Information card for entry 4323970

Structure parameters

• Formula: C36 H52 Ni P4
• Calculated formula: C36 H44 Ni P4
• Title of publication: Metal Complexes of Mesitylphosphine: Synthesis, Structure, and Spectroscopy
• Authors of publication: Igor V. Kourkine; Stanislav V. Maslennikov; Robert Ditchfield; David S. Glueck; Glenn P. A. Yap; Louise M. Liable-Sands; Arnold L. Rheingold
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 6708 - 6716
• a: 18.584 ± 0.004 Å
• b: 11.506 ± 0.002 Å
• c: 18.965 ± 0.004 Å
• α: 90°
• β: 115.84 ± 0.05°
• γ: 90°
• Cell volume: 3650 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 252 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1489
• Residual factor for significantly intense reflections: 0.09
• Weighted residual factors for all reflections: 0.2671
• Weighted residual factors for significantly intense reflections: 0.1064
• Goodness-of-fit parameter for all reflections: 1.97
• Goodness-of-fit parameter for significantly intense reflections: 1.56
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No