Information card for entry 4305081

Structure parameters

• Formula: C74 H92 N2 Ni
• Calculated formula: C74 H92 N2 Ni
• Title of publication: Synthesis and Characterization of Linear and Square-Planar Nickel Complexes with Primary Amido Ligands
• Authors of publication: Jianfeng Li; Haibin Song; Chunming Cui; Jin-Pei Cheng
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 3468 - 3470
• a: 10.91 ± 0.001 Å
• b: 11.754 ± 0.001 Å
• c: 13.374 ± 0.0014 Å
• α: 76.56 ± 0.008°
• β: 76.32 ± 0.008°
• γ: 70.59 ± 0.008°
• Cell volume: 1549.4 ± 0.3 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1073
• Residual factor for significantly intense reflections: 0.0769
• Weighted residual factors for significantly intense reflections: 0.2028
• Weighted residual factors for all reflections included in the refinement: 0.2288
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No