Information card for entry 4503076

Structure parameters

• Formula: C44 H60 Cu2 N8 O82.5 V2 W18 Y
• Calculated formula: C44 H32 Cu2 N8 O82.5 V2 W18 Y
• Title of publication: Novel Tungstovanadate Wells−Dawson Organic‒Inorganic Heteropolyoxometalate Compound: Synthesis and Crystal Structure of [Cu2(2,2′-bipy)2(Inic)2(H2O)2][Y(Inic)2(H2O)5]H3[V2W18O62]·5.5H2O (Where 2,2′-bipy = 2,2′-Bipyridine, Inic = γ-Picolinic Acid)
• Authors of publication: Wang, Jingping; Li, Suzhi; Shen, Yue; Niu, Jingyang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2008
• Journal volume: 8
• Journal issue: 2
• Pages of publication: 372
• a: 15.061 ± 0.004 Å
• b: 19.05 ± 0.005 Å
• c: 18.765 ± 0.005 Å
• α: 90°
• β: 106.909 ± 0.004°
• γ: 90°
• Cell volume: 5151 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.1254
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No