Information card for entry 4327866

Structure parameters

• Formula: C71 H75 B Co F24 P4 Si
• Calculated formula: C78.0128 H79 B Co F24 P4 Si
• Title of publication: A Homologous Series of Cobalt, Rhodium, and Iridium Metalloradicals
• Authors of publication: Ayumi Takaoka; Jonas C. Peters
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 16 - 18
• a: 38.7112 ± 0.0011 Å
• b: 14.863 ± 0.0004 Å
• c: 29.3525 ± 0.0008 Å
• α: 90°
• β: 110.296 ± 0.002°
• γ: 90°
• Cell volume: 15839.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0587
• Weighted residual factors for significantly intense reflections: 0.151
• Weighted residual factors for all reflections included in the refinement: 0.1763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No