The Potentially Hexadentate Isomeric Macrocycles trans- and cis-6,13-Diethyl-1,4,8,11-tetraazacyclotetradecane-6,13-diamine and Their Cobalt(III) Complexes: Unexpected Conformational Behavior
Authors of publication
Paul V. Bernhardt; Karl A. Byriel; Colin H. L. Kennard; Philip C. Sharpe
Journal of publication
Inorganic Chemistry
Year of publication
1996
Journal volume
35
Pages of publication
2045 - 2052
a
14.461 ± 0.006 Å
b
11.58 ± 0.002 Å
c
15.865 ± 0.005 Å
α
90°
β
111.96 ± 0.01°
γ
90°
Cell volume
2464 ± 1.4 Å3
Cell temperature
296 K
Ambient diffraction temperature
296 K
Number of distinct elements
6
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0755
Residual factor for significantly intense reflections
0.0586
Weighted residual factors for all reflections
0.1706
Weighted residual factors for significantly intense reflections
0.1543
Goodness-of-fit parameter for all reflections
1.046
Goodness-of-fit parameter for significantly intense reflections
