Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4323168
Preview
Coordinates | 4323168.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C61 H69 B N4 Ni |
---|---|
Calculated formula | C61 H69 B N4 Ni |
Title of publication | The Intra- and Intermolecular Oxidative Coupling of Ni(II)-meso-Octaethyl Mono(pyridine)-Tris(pyrrole) Complex Leading to CC Bonds: Pathways to Oligomeric Porphyrinogens |
Authors of publication | Raffaella Crescenzi; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli |
Journal of publication | Inorganic Chemistry |
Year of publication | 1998 |
Journal volume | 37 |
Pages of publication | 6044 - 6051 |
a | 14.275 ± 0.003 Å |
b | 14.482 ± 0.003 Å |
c | 12.745 ± 0.002 Å |
α | 100.19 ± 0.02° |
β | 101.47 ± 0.02° |
γ | 99.03 ± 0.02° |
Cell volume | 2490.5 ± 0.9 Å3 |
Cell temperature | 25 K |
Ambient diffraction temperature | 143 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2727 |
Residual factor for significantly intense reflections | 0.0721 |
Weighted residual factors for all reflections | 0.2973 |
Weighted residual factors for significantly intense reflections | 0.1748 |
Goodness-of-fit parameter for all reflections | 1.105 |
Goodness-of-fit parameter for significantly intense reflections | 1.335 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKa |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323168.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.