
C10 C10B 0.898(17) 4_565 ?
C10 C10 1.010(15) 19_565 ?
C10 C10A 1.528(14) . ?
C10 C10C 1.535(15) 19_565 ?
C10 C10A 1.802(16) 4_565 ?
C10 C5 1.836(9) 19_565 ?
C10 C10B 1.878(19) 18 ?
C10 C10B 1.977(16) 19_565 ?
C10 C18 2.02(3) 20 ?
C11 C11 0.40(2) 20 ?
C11 C16 1.058(16) 20 ?
C11 C12 1.3900 . ?
C11 C16 1.3900 . ?
C11 C11 1.489(17) 19_565 ?
C11 C12 1.528(7) 20 ?
C11 C11 1.544(18) 2_565 ?
C11 C24 1.745(14) 19_565 ?
C11 C23 1.790(12) 19_565 ?
C11 C24 1.887(13) 2_565 ?
C11 P1 2.022(10) 2_565 ?
C12 C12 0.993(16) 20 ?
C12 C13 1.0525(14) 20 ?
C12 C13 1.3900 . ?
C12 C11 1.528(8) 20 ?
C12 C24 1.58(2) 19_565 ?
C12 C14 1.606(12) 20 ?
C12 C24 1.940(17) 2_565 ?
C12 C16 1.951(6) 20 ?
C12 C15 1.982(12) 20 ?
C12 C23 2.033(12) 19_565 ?
C13 C13 0.830(18) 20 ?
C13 C12 1.0525(13) 20 ?
C13 C14 1.3900 . ?
C13 C24 1.75(3) 2_565 ?
C13 C24 2.03(3) 19_565 ?
C14 C15 1.3900 . ?
C14 C24 1.47(4) 2_565 ?
C14 C20 1.52(3) 26_455 ?
C14 C12 1.606(11) 20 ?
C14 C23 1.771(12) 2_565 ?
C14 C25 1.80(4) 2_565 ?
C14 C21 1.914(17) 26_455 ?
C15 C23 0.471(12) 2_565 ?
C15 C28 1.24(2) 2_565 ?
C15 C16 1.3900 . ?
C15 C24 1.39(3) 2_565 ?
C15 C21 1.59(3) 26_455 ?
C15 C17 1.937(12) 20 ?
C15 C12 1.982(12) 20 ?
C15 P1 2.291(11) 2_565 ?
C16 C23 0.970(12) 2_565 ?
C16 C11 1.058(15) 20 ?
C16 P1 1.292(9) 2_565 ?
C16 C24 1.63(2) 2_565 ?
C16 C12 1.951(4) 20 ?
C16 C16 2.01(2) 20 ?
C16 C17 2.008(12) 20 ?
C23 C15 0.47(2) 2_565 ?
C23 C16 0.970(12) 2_565 ?
C23 C24 1.3900 . ?
C23 C28 1.3900 . ?
C23 C14 1.77(3) 2_565 ?
C23 C17 1.770(11) 19_565 ?
C23 C11 1.790(12) 19_565 ?
C23 C21 1.954(19) 25_565 ?
C23 C12 2.033(18) 19_565 ?
C24 C24 1.275(14) 20 ?
C24 C25 1.3900 . ?
C24 C15 1.39(3) 2_565 ?
C24 C14 1.47(3) 2_565 ?
C24 C12 1.581(15) 19_565 ?
C24 C16 1.628(16) 2_565 ?
C24 C13 1.75(2) 2_565 ?
C24 C11 1.745(12) 19_565 ?
C24 C11 1.887(10) 2_565 ?
C24 C12 1.940(16) 2_565 ?
C24 C25 1.992(11) 20 ?
C25 C26 1.3900 . ?
C25 C25 1.599(15) 20 ?
C25 C26 1.617(11) 8_565 ?
C25 C25 1.68(2) 8_565 ?
C25 C14 1.80(3) 2_565 ?
C25 C24 1.992(10) 20 ?
C26 C26 0.628(18) 8_565 ?
C26 C27 1.263(10) 8_565 ?
C26 C27 1.3900 . ?
C26 C25 1.617(16) 8_565 ?
C27 C26 1.263(7) 8_565 ?
C27 C28 1.3900 . ?
C27 C27 1.494(15) 8_565 ?
C28 C15 1.245(19) 2_565 ?
C28 C21 1.50(2) 25_565 ?
C28 C17 1.735(10) 19_565 ?
C28 C22 1.805(12) 19_565 ?
C17 C18 1.3900 . ?
C17 C22 1.3900 . ?
C17 C17 1.570(14) 19_565 ?
C17 C28 1.735(14) 19_565 ?
C17 C23 1.770(11) 19_565 ?
C17 C15 1.937(16) 20 ?
C17 C16 2.008(14) 20 ?
C18 C6 0.93(3) 20 ?
C18 C5 1.336(10) 20 ?
C18 C19 1.3900 . ?
C18 C7 1.50(4) 20 ?
C18 C10C 1.634(18) 2_565 ?
C18 C10B 2.001(16) 17_565 ?
C18 C10 2.02(4) 20 ?
C19 C10C 0.769(15) 2_565 ?
C19 C8 0.81(4) 20 ?
C19 C7 1.09(2) 20 ?
C19 C20 1.3900 . ?
C19 C9 1.55(4) 20 ?
C19 C10B 1.802(17) 17_565 ?
C19 C6 1.859(15) 20 ?
C20 C21 1.3900 . ?
C20 C14 1.522(14) 26 ?
C20 C8 1.62(5) 20 ?
C20 C10C 1.815(15) 2_565 ?
C21 C22 1.226(15) 11 ?
C21 C22 1.3900 . ?
C21 C28 1.50(3) 25_565 ?
C21 C15 1.586(18) 26 ?
C21 C21 1.833(17) 11 ?
C21 C14 1.91(2) 26 ?
C21 C23 1.954(11) 25_565 ?
C22 C22 1.034(14) 11 ?
C22 C21 1.226(9) 11 ?
C22 C22 1.704(16) 19_565 ?
C22 C28 1.805(17) 19_565 ?
C22 C22 1.993(15) 25_565 ?
C10A C10B 0.766(17) 18 ?
C10A C10 0.787(18) 19_565 ?
C10A C9 1.03(2) 19_565 ?
C10A C10A 1.25(3) 18 ?
C10A C10C 1.514(14) . ?
C10A C10B 1.556(14) . ?
C10A C10D 1.564(15) . ?
C10A C10A 1.70(3) 19_565 ?
C10A C10 1.80(2) 4_565 ?
C10A C10D 1.871(18) 18 ?
C10A C5 2.033(15) 19_565 ?
C10B C10A 0.766(17) 18 ?
C10B C10 0.90(2) 4_565 ?
C10B C9 1.11(3) 4_565 ?
C10B C10C 1.13(2) 18 ?
C10B C10B 1.47(3) 18 ?
C10B C5 1.584(16) 4_565 ?
C10B C19 1.80(4) 17_565 ?
C10B C8 1.834(19) 4_565 ?
C10B C10 1.88(2) 18 ?
C10B C10 1.977(18) 19_565 ?
C10B C18 2.00(5) 17_565 ?
C10C C19 0.77(5) 2_565 ?
C10C C9 0.825(19) 19_565 ?
C10C C8 0.897(19) 19_565 ?
C10C C10B 1.13(2) 18 ?
C10C C10 1.535(15) 19_565 ?
C10C C7 1.61(2) 19_565 ?
C10C C18 1.63(3) 2_565 ?
C10C C20 1.82(4) 2_565 ?
C10C C5 2.038(16) 19_565 ?
C10D C10D 0.85(3) 18 ?
C10D C10D 1.63(3) 19_565 ?
C10D C9 1.659(19) 19_565 ?
C10D C10D 1.84(3) 4_565 ?
C10D C10A 1.871(18) 18 ?
