#------------------------------------------------------------------------------
#$Date: 2016-03-24 16:08:07 +0100 (jue 24 de mar de 2016) $
#$Revision: 179678 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/00/7000073.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7000073
loop_
_publ_author_name
'Duraczyńska, Dorota'
'Nelson, John H.'
_publ_section_title
;
 Phosphaallyl complexes of Ru(II) derived from
 dicyclohexylvinylphosphine (DCVP).
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              92
_journal_page_last               103
_journal_paper_doi               10.1039/b413446j
_journal_year                    2005
_chemical_formula_sum            'C35 H59 Cl2 F6 P3 Ru'
_chemical_formula_weight         858.70
_chemical_name_common            2
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                101.606(11)
_cell_angle_beta                 100.011(14)
_cell_angle_gamma                113.171(11)
_cell_formula_units_Z            2
_cell_length_a                   10.1094(14)
_cell_length_b                   12.8338(14)
_cell_length_c                   17.610(2)
_cell_measurement_reflns_used    33
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      12.46
_cell_measurement_theta_min      2.44
_cell_volume                     1974.6(5)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.862
_diffrn_measured_fraction_theta_max 0.862
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1361
_diffrn_reflns_av_sigmaI/netI    0.1356
_diffrn_reflns_limit_h_max       1
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            7905
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.81
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.706
_exptl_absorpt_correction_T_max  0.9463
_exptl_absorpt_correction_T_min  0.9179
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.444
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             892
_exptl_crystal_size_max          .46
_exptl_crystal_size_mid          .32
_exptl_crystal_size_min          .16
_refine_diff_density_max         1.510
_refine_diff_density_min         -0.763
_refine_diff_density_rms         0.101
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.048
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     424
_refine_ls_number_reflns         6763
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.1354
_refine_ls_R_factor_gt           0.0721
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0760P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1488
_refine_ls_wR_factor_ref         0.1825
_reflns_number_gt                4136
_reflns_number_total             6763
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b413446j.txt
_cod_data_source_block           jhn521a
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1974.7(4)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7000073
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.72790(7) 0.83627(5) 0.65484(4) 0.0325(2) Uani 1 1 d . . .
P1 P 0.8686(2) 1.01647(17) 0.75454(12) 0.0381(5) Uani 1 1 d . . .
P2 P 0.4853(2) 0.81718(16) 0.65250(11) 0.0340(5) Uani 1 1 d . . .
C1 C 0.8320(9) 0.7429(7) 0.5850(5) 0.048(2) Uani 1 1 d . . .
C2 C 0.8811(10) 0.7535(8) 0.6682(6) 0.055(2) Uani 1 1 d . . .
H2A H 0.9855 0.7933 0.7017 0.066 Uiso 1 1 calc R . .
C3 C 0.7574(10) 0.6885(7) 0.6917(5) 0.052(2) Uani 1 1 d . . .
H3A H 0.7587 0.6750 0.7446 0.062 Uiso 1 1 calc R . .
C4 C 0.6313(9) 0.6395(6) 0.6240(5) 0.046(2) Uani 1 1 d . . .
H4A H 0.5289 0.5864 0.6221 0.055 Uiso 1 1 calc R . .
C5 C 0.6776(9) 0.6733(7) 0.5582(5) 0.0437(19) Uani 1 1 d . . .
H5A H 0.6140 0.6473 0.5027 0.052 Uiso 1 1 calc R . .
C6 C 0.9359(13) 0.7925(10) 0.5358(7) 0.095(4) Uani 1 1 d . . .
H6A H 0.9660 0.7343 0.5122 0.143 Uiso 1 1 calc R . .
H6B H 1.0229 0.8626 0.5701 0.143 Uiso 1 1 calc R . .
H6C H 0.8850 0.8122 0.4938 0.143 Uiso 1 1 calc R . .
C7 C 0.7544(9) 0.9771(6) 0.5954(5) 0.0446(19) Uani 1 1 d . . .
H7A H 0.7572 0.9585 0.5397 0.054 Uiso 1 1 calc R . .
H7B H 0.6981 1.0218 0.6064 0.054 Uiso 1 1 calc R . .
C8 C 0.8869(9) 1.0094(6) 0.6549(5) 0.0435(19) Uani 1 1 d . . .
H8A H 0.9817 1.0227 0.6421 0.052 Uiso 1 1 calc R . .
C9 C 0.8211(8) 1.1369(6) 0.7928(5) 0.0401(18) Uani 1 1 d . . .
H9A H 0.7281 1.1220 0.7545 0.048 Uiso 1 1 calc R . .
C10 C 0.9415(9) 1.2601(7) 0.7966(6) 0.053(2) Uani 1 1 d . . .
H10A H 1.0373 1.2751 0.8307 0.063 Uiso 1 1 calc R . .
H10B H 0.9517 1.2600 0.7428 0.063 Uiso 1 1 calc R . .
C11 C 0.9007(11) 1.3587(8) 0.8298(6) 0.066(3) Uani 1 1 d . . .
H11A H 0.9816 1.4349 0.8350 0.080 Uiso 1 1 calc R . .
H11B H 0.8114 1.3493 0.7923 0.080 Uiso 1 1 calc R . .
C12 C 0.8728(11) 1.3569(8) 0.9115(6) 0.073(3) Uani 1 1 d . . .
H12A H 0.9641 1.3717 0.9500 0.087 Uiso 1 1 calc R . .
H12B H 0.8451 1.4195 0.9307 0.087 Uiso 1 1 calc R . .
C13 C 0.7491(12) 1.2384(9) 0.9061(6) 0.075(3) Uani 1 1 d . . .
H13A H 0.6562 1.2253 0.8699 0.090 Uiso 1 1 calc R . .
H13B H 0.7341 1.2384 0.9590 0.090 Uiso 1 1 calc R . .
C14 C 0.7901(10) 1.1390(7) 0.8748(5) 0.052(2) Uani 1 1 d . . .
H14A H 0.7086 1.0635 0.8701 0.063 Uiso 1 1 calc R . .
H14B H 0.8784 1.1490 0.9135 0.063 Uiso 1 1 calc R . .
C15 C 1.0441(9) 1.0484(8) 0.8290(5) 0.053(2) Uani 1 1 d . . .
H15A H 1.0670 1.1227 0.8691 0.064 Uiso 1 1 calc R . .
C16 C 1.1774(11) 1.0757(12) 0.7999(8) 0.104(5) Uani 1 1 d . . .
H16A H 1.1900 1.1380 0.7744 0.124 Uiso 1 1 calc R . .
H16B H 1.1638 1.0057 0.7596 0.124 Uiso 1 1 calc R . .
C17 C 1.3184(10) 1.1158(11) 0.8691(8) 0.094(4) Uani 1 1 d . . .
H17A H 1.4031 1.1266 0.8474 0.112 Uiso 1 1 calc R . .
H17B H 1.3397 1.1915 0.9056 0.112 Uiso 1 1 calc R . .
C18 C 1.2995(14) 1.0273(11) 0.9147(8) 0.103(4) Uani 1 1 d . . .
H18A H 1.2942 0.9556 0.8803 0.123 Uiso 1 1 calc R . .
H18B H 1.3865 1.0590 0.9610 0.123 Uiso 1 1 calc R . .
C19 C 1.1670(14) 0.9977(13) 0.9418(7) 0.099(4) Uani 1 1 d . . .
H19A H 1.1820 1.0657 0.9845 0.119 Uiso 1 1 calc R . .
H19B H 1.1543 0.9331 0.9650 0.119 Uiso 1 1 calc R . .
C20 C 1.0216(10) 0.9611(8) 0.8759(5) 0.058(2) Uani 1 1 d . . .
H20A H 0.9919 0.8829 0.8398 0.069 Uiso 1 1 calc R . .
H20B H 0.9420 0.9569 0.9008 0.069 Uiso 1 1 calc R . .
C21 C 0.4634(8) 0.9513(6) 0.6889(5) 0.0389(18) Uani 1 1 d . . .
H21A H 0.5010 0.9883 0.7443 0.047 Uiso 1 1 calc R . .
C22 C 0.4016(10) 1.0022(8) 0.6471(6) 0.062(2) Uani 1 1 d . . .
H22A H 0.3619 0.9696 0.5914 0.074 Uiso 1 1 calc R . .
H22B H 0.3975 1.0710 0.6732 0.074 Uiso 1 1 calc R . .
C23 C 0.3979(8) 0.7314(6) 0.7197(4) 0.0347(17) Uani 1 1 d . . .
H23A H 0.3870 0.6507 0.6994 0.042 Uiso 1 1 calc R . .
C24 C 0.4974(9) 0.7826(7) 0.8074(5) 0.047(2) Uani 1 1 d . . .
H24A H 0.5960 0.7877 0.8083 0.056 Uiso 1 1 calc R . .
H24B H 0.5090 0.8622 0.8298 0.056 Uiso 1 1 calc R . .
C25 C 0.4297(10) 0.7055(8) 0.8589(5) 0.058(2) Uani 1 1 d . . .
H25A H 0.4268 0.6282 0.8393 0.069 Uiso 1 1 calc R . .
H25B H 0.4929 0.7416 0.9142 0.069 Uiso 1 1 calc R . .
C26 C 0.2727(10) 0.6902(8) 0.8571(5) 0.057(2) Uani 1 1 d . . .
H26A H 0.2769 0.7658 0.8835 0.069 Uiso 1 1 calc R . .
H26B H 0.2300 0.6349 0.8864 0.069 Uiso 1 1 calc R . .
C27 C 0.1724(9) 0.6433(8) 0.7698(5) 0.056(2) Uani 1 1 d . . .
H27A H 0.1569 0.5629 0.7458 0.067 Uiso 1 1 calc R . .
H27B H 0.0754 0.6409 0.7700 0.067 Uiso 1 1 calc R . .
C28 C 0.2420(8) 0.7210(7) 0.7192(5) 0.045(2) Uani 1 1 d . . .
H28A H 0.2491 0.7995 0.7403 0.054 Uiso 1 1 calc R . .
H28B H 0.1780 0.6874 0.6641 0.054 Uiso 1 1 calc R . .
C29 C 0.3402(8) 0.7415(6) 0.5517(4) 0.0357(17) Uani 1 1 d . . .
H29A H 0.2559 0.7593 0.5572 0.043 Uiso 1 1 calc R . .
C30 C 0.3978(9) 0.7931(7) 0.4850(5) 0.0446(19) Uani 1 1 d . . .
H30A H 0.4360 0.8788 0.5024 0.054 Uiso 1 1 calc R . .
H30B H 0.4790 0.7747 0.4756 0.054 Uiso 1 1 calc R . .
C31 C 0.2706(9) 0.7403(7) 0.4069(5) 0.056(2) Uani 1 1 d . . .
H31A H 0.3095 0.7692 0.3648 0.067 Uiso 1 1 calc R . .
H31B H 0.1951 0.7668 0.4151 0.067 Uiso 1 1 calc R . .
C32 C 0.1477(9) 0.5549(7) 0.4456(5) 0.052(2) Uani 1 1 d . . .
H32A H 0.1084 0.4691 0.4278 0.063 Uiso 1 1 calc R . .
H32B H 0.0673 0.5735 0.4564 0.063 Uiso 1 1 calc R . .
C33 C 0.1971(10) 0.6035(7) 0.3793(5) 0.054(2) Uani 1 1 d . . .
H33A H 0.1112 0.5736 0.3326 0.065 Uiso 1 1 calc R . .
H33B H 0.2683 0.5765 0.3635 0.065 Uiso 1 1 calc R . .
C34 C 0.2771(9) 0.6061(6) 0.5249(5) 0.0437(19) Uani 1 1 d . . .
H34A H 0.2399 0.5746 0.5666 0.052 Uiso 1 1 calc R . .
H34B H 0.3554 0.5835 0.5159 0.052 Uiso 1 1 calc R . .
P3 P 0.3687(3) 0.3542(2) 0.70252(16) 0.0649(7) Uani 1 1 d . . .
F1 F 0.2887(9) 0.4117(6) 0.6525(5) 0.132(3) Uani 1 1 d . . .
F2 F 0.5080(8) 0.4811(6) 0.7426(4) 0.122(3) Uani 1 1 d . . .
F3 F 0.4306(10) 0.3290(9) 0.6302(5) 0.154(3) Uani 1 1 d . . .
F4 F 0.4522(9) 0.2978(7) 0.7510(5) 0.132(3) Uani 1 1 d . . .
F5 F 0.2293(9) 0.2315(6) 0.6644(5) 0.137(3) Uani 1 1 d . . .
F6 F 0.3058(10) 0.3810(7) 0.7748(5) 0.145(3) Uani 1 1 d . . .
C35 C 0.6675(14) 0.5547(12) 0.9294(8) 0.110(5) Uani 1 1 d . . .
H35A H 0.5792 0.5678 0.9164 0.132 Uiso 1 1 calc R . .
H35B H 0.6482 0.4805 0.8917 0.132 Uiso 1 1 calc R . .
Cl1 Cl 0.8171(5) 0.6681(4) 0.9176(3) 0.1555(19) Uani 1 1 d . . .
Cl2 Cl 0.6967(4) 0.5427(4) 1.0250(2) 0.1358(16) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C8 Ru1 C2 98.7(3) . . ?
C8 Ru1 C1 92.8(3) . . ?
C2 Ru1 C1 37.6(3) . . ?
C8 Ru1 C7 37.3(3) . . ?
C2 Ru1 C7 124.7(3) . . ?
C1 Ru1 C7 99.1(3) . . ?
C8 Ru1 C4 153.9(3) . . ?
C2 Ru1 C4 61.2(3) . . ?
C1 Ru1 C4 61.0(3) . . ?
C7 Ru1 C4 140.1(3) . . ?
C8 Ru1 C5 120.6(3) . . ?
C2 Ru1 C5 61.9(3) . . ?
C1 Ru1 C5 36.5(3) . . ?
C7 Ru1 C5 106.3(3) . . ?
C4 Ru1 C5 36.8(3) . . ?
C8 Ru1 C3 132.4(3) . . ?
C2 Ru1 C3 36.5(3) . . ?
C1 Ru1 C3 61.7(3) . . ?
C7 Ru1 C3 160.1(3) . . ?
C4 Ru1 C3 36.8(3) . . ?
C5 Ru1 C3 61.8(3) . . ?
C8 Ru1 P1 46.8(2) . . ?
C2 Ru1 P1 100.4(2) . . ?
C1 Ru1 P1 122.3(2) . . ?
C7 Ru1 P1 73.1(2) . . ?
C4 Ru1 P1 146.7(2) . . ?
C5 Ru1 P1 158.8(2) . . ?
C3 Ru1 P1 111.8(2) . . ?
C8 Ru1 P2 114.9(2) . . ?
C2 Ru1 P2 146.0(3) . . ?
C1 Ru1 P2 137.9(2) . . ?
C7 Ru1 P2 87.4(2) . . ?
C4 Ru1 P2 87.6(2) . . ?
C5 Ru1 P2 101.7(2) . . ?
C3 Ru1 P2 110.0(3) . . ?
P1 Ru1 P2 99.41(7) . . ?
C8 P1 C9 110.6(3) . . ?
C8 P1 C15 113.3(4) . . ?
C9 P1 C15 105.4(4) . . ?
C8 P1 Ru1 62.3(2) . . ?
C9 P1 Ru1 130.7(3) . . ?
C15 P1 Ru1 122.5(3) . . ?
C21 P2 C23 99.5(3) . . ?
C21 P2 C29 102.5(3) . . ?
C23 P2 C29 103.9(3) . . ?
C21 P2 Ru1 118.5(2) . . ?
C23 P2 Ru1 113.8(2) . . ?
C29 P2 Ru1 116.4(2) . . ?
C5 C1 C2 108.1(7) . . ?
C5 C1 C6 127.8(9) . . ?
C2 C1 C6 124.0(9) . . ?
C5 C1 Ru1 72.2(4) . . ?
C2 C1 Ru1 70.7(4) . . ?
C6 C1 Ru1 126.2(6) . . ?
C3 C2 C1 108.3(8) . . ?
C3 C2 Ru1 72.9(4) . . ?
C1 C2 Ru1 71.7(4) . . ?
C2 C3 C4 107.4(8) . . ?
C2 C3 Ru1 70.6(5) . . ?
C4 C3 Ru1 71.3(4) . . ?
C5 C4 C3 108.9(8) . . ?
C5 C4 Ru1 71.7(4) . . ?
C3 C4 Ru1 71.9(4) . . ?
C1 C5 C4 107.4(7) . . ?
C1 C5 Ru1 71.3(5) . . ?
C4 C5 Ru1 71.5(4) . . ?
C8 C7 Ru1 69.6(4) . . ?
C7 C8 P1 115.3(6) . . ?
C7 C8 Ru1 73.1(4) . . ?
P1 C8 Ru1 70.9(3) . . ?
C14 C9 C10 110.3(7) . . ?
C14 C9 P1 112.4(5) . . ?
C10 C9 P1 112.7(5) . . ?
C11 C10 C9 111.6(7) . . ?
C12 C11 C10 111.2(7) . . ?
C13 C12 C11 110.9(8) . . ?
C12 C13 C14 110.0(8) . . ?
C13 C14 C9 112.3(7) . . ?
C16 C15 C20 113.9(7) . . ?
C16 C15 P1 116.2(7) . . ?
C20 C15 P1 112.7(6) . . ?
C15 C16 C17 111.3(10) . . ?
C18 C17 C16 111.4(9) . . ?
C19 C18 C17 112.4(10) . . ?
C18 C19 C20 115.0(9) . . ?
C15 C20 C19 110.6(8) . . ?
C22 C21 P2 128.4(7) . . ?
C28 C23 C24 108.9(6) . . ?
C28 C23 P2 113.7(5) . . ?
C24 C23 P2 112.4(5) . . ?
C25 C24 C23 111.2(7) . . ?
C26 C25 C24 111.8(7) . . ?
C25 C26 C27 110.9(7) . . ?
C28 C27 C26 111.4(7) . . ?
C27 C28 C23 111.3(6) . . ?
C34 C29 C30 110.6(6) . . ?
C34 C29 P2 114.3(5) . . ?
C30 C29 P2 111.8(5) . . ?
C31 C30 C29 110.0(6) . . ?
C30 C31 C33 112.2(7) . . ?
C33 C32 C34 112.5(7) . . ?
C32 C33 C31 111.0(7) . . ?
C29 C34 C32 108.7(6) . . ?
F3 P3 F5 89.9(5) . . ?
F3 P3 F6 179.1(5) . . ?
F5 P3 F6 90.4(5) . . ?
F3 P3 F4 91.8(5) . . ?
F5 P3 F4 90.5(4) . . ?
F6 P3 F4 89.1(5) . . ?
F3 P3 F1 86.6(5) . . ?
F5 P3 F1 90.3(4) . . ?
F6 P3 F1 92.5(5) . . ?
F4 P3 F1 178.2(5) . . ?
F3 P3 F2 91.6(5) . . ?
F5 P3 F2 178.3(5) . . ?
F6 P3 F2 88.1(5) . . ?
F4 P3 F2 90.4(4) . . ?
F1 P3 F2 88.9(4) . . ?
Cl2 C35 Cl1 112.8(7) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 C8 2.170(7) . ?
Ru1 C2 2.203(7) . ?
Ru1 C1 2.215(7) . ?
Ru1 C7 2.216(7) . ?
Ru1 C4 2.225(7) . ?
Ru1 C5 2.227(7) . ?
Ru1 C3 2.232(8) . ?
Ru1 P1 2.316(2) . ?
Ru1 P2 2.359(2) . ?
P1 C8 1.785(8) . ?
P1 C9 1.830(7) . ?
P1 C15 1.854(8) . ?
P2 C21 1.825(7) . ?
P2 C23 1.875(7) . ?
P2 C29 1.878(7) . ?
C1 C5 1.391(11) . ?
C1 C2 1.424(12) . ?
C1 C6 1.506(13) . ?
C2 C3 1.388(12) . ?
C3 C4 1.408(11) . ?
C4 C5 1.407(11) . ?
C7 C8 1.402(11) . ?
C9 C14 1.528(11) . ?
C9 C10 1.549(10) . ?
C10 C11 1.519(11) . ?
C11 C12 1.517(13) . ?
C12 C13 1.513(14) . ?
C13 C14 1.521(12) . ?
C15 C16 1.464(13) . ?
C15 C20 1.492(10) . ?
C16 C17 1.533(14) . ?
C17 C18 1.490(15) . ?
C18 C19 1.436(16) . ?
C19 C20 1.540(13) . ?
C21 C22 1.308(10) . ?
C23 C28 1.527(10) . ?
C23 C24 1.536(10) . ?
C24 C25 1.521(10) . ?
C25 C26 1.514(11) . ?
C26 C27 1.536(12) . ?
C27 C28 1.519(10) . ?
C29 C34 1.531(10) . ?
C29 C30 1.550(10) . ?
C30 C31 1.526(11) . ?
C31 C33 1.541(11) . ?
C32 C33 1.502(11) . ?
C32 C34 1.553(11) . ?
P3 F3 1.545(7) . ?
P3 F5 1.554(7) . ?
P3 F6 1.556(7) . ?
P3 F4 1.563(7) . ?
P3 F1 1.567(7) . ?
P3 F2 1.588(7) . ?
C35 Cl2 1.706(13) . ?
C35 Cl1 1.717(13) . ?
