#------------------------------------------------------------------------------
#$Date: 2016-03-25 08:50:59 +0100 (vie 25 de mar de 2016) $
#$Revision: 179734 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/30/7003074.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7003074
loop_
_publ_author_name
'Zhou, Yongbo'
'Chen, Wanzhi'
'Wang, Daqi'
_publ_section_title
;
 Mononuclear, dinuclear, hexanuclear, and one-dimensional polymeric
 silver complexes having ligand-supported and unsupported argentophilic
 interactions stabilized by pincer-like 2,6-bis(5-pyrazolyl)pyridine
 ligands
;
_journal_issue                   11
_journal_name_full               'Dalton Transactions'
_journal_page_first              1444
_journal_page_last               1453
_journal_paper_doi               10.1039/b710916d
_journal_year                    2008
_chemical_formula_moiety         'C26 H26 Ag2 N10, 2(N O3), H2 O'
_chemical_formula_sum            'C26 H28 Ag2 N12 O7'
_chemical_formula_weight         836.34
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 97.296(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.179(2)
_cell_length_b                   10.5389(16)
_cell_length_c                   22.155(3)
_cell_measurement_reflns_used    6585
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      27.182
_cell_measurement_theta_min      2.483
_cell_volume                     3052.2(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type
'Bruker SMART CCD area-detector diffractometer'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0249
_diffrn_reflns_av_sigmaI/netI    0.0270
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            15613
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.85
_exptl_absorpt_coefficient_mu    1.350
_exptl_absorpt_correction_T_max  0.8882
_exptl_absorpt_correction_T_min  0.6280
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.820
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1672
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.09
_refine_diff_density_max         1.468
_refine_diff_density_min         -1.564
_refine_diff_density_rms         0.074
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     430
_refine_ls_number_reflns         5371
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.015
_refine_ls_R_factor_all          0.0481
_refine_ls_R_factor_gt           0.0346
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0376P)²+5.4399P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0829
_refine_ls_wR_factor_ref         0.0921
_reflns_number_gt                4297
_reflns_number_total             5371
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b710916d.txt
_cod_data_source_block           complex_4
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7003074
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.75334(2) 0.08258(3) 0.727091(16) 0.05279(12) Uani 1 1 d . . .
Ag2 Ag 0.81840(3) 0.34492(3) 0.729006(15) 0.06376(13) Uani 1 1 d . . .
N1 N 0.7398(2) 0.2287(3) 0.82940(15) 0.0431(8) Uani 1 1 d . . .
N2 N 0.9306(2) 0.2999(3) 0.80445(14) 0.0445(8) Uani 1 1 d . . .
N3 N 1.0328(3) 0.3024(3) 0.80438(16) 0.0496(8) Uani 1 1 d . . .
H29 H 1.0622 0.3182 0.7727 0.060 Uiso 1 1 calc R . .
N4 N 0.6013(2) 0.1399(3) 0.73570(17) 0.0495(9) Uani 1 1 d . . .
N5 N 0.5150(3) 0.1219(4) 0.69646(19) 0.0583(10) Uani 1 1 d . . .
H5 H 0.5144 0.0987 0.6592 0.070 Uiso 1 1 calc R . .
N6 N 0.6099(2) 0.4512(3) 0.67769(13) 0.0367(7) Uani 1 1 d . . .
N7 N 0.7946(2) 0.3886(3) 0.63465(14) 0.0425(8) Uani 1 1 d . . .
N8 N 0.8696(2) 0.3726(3) 0.59945(15) 0.0475(8) Uani 1 1 d . . .
H8 H 0.9325 0.3594 0.6136 0.057 Uiso 1 1 calc R . .
N9 N 0.6033(2) 0.5273(3) 0.79807(14) 0.0419(7) Uani 1 1 d . . .
N10 N 0.5751(2) 0.5477(3) 0.85377(15) 0.0470(8) Uani 1 1 d . . .
H10 H 0.6169 0.5694 0.8850 0.056 Uiso 1 1 calc R . .
N11 N 0.7174(4) 0.0820(4) 0.5405(3) 0.0802(15) Uani 1 1 d . . .
N12 N 0.1315(3) 0.3889(4) 0.6702(2) 0.0619(10) Uani 1 1 d . . .
O1 O 0.7070(3) 0.0889(4) 0.5939(2) 0.0992(14) Uani 1 1 d . . .
O2 O 0.6420(4) 0.0897(5) 0.5018(2) 0.126(2) Uani 1 1 d . . .
O3 O 0.8054(4) 0.0724(4) 0.5260(2) 0.1002(14) Uani 1 1 d . . .
O4 O 0.1962(3) 0.4046(4) 0.71456(19) 0.0900(13) Uani 1 1 d . . .
O5 O 0.0487(2) 0.3403(4) 0.67866(15) 0.0692(9) Uani 1 1 d . . .
O6 O 0.1471(4) 0.4172(6) 0.6193(2) 0.129(2) Uani 1 1 d . . .
O7 O 0.5296(4) 0.9047(5) 0.4298(2) 0.1092(15) Uani 1 1 d D . .
C1 C 0.6438(3) 0.2069(4) 0.8405(2) 0.0507(10) Uani 1 1 d . . .
C2 C 0.6165(4) 0.2125(5) 0.8990(2) 0.0708(14) Uani 1 1 d . . .
H2 H 0.5493 0.1976 0.9058 0.085 Uiso 1 1 calc R . .
C3 C 0.6899(5) 0.2401(6) 0.9465(2) 0.0787(16) Uani 1 1 d . . .
H3 H 0.6733 0.2440 0.9860 0.094 Uiso 1 1 calc R . .
C4 C 0.7884(4) 0.2619(5) 0.9352(2) 0.0631(12) Uani 1 1 d . . .
H4 H 0.8391 0.2814 0.9670 0.076 Uiso 1 1 calc R . .
C5 C 0.8115(3) 0.2547(4) 0.87629(18) 0.0449(9) Uani 1 1 d . . .
C6 C 0.9156(3) 0.2721(4) 0.86131(17) 0.0430(9) Uani 1 1 d . . .
C7 C 1.0092(3) 0.2587(4) 0.89729(19) 0.0536(11) Uani 1 1 d . . .
H7 H 1.0200 0.2406 0.9387 0.064 Uiso 1 1 calc R . .
C8 C 1.0831(3) 0.2776(4) 0.8593(2) 0.0526(11) Uani 1 1 d . . .
C9 C 1.1973(4) 0.2701(6) 0.8696(3) 0.0743(15) Uani 1 1 d . . .
H9A H 1.2242 0.2884 0.8323 0.111 Uiso 1 1 calc R . .
H9B H 1.2178 0.1862 0.8831 0.111 Uiso 1 1 calc R . .
H9C H 1.2233 0.3307 0.9000 0.111 Uiso 1 1 calc R . .
C10 C 0.5689(3) 0.1747(4) 0.7882(2) 0.0503(11) Uani 1 1 d . . .
C11 C 0.4625(3) 0.1773(5) 0.7809(3) 0.0662(14) Uani 1 1 d . . .
H11 H 0.4211 0.1976 0.8105 0.079 Uiso 1 1 calc R . .
C12 C 0.4309(3) 0.1447(4) 0.7227(3) 0.0654(14) Uani 1 1 d . . .
C13 C 0.3262(4) 0.1333(6) 0.6870(3) 0.090(2) Uani 1 1 d . . .
H13A H 0.3326 0.1066 0.6463 0.135 Uiso 1 1 calc R . .
H13B H 0.2925 0.2142 0.6860 0.135 Uiso 1 1 calc R . .
H13C H 0.2868 0.0720 0.7061 0.135 Uiso 1 1 calc R . .
C14 C 0.5184(3) 0.4638(3) 0.69834(17) 0.0378(8) Uani 1 1 d . . .
C15 C 0.4262(3) 0.4473(4) 0.66124(18) 0.0458(10) Uani 1 1 d . . .
H15 H 0.3643 0.4570 0.6767 0.055 Uiso 1 1 calc R . .
C16 C 0.4282(3) 0.4164(4) 0.60112(19) 0.0506(10) Uani 1 1 d . . .
H16 H 0.3675 0.4038 0.5755 0.061 Uiso 1 1 calc R . .
C17 C 0.5203(3) 0.4045(4) 0.57931(18) 0.0468(10) Uani 1 1 d . . .
H17 H 0.5227 0.3846 0.5386 0.056 Uiso 1 1 calc R . .
C18 C 0.6102(3) 0.4223(3) 0.61867(17) 0.0374(8) Uani 1 1 d . . .
C19 C 0.7096(3) 0.4059(4) 0.59627(17) 0.0391(8) Uani 1 1 d . . .
C20 C 0.7329(3) 0.4011(4) 0.53633(18) 0.0484(10) Uani 1 1 d . . .
H20 H 0.6875 0.4106 0.5009 0.058 Uiso 1 1 calc R . .
C21 C 0.8359(3) 0.3795(4) 0.54027(19) 0.0480(10) Uani 1 1 d . . .
C22 C 0.9060(4) 0.3599(5) 0.4928(2) 0.0679(14) Uani 1 1 d . . .
H22A H 0.9745 0.3469 0.5123 0.102 Uiso 1 1 calc R . .
H22B H 0.9042 0.4334 0.4671 0.102 Uiso 1 1 calc R . .
H22C H 0.8842 0.2869 0.4687 0.102 Uiso 1 1 calc R . .
C23 C 0.5185(3) 0.4964(4) 0.76288(17) 0.0386(8) Uani 1 1 d . . .
C24 C 0.4358(3) 0.4966(4) 0.79709(19) 0.0502(10) Uani 1 1 d . . .
H24 H 0.3679 0.4777 0.7832 0.060 Uiso 1 1 calc R . .
C25 C 0.4753(3) 0.5304(4) 0.85488(19) 0.0502(10) Uani 1 1 d . . .
C26 C 0.4273(4) 0.5502(6) 0.9120(2) 0.0795(17) Uani 1 1 d . . .
H26A H 0.4790 0.5740 0.9445 0.119 Uiso 1 1 calc R . .
H26B H 0.3951 0.4730 0.9225 0.119 Uiso 1 1 calc R . .
H26C H 0.3769 0.6163 0.9056 0.119 Uiso 1 1 calc R . .
H28 H 0.4697(19) 0.913(5) 0.441(2) 0.080 Uiso 1 1 d D . .
H27 H 0.565(3) 0.963(4) 0.449(2) 0.080 Uiso 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N9 Ag1 N4 169.97(13) 2_646 . ?
N9 Ag1 Ag2 101.02(9) 2_646 2_646 ?
N4 Ag1 Ag2 82.16(10) . 2_646 ?
N9 Ag1 Ag2 89.66(9) 2_646 . ?
N4 Ag1 Ag2 90.47(9) . . ?
Ag2 Ag1 Ag2 158.828(15) 2_646 . ?
N7 Ag2 N2 144.87(12) . . ?
N7 Ag2 Ag1 97.45(9) . 2_656 ?
N2 Ag2 Ag1 98.78(9) . 2_656 ?
N7 Ag2 Ag1 100.73(9) . . ?
N2 Ag2 Ag1 88.48(9) . . ?
Ag1 Ag2 Ag1 136.413(18) 2_656 . ?
C1 N1 C5 118.8(3) . . ?
C6 N2 N3 105.9(3) . . ?
C6 N2 Ag2 128.1(3) . . ?
N3 N2 Ag2 125.9(2) . . ?
C8 N3 N2 112.1(3) . . ?
C8 N3 H29 124.0 . . ?
N2 N3 H29 124.0 . . ?
C10 N4 N5 105.2(3) . . ?
C10 N4 Ag1 124.3(3) . . ?
N5 N4 Ag1 128.8(3) . . ?
C12 N5 N4 111.7(4) . . ?
C12 N5 H5 124.1 . . ?
N4 N5 H5 124.1 . . ?
C18 N6 C14 117.8(3) . . ?
C19 N7 N8 105.5(3) . . ?
C19 N7 Ag2 131.7(3) . . ?
N8 N7 Ag2 121.0(2) . . ?
C21 N8 N7 112.7(3) . . ?
C21 N8 H8 123.7 . . ?
N7 N8 H8 123.7 . . ?
C23 N9 N10 105.6(3) . . ?
C23 N9 Ag1 129.0(3) . 2_656 ?
N10 N9 Ag1 123.7(2) . 2_656 ?
C25 N10 N9 112.5(3) . . ?
C25 N10 H10 123.8 . . ?
N9 N10 H10 123.8 . . ?
O1 N11 O2 119.8(7) . . ?
O1 N11 O3 118.8(5) . . ?
O2 N11 O3 121.4(6) . . ?
O6 N12 O4 122.1(5) . . ?
O6 N12 O5 120.0(5) . . ?
O4 N12 O5 117.9(4) . . ?
H28 O7 H28 0(6) . . ?
H28 O7 H27 105(3) . . ?
H28 O7 H27 105(3) . . ?
N1 C1 C2 121.7(4) . . ?
N1 C1 C10 116.9(4) . . ?
C2 C1 C10 121.4(4) . . ?
C3 C2 C1 119.0(5) . . ?
C3 C2 H2 120.5 . . ?
C1 C2 H2 120.5 . . ?
C2 C3 C4 119.3(5) . . ?
C2 C3 H3 120.3 . . ?
C4 C3 H3 120.3 . . ?
C3 C4 C5 119.4(5) . . ?
C3 C4 H4 120.3 . . ?
C5 C4 H4 120.3 . . ?
N1 C5 C4 121.7(4) . . ?
N1 C5 C6 116.0(3) . . ?
C4 C5 C6 122.3(4) . . ?
N2 C6 C7 109.7(4) . . ?
N2 C6 C5 119.9(3) . . ?
C7 C6 C5 130.3(4) . . ?
C8 C7 C6 106.3(4) . . ?
C8 C7 H7 126.9 . . ?
C6 C7 H7 126.9 . . ?
N3 C8 C7 106.1(4) . . ?
N3 C8 C9 121.5(4) . . ?
C7 C8 C9 132.4(4) . . ?
C8 C9 H9A 109.5 . . ?
C8 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C8 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
N4 C10 C11 109.4(4) . . ?
N4 C10 C1 119.6(3) . . ?
C11 C10 C1 131.0(4) . . ?
C12 C11 C10 106.9(4) . . ?
C12 C11 H11 126.6 . . ?
C10 C11 H11 126.6 . . ?
N5 C12 C11 106.8(4) . . ?
N5 C12 C13 120.9(6) . . ?
C11 C12 C13 132.3(5) . . ?
C12 C13 H13A 109.5 . . ?
C12 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C12 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
N6 C14 C15 122.6(4) . . ?
N6 C14 C23 117.5(3) . . ?
C15 C14 C23 119.9(3) . . ?
C16 C15 C14 118.7(4) . . ?
C16 C15 H15 120.7 . . ?
C14 C15 H15 120.7 . . ?
C17 C16 C15 119.4(4) . . ?
C17 C16 H16 120.3 . . ?
C15 C16 H16 120.3 . . ?
C16 C17 C18 119.3(4) . . ?
C16 C17 H17 120.4 . . ?
C18 C17 H17 120.4 . . ?
N6 C18 C17 122.2(4) . . ?
N6 C18 C19 118.0(3) . . ?
C17 C18 C19 119.8(3) . . ?
N7 C19 C20 109.4(3) . . ?
N7 C19 C18 121.0(3) . . ?
C20 C19 C18 129.6(3) . . ?
C21 C20 C19 106.3(4) . . ?
C21 C20 H20 126.8 . . ?
C19 C20 H20 126.8 . . ?
N8 C21 C20 106.1(4) . . ?
N8 C21 C22 121.6(4) . . ?
C20 C21 C22 132.3(4) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
N9 C23 C24 109.7(3) . . ?
N9 C23 C14 121.9(3) . . ?
C24 C23 C14 128.3(3) . . ?
C25 C24 C23 106.0(3) . . ?
C25 C24 H24 127.0 . . ?
C23 C24 H24 127.0 . . ?
N10 C25 C24 106.2(4) . . ?
N10 C25 C26 121.4(4) . . ?
C24 C25 C26 132.5(4) . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N9 2.118(3) 2_646 ?
Ag1 N4 2.125(3) . ?
Ag1 Ag2 2.8891(6) 2_646 ?
Ag1 Ag2 2.8933(6) . ?
Ag2 N7 2.125(3) . ?
Ag2 N2 2.139(3) . ?
Ag2 Ag1 2.8891(6) 2_656 ?
N1 C1 1.340(5) . ?
N1 C5 1.341(5) . ?
N2 C6 1.332(5) . ?
N2 N3 1.347(4) . ?
N3 C8 1.336(5) . ?
N3 H29 0.8600 . ?
N4 C10 1.340(5) . ?
N4 N5 1.354(5) . ?
N5 C12 1.337(6) . ?
N5 H5 0.8600 . ?
N6 C18 1.343(5) . ?
N6 C14 1.349(5) . ?
N7 C19 1.330(5) . ?
N7 N8 1.345(4) . ?
N8 C21 1.332(5) . ?
N8 H8 0.8600 . ?
N9 C23 1.320(5) . ?
N9 N10 1.350(4) . ?
N9 Ag1 2.118(3) 2_656 ?
N10 C25 1.331(5) . ?
N10 H10 0.8600 . ?
N11 O1 1.209(6) . ?
N11 O2 1.231(6) . ?
N11 O3 1.247(7) . ?
N12 O6 1.209(5) . ?
N12 O4 1.228(5) . ?
N12 O5 1.242(5) . ?
O7 H28 0.861(19) . ?
O7 H28 0.861(19) . ?
O7 H27 0.852(19) . ?
C1 C2 1.391(6) . ?
C1 C10 1.462(6) . ?
C2 C3 1.366(8) . ?
C2 H2 0.9300 . ?
C3 C4 1.372(7) . ?
C3 H3 0.9300 . ?
C4 C5 1.380(6) . ?
C4 H4 0.9300 . ?
C5 C6 1.463(6) . ?
C6 C7 1.389(6) . ?
C7 C8 1.379(6) . ?
C7 H7 0.9300 . ?
C8 C9 1.496(6) . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C10 C11 1.392(6) . ?
C11 C12 1.349(7) . ?
C11 H11 0.9300 . ?
C12 C13 1.504(7) . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C14 C15 1.388(5) . ?
C14 C23 1.470(5) . ?
C15 C16 1.375(6) . ?
C15 H15 0.9300 . ?
C16 C17 1.367(6) . ?
C16 H16 0.9300 . ?
C17 C18 1.392(5) . ?
C17 H17 0.9300 . ?
C18 C19 1.468(5) . ?
C19 C20 1.402(6) . ?
C20 C21 1.367(6) . ?
C20 H20 0.9300 . ?
C21 C22 1.499(6) . ?
C22 H22A 0.9600 . ?
C22 H22B 0.9600 . ?
C22 H22C 0.9600 . ?
C23 C24 1.405(5) . ?
C24 C25 1.366(6) . ?
C24 H24 0.9300 . ?
C25 C26 1.500(6) . ?
C26 H26A 0.9600 . ?
C26 H26B 0.9600 . ?
C26 H26C 0.9600 . ?
