#------------------------------------------------------------------------------
#$Date: 2016-03-25 08:10:57 +0100 (vie 25 de mar de 2016) $
#$Revision: 179716 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/18/7001843.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7001843
loop_
_publ_author_name
'Deng, Zhao-Peng'
'Zhu, Zhi-Biao'
'Gao, Shan'
'Huo, Li-Hua'
'Zhao, Hui'
'Ng, Seik Weng'
_publ_section_title
;
 A series of silver(i) pyridone-sulfonates with 1-D
 “butterfly” chain, 2-D lamellar network and 3-D pillared
 layered frameworks: syntheses, structures and characterizations
;
_journal_issue                   33
_journal_name_full               'Dalton Transactions'
_journal_page_first              6552
_journal_page_last               6561
_journal_paper_doi               10.1039/b907389b
_journal_year                    2009
_chemical_formula_moiety         'C10 H10 Ag3 N3 O12 S2'
_chemical_formula_sum            'C10 H10 Ag3 N3 O12 S2'
_chemical_formula_weight         751.94
_chemical_name_systematic
;
?
;
_space_group_IT_number           7
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P -2yc'
_symmetry_space_group_name_H-M   'P 1 c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 125.214(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   11.8808(12)
_cell_length_b                   5.3522(3)
_cell_length_c                   17.1234(12)
_cell_measurement_reflns_used    7691
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.17
_cell_volume                     889.59(12)
_computing_cell_refinement       RAPID-AUTO
_computing_data_collection       'RAPID-AUTO (Rigaku Corporation, 1998)'
_computing_data_reduction
'CrystalStructure (Rigaku/MSC and Rigaku Corporation, 2002)'
_computing_molecular_graphics    'ORTEP-II (Johnson, 1976)'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      295(2)
_diffrn_detector_area_resol_mean 10.000
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0258
_diffrn_reflns_av_sigmaI/netI    0.0345
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            8079
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.46
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.578
_exptl_absorpt_correction_T_max  0.591
_exptl_absorpt_correction_T_min  0.425
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'ABSCOR (Higashi, 1995)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.807
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             720
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.243
_refine_diff_density_min         -0.777
_refine_diff_density_rms         0.116
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.45(3)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.108
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     278
_refine_ls_number_reflns         3921
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      1.107
_refine_ls_R_factor_all          0.0310
_refine_ls_R_factor_gt           0.0272
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0301P)²+1.0931P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0619
_refine_ls_wR_factor_ref         0.0699
_reflns_number_gt                3698
_reflns_number_total             3921
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            b907389b.txt
_cod_data_source_block           complex4
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P c'
_cod_database_code               7001843
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.49989(5) 0.88380(8) 0.49997(3) 0.03588(10) Uani 1 1 d . . .
Ag2 Ag 0.34752(6) 1.25484(8) 0.58135(4) 0.05239(17) Uani 1 1 d . . .
Ag3 Ag 0.23010(4) 0.76967(10) 0.66038(3) 0.04440(13) Uani 1 1 d . . .
S1 S 0.15587(11) 0.7230(2) 0.44094(8) 0.0211(2) Uani 1 1 d . . .
S2 S 0.55573(12) 0.7731(2) 0.71672(8) 0.0237(3) Uani 1 1 d . . .
O1 O 0.2713(4) 0.8932(7) 0.4754(3) 0.0323(8) Uani 1 1 d . . .
O2 O 0.0923(5) 0.7536(8) 0.4919(3) 0.0369(10) Uani 1 1 d . . .
O3 O 0.1888(4) 0.4658(7) 0.4366(3) 0.0327(9) Uani 1 1 d . . .
O4 O -0.2641(4) 1.0489(7) 0.0528(2) 0.0295(8) Uani 1 1 d . . .
O5 O 0.6107(5) 0.7310(9) 0.6616(3) 0.0429(11) Uani 1 1 d . . .
O6 O 0.5234(4) 1.0326(7) 0.7193(3) 0.0418(10) Uani 1 1 d . . .
O7 O 0.4415(4) 0.6081(7) 0.6904(3) 0.0350(9) Uani 1 1 d . . .
O8 O 0.9950(3) 0.4928(8) 1.1079(2) 0.0306(8) Uani 1 1 d . . .
O9 O 0.4807(4) 1.3466(8) 0.4783(3) 0.0415(10) Uani 1 1 d . . .
O10 O 0.3938(5) 1.6114(8) 0.3630(3) 0.0420(10) Uani 1 1 d . . .
O11 O 0.3419(5) 1.2182(8) 0.3336(3) 0.0469(12) Uani 1 1 d . . .
O1W O 0.2222(4) 1.2133(9) 0.6769(3) 0.0425(11) Uani 1 1 d D . .
H1W1 H 0.140(3) 1.250(14) 0.656(6) 0.064 Uiso 1 1 d D . .
H1W2 H 0.278(7) 1.279(14) 0.731(3) 0.064 Uiso 1 1 d D . .
N1 N -0.0531(4) 1.0841(8) 0.1931(3) 0.0256(9) Uani 1 1 d . . .
H1N H -0.0376 1.2116 0.1700 0.031 Uiso 1 1 calc R . .
N2 N 0.7819(4) 0.4335(7) 0.9691(3) 0.0247(8) Uani 1 1 d . . .
H2N H 0.7710 0.3073 0.9952 0.030 Uiso 1 1 calc R . .
N3 N 0.4049(4) 1.3902(8) 0.3914(3) 0.0266(9) Uani 1 1 d . . .
C1 C 0.0284(5) 0.8114(9) 0.3225(3) 0.0223(10) Uani 1 1 d . . .
C2 C -0.0979(5) 0.6790(9) 0.2678(3) 0.0240(10) Uani 1 1 d . . .
H2 H -0.1122 0.5401 0.2937 0.029 Uiso 1 1 calc R . .
C3 C -0.1981(5) 0.7549(9) 0.1777(4) 0.0271(11) Uani 1 1 d . . .
H3 H -0.2808 0.6675 0.1425 0.033 Uiso 1 1 calc R . .
C4 C -0.1783(5) 0.9662(9) 0.1363(3) 0.0215(9) Uani 1 1 d . . .
C5 C 0.0479(5) 1.0110(9) 0.2837(3) 0.0230(9) Uani 1 1 d . . .
H5 H 0.1304 1.0990 0.3189 0.028 Uiso 1 1 calc R . .
C6 C 0.6900(5) 0.6939(9) 0.8356(3) 0.0223(9) Uani 1 1 d . . .
C7 C 0.8123(5) 0.8349(10) 0.8853(4) 0.0281(11) Uani 1 1 d . . .
H7 H 0.8214 0.9731 0.8564 0.034 Uiso 1 1 calc R . .
C8 C 0.9170(6) 0.7687(9) 0.9755(4) 0.0299(12) Uani 1 1 d . . .
H8 H 0.9985 0.8601 1.0076 0.036 Uiso 1 1 calc R . .
C9 C 0.9035(5) 0.5600(10) 1.0218(3) 0.0250(10) Uani 1 1 d . . .
C10 C 0.6765(5) 0.4933(9) 0.8779(3) 0.0252(10) Uani 1 1 d . . .
H10 H 0.5965 0.3978 0.8451 0.030 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O10 Ag1 O5 122.88(16) 1_545 . ?
O10 Ag1 O4 107.23(14) 1_545 2_675 ?
O5 Ag1 O4 82.75(14) . 2_675 ?
O10 Ag1 O9 120.27(13) 1_545 . ?
O5 Ag1 O9 116.63(15) . . ?
O4 Ag1 O9 83.96(14) 2_675 . ?
O10 Ag1 O1 86.59(14) 1_545 . ?
O5 Ag1 O1 91.23(14) . . ?
O4 Ag1 O1 166.07(11) 2_675 . ?
O9 Ag1 O1 87.57(13) . . ?
O1 Ag1 O9 90.02(14) . 1_545 ?
O5 Ag1 O9 76.21(14) . 1_545 ?
O9 Ag1 O9 166.92(15) . 1_545 ?
O11 Ag1 O9 121.39(13) . 1_545 ?
O4 Ag1 O9 100.61(14) 2_675 1_545 ?
O10 Ag1 O9 46.75(14) 1_545 1_545 ?
O11 Ag1 O1 78.46(15) . . ?
O11 Ag1 O5 159.12(13) . . ?
O11 Ag1 O9 45.56(14) . . ?
O11 Ag1 O4 103.05(14) . 2_675 ?
O11 Ag1 O10 75.07(13) . 1_545 ?
O3 Ag2 O6 172.90(16) 1_565 . ?
O3 Ag2 O7 99.74(12) 1_565 1_565 ?
O6 Ag2 O7 82.82(13) . 1_565 ?
O3 Ag2 O1 82.51(12) 1_565 . ?
O6 Ag2 O1 94.50(13) . . ?
O7 Ag2 O1 175.50(14) 1_565 . ?
O1W Ag2 O1 106.14(15) . . ?
O1 Ag2 O9 77.76(15) . . ?
O1W Ag2 O6 80.69(15) . . ?
O6 Ag2 O9 101.86(14) . . ?
O1W Ag2 O9 175.26(15) . . ?
O1W Ag2 O3 106.30(16) . 1_565 ?
O9 Ag2 O3 71.25(14) . 1_565 ?
O9 Ag2 O7 99.22(15) . 1_565 ?
O1W Ag2 O7 77.04(15) . 1_565 ?
O2 Ag3 O1W 97.68(15) . . ?
O2 Ag3 O7 98.65(14) . . ?
O1W Ag3 O7 115.85(15) . . ?
O2 Ag3 O11 171.67(16) . 2_575 ?
O1W Ag3 O11 82.07(15) . 2_575 ?
O7 Ag3 O11 88.89(14) . 2_575 ?
O1W Ag3 O1W 164.99(13) . 1_545 ?
O2 Ag3 O1W 92.42(13) . 1_545 ?
O7 Ag3 O1W 73.15(13) . 1_545 ?
O8 Ag3 O1W 56.35(13) 2_464 1_545 ?
O11 Ag3 O1W 86.35(14) 2_575 1_545 ?
O8 Ag3 O1W 115.97(14) 2_464 . ?
O8 Ag3 O2 74.10(14) 2_464 . ?
O8 Ag3 O7 128.09(16) 2_464 . ?
O8 Ag3 O11 98.43(14) 2_464 2_575 ?
O3 S1 O2 112.8(2) . . ?
O3 S1 O1 113.4(2) . . ?
O2 S1 O1 112.3(3) . . ?
O3 S1 C1 106.0(2) . . ?
O2 S1 C1 105.2(2) . . ?
O1 S1 C1 106.4(2) . . ?
O5 S2 O6 113.4(3) . . ?
O5 S2 O7 113.3(3) . . ?
O6 S2 O7 112.1(2) . . ?
O5 S2 C6 105.5(2) . . ?
O6 S2 C6 105.9(2) . . ?
O7 S2 C6 105.8(2) . . ?
S1 O1 Ag2 130.9(2) . . ?
S1 O1 Ag1 137.2(2) . . ?
Ag2 O1 Ag1 89.41(12) . . ?
S1 O2 Ag3 120.2(2) . . ?
S1 O3 Ag2 118.5(2) . 1_545 ?
C4 O4 Ag1 118.6(3) . 2_474 ?
S2 O5 Ag1 122.8(3) . . ?
S2 O6 Ag2 123.1(2) . . ?
S2 O7 Ag3 121.2(2) . . ?
S2 O7 Ag2 130.1(3) . 1_545 ?
Ag3 O7 Ag2 98.90(13) . 1_545 ?
N3 O9 Ag1 107.8(3) . . ?
N3 O10 Ag1 108.3(3) . 1_565 ?
N3 O11 Ag3 127.1(3) . 2_574 ?
Ag3 O1W H1W1 107(5) . . ?
Ag3 O1W H1W2 119(6) . . ?
H1W1 O1W H1W2 111(8) . . ?
C5 N1 C4 123.9(4) . . ?
C5 N1 H1N 118.0 . . ?
C4 N1 H1N 118.0 . . ?
C10 N2 C9 124.4(4) . . ?
C10 N2 H2N 117.8 . . ?
C9 N2 H2N 117.8 . . ?
O11 N3 O9 120.4(4) . . ?
O11 N3 O10 120.7(4) . . ?
O9 N3 O10 118.9(4) . . ?
C5 C1 C2 119.2(4) . . ?
C5 C1 S1 120.3(4) . . ?
C2 C1 S1 120.5(4) . . ?
C3 C2 C1 120.0(4) . . ?
C3 C2 H2 120.0 . . ?
C1 C2 H2 120.0 . . ?
C2 C3 C4 121.0(4) . . ?
C2 C3 H3 119.5 . . ?
C4 C3 H3 119.5 . . ?
O4 C4 N1 118.5(4) . . ?
O4 C4 C3 125.8(4) . . ?
N1 C4 C3 115.7(4) . . ?
C1 C5 N1 120.1(4) . . ?
C1 C5 H5 120.0 . . ?
N1 C5 H5 120.0 . . ?
C10 C6 C7 120.0(4) . . ?
C10 C6 S2 119.9(4) . . ?
C7 C6 S2 120.0(4) . . ?
C8 C7 C6 119.9(4) . . ?
C8 C7 H7 120.1 . . ?
C6 C7 H7 120.1 . . ?
C7 C8 C9 120.8(5) . . ?
C7 C8 H8 119.6 . . ?
C9 C8 H8 119.6 . . ?
O8 C9 N2 119.7(4) . . ?
O8 C9 C8 124.5(5) . . ?
N2 C9 C8 115.8(4) . . ?
C6 C10 N2 119.0(4) . . ?
C6 C10 H10 120.5 . . ?
N2 C10 H10 120.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O10 2.410(4) 1_545 ?
Ag1 O5 2.421(4) . ?
Ag1 O4 2.426(4) 2_675 ?
Ag1 O9 2.495(5) . ?
Ag1 O1 2.497(4) . ?
Ag1 O9 2.893(5) 1_545 ?
Ag1 O11 2.946(4) . ?
Ag2 O3 2.362(4) 1_565 ?
Ag2 O6 2.381(4) . ?
Ag2 O7 2.429(4) 1_565 ?
Ag2 O1 2.442(4) . ?
Ag2 O1w 2.788(6) . ?
Ag2 O9 3.013(6) . ?
Ag3 O2 2.359(4) . ?
Ag3 O1W 2.400(5) . ?
Ag3 O7 2.415(4) . ?
Ag3 O11 2.454(4) 2_575 ?
Ag3 O1W 2.998(5) 1_545 ?
Ag3 O8 2.773(4) 2_464 ?
S1 O3 1.445(4) . ?
S1 O2 1.456(4) . ?
S1 O1 1.458(4) . ?
S1 C1 1.757(5) . ?
S2 O5 1.442(4) . ?
S2 O6 1.448(4) . ?
S2 O7 1.456(4) . ?
S2 C6 1.767(5) . ?
O3 Ag2 2.362(4) 1_545 ?
O4 C4 1.263(5) . ?
O4 Ag1 2.426(4) 2_474 ?
O7 Ag2 2.429(4) 1_545 ?
O8 C9 1.280(5) . ?
O9 N3 1.239(6) . ?
O10 N3 1.258(6) . ?
O10 Ag1 2.410(4) 1_565 ?
O11 N3 1.238(6) . ?
O11 Ag3 2.454(4) 2_574 ?
O1W H1W1 0.85(7) . ?
O1W H1W2 0.84(5) . ?
N1 C5 1.362(6) . ?
N1 C4 1.374(6) . ?
N1 H1N 0.8600 . ?
N2 C10 1.362(6) . ?
N2 C9 1.363(6) . ?
N2 H2N 0.8600 . ?
C1 C5 1.346(7) . ?
C1 C2 1.418(7) . ?
C2 C3 1.358(7) . ?
C2 H2 0.9300 . ?
C3 C4 1.424(6) . ?
C3 H3 0.9300 . ?
C5 H5 0.9300 . ?
C6 C10 1.356(7) . ?
C6 C7 1.407(7) . ?
C7 C8 1.357(7) . ?
C7 H7 0.9300 . ?
C8 C9 1.431(7) . ?
C8 H8 0.9300 . ?
C10 H10 0.9300 . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O1W H1W1 O8 0.85(7) 1.97(4) 2.735(6) 148(7) 2_474
O1W H1W2 O10 0.84(5) 1.94(5) 2.774(6) 170(8) 2_585
N1 H1N O8 0.86 2.00 2.863(6) 175.7 1_464
N2 H2N O4 0.86 1.88 2.738(5) 174.9 1_646
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O3 S1 O1 Ag2 -140.9(2) . . . . ?
O2 S1 O1 Ag2 -11.5(4) . . . . ?
C1 S1 O1 Ag2 103.0(3) . . . . ?
O3 S1 O1 Ag1 15.3(4) . . . . ?
O2 S1 O1 Ag1 144.6(3) . . . . ?
C1 S1 O1 Ag1 -100.9(3) . . . . ?
O3 Ag2 O1 S1 -87.3(3) 1_565 . . . ?
O6 Ag2 O1 S1 99.2(3) . . . . ?
O3 Ag2 O1 Ag1 108.70(13) 1_565 . . . ?
O6 Ag2 O1 Ag1 -64.83(15) . . . . ?
O10 Ag1 O1 S1 32.9(3) 1_545 . . . ?
O5 Ag1 O1 S1 -90.0(3) . . . . ?
O4 Ag1 O1 S1 -154.1(4) 2_675 . . . ?
O9 Ag1 O1 S1 153.4(3) . . . . ?
O10 Ag1 O1 Ag2 -164.95(13) 1_545 . . . ?
O5 Ag1 O1 Ag2 72.19(14) . . . . ?
O4 Ag1 O1 Ag2 8.1(6) 2_675 . . . ?
O9 Ag1 O1 Ag2 -44.42(12) . . . . ?
O3 S1 O2 Ag3 81.7(3) . . . . ?
O1 S1 O2 Ag3 -47.9(3) . . . . ?
C1 S1 O2 Ag3 -163.2(2) . . . . ?
O1W Ag3 O2 S1 102.4(3) . . . . ?
O7 Ag3 O2 S1 -15.3(3) . . . . ?
O2 S1 O3 Ag2 -61.7(3) . . . 1_545 ?
O1 S1 O3 Ag2 67.3(3) . . . 1_545 ?
C1 S1 O3 Ag2 -176.3(2) . . . 1_545 ?
O6 S2 O5 Ag1 -51.1(4) . . . . ?
O7 S2 O5 Ag1 78.1(3) . . . . ?
C6 S2 O5 Ag1 -166.6(3) . . . . ?
O10 Ag1 O5 S2 -111.4(3) 1_545 . . . ?
O4 Ag1 O5 S2 142.7(3) 2_675 . . . ?
O9 Ag1 O5 S2 63.2(4) . . . . ?
O1 Ag1 O5 S2 -24.7(3) . . . . ?
O5 S2 O6 Ag2 65.6(4) . . . . ?
O7 S2 O6 Ag2 -64.2(4) . . . . ?
C6 S2 O6 Ag2 -179.2(3) . . . . ?
O7 Ag2 O6 S2 -173.0(4) 1_565 . . . ?
O1 Ag2 O6 S2 3.4(3) . . . . ?
O5 S2 O7 Ag3 -131.5(3) . . . . ?
O6 S2 O7 Ag3 -1.6(3) . . . . ?
C6 S2 O7 Ag3 113.4(2) . . . . ?
O5 S2 O7 Ag2 6.7(4) . . . 1_545 ?
O6 S2 O7 Ag2 136.6(3) . . . 1_545 ?
C6 S2 O7 Ag2 -108.4(3) . . . 1_545 ?
O2 Ag3 O7 S2 102.9(3) . . . . ?
O1W Ag3 O7 S2 0.0(3) . . . . ?
O11 Ag3 O7 S2 -80.6(3) 2_575 . . . ?
O2 Ag3 O7 Ag2 -45.98(16) . . . 1_545 ?
O1W Ag3 O7 Ag2 -148.92(14) . . . 1_545 ?
O11 Ag3 O7 Ag2 130.45(16) 2_575 . . 1_545 ?
O10 Ag1 O9 N3 4.3(4) 1_545 . . . ?
O5 Ag1 O9 N3 -170.5(3) . . . . ?
O4 Ag1 O9 N3 110.7(4) 2_675 . . . ?
O1 Ag1 O9 N3 -80.3(4) . . . . ?
Ag3 O11 N3 O9 -164.8(4) 2_574 . . . ?
Ag3 O11 N3 O10 14.9(7) 2_574 . . . ?
Ag1 O9 N3 O11 8.2(6) . . . . ?
Ag1 O9 N3 O10 -171.5(4) . . . . ?
Ag1 O10 N3 O11 169.8(4) 1_565 . . . ?
Ag1 O10 N3 O9 -10.6(6) 1_565 . . . ?
O3 S1 C1 C5 -123.9(4) . . . . ?
O2 S1 C1 C5 116.4(4) . . . . ?
O1 S1 C1 C5 -2.9(5) . . . . ?
O3 S1 C1 C2 58.3(5) . . . . ?
O2 S1 C1 C2 -61.4(5) . . . . ?
O1 S1 C1 C2 179.3(4) . . . . ?
C5 C1 C2 C3 -0.5(8) . . . . ?
S1 C1 C2 C3 177.3(4) . . . . ?
C1 C2 C3 C4 0.4(8) . . . . ?
Ag1 O4 C4 N1 -131.8(4) 2_474 . . . ?
Ag1 O4 C4 C3 49.5(6) 2_474 . . . ?
C5 N1 C4 O4 -179.4(4) . . . . ?
C5 N1 C4 C3 -0.5(7) . . . . ?
C2 C3 C4 O4 178.9(5) . . . . ?
C2 C3 C4 N1 0.1(7) . . . . ?
C2 C1 C5 N1 0.2(7) . . . . ?
S1 C1 C5 N1 -177.7(4) . . . . ?
C4 N1 C5 C1 0.4(7) . . . . ?
O5 S2 C6 C10 -113.3(5) . . . . ?
O6 S2 C6 C10 126.2(4) . . . . ?
O7 S2 C6 C10 7.1(5) . . . . ?
O5 S2 C6 C7 64.9(5) . . . . ?
O6 S2 C6 C7 -55.6(5) . . . . ?
O7 S2 C6 C7 -174.7(4) . . . . ?
C10 C6 C7 C8 0.3(8) . . . . ?
S2 C6 C7 C8 -177.9(4) . . . . ?
C6 C7 C8 C9 -1.5(9) . . . . ?
C10 N2 C9 O8 178.2(5) . . . . ?
C10 N2 C9 C8 0.1(7) . . . . ?
C7 C8 C9 O8 -176.8(6) . . . . ?
C7 C8 C9 N2 1.3(8) . . . . ?
C7 C6 C10 N2 0.9(8) . . . . ?
S2 C6 C10 N2 179.1(4) . . . . ?
C9 N2 C10 C6 -1.1(8) . . . . ?
