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Information card for entry 4323174
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Coordinates | 4323174.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Tetra-n-butylammonium-tris(μ2-diethylphosphido)-hexachloro- di-rhenium (IV), toluene solvate |
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Chemical name | Tetra-n-butylammonium-tris(μ2-diethylphosphido)-bis(trichloro)- di-rhenium (IV), toluene solvate |
Formula | C38.5 H78 Cl6 N P3 Re2 |
Calculated formula | C38.5 H78 Cl6 N P3 Re2 |
Title of publication | Mixed Chloride/Phosphine Complexes of the Dirhenium Core. 3. Novel Structures with Diethylphosphido-bridges and Terminal Diethylphosphines |
Authors of publication | F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina |
Journal of publication | Inorganic Chemistry |
Year of publication | 1998 |
Journal volume | 37 |
Pages of publication | 6035 - 6043 |
a | 38.746 ± 0.009 Å |
b | 10.322 ± 0.002 Å |
c | 27.277 ± 0.003 Å |
α | 90° |
β | 110.35 ± 0.01° |
γ | 90° |
Cell volume | 10228 ± 3 Å3 |
Cell temperature | 213 ± 2 K |
Ambient diffraction temperature | 213 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0654 |
Residual factor for significantly intense reflections | 0.0522 |
Weighted residual factors for all reflections | 0.1423 |
Weighted residual factors for significantly intense reflections | 0.1265 |
Goodness-of-fit parameter for all reflections | 1.086 |
Goodness-of-fit parameter for significantly intense reflections | 1.106 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323174.html
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