#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:14:32 +0100 (vie 25 de mar de 2016) $
#$Revision: 179805 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/01/7010115.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7010115
loop_
_publ_author_name
'Charmant, Jonathan P. H.'
'Crawford, Paul'
'King, Philip J.'
'Quesada-Pato, Roberto'
'Sappa, Enrico'
_publ_section_title
;
 Acid promoted formation of tri- and penta-ruthenium allenylidene
 complexes
;
_journal_issue                   23
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              4390
_journal_paper_doi               10.1039/b006146h
_journal_year                    2000
_chemical_formula_sum            'C30 H10 O15 Ru5'
_chemical_formula_weight         1115.73
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.72(5)
_cell_angle_beta                 104.12(6)
_cell_angle_gamma                110.94(4)
_cell_formula_units_Z            2
_cell_length_a                   9.820(5)
_cell_length_b                   12.992(5)
_cell_length_c                   14.957(5)
_cell_measurement_reflns_used    128
_cell_measurement_temperature    173(2)
_cell_volume                     1667.2(15)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'frames, each covering 0.3 deg in ω'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0343
_diffrn_reflns_av_sigmaI/netI    0.0568
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            17369
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         1.46
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    2.284
_exptl_absorpt_correction_T_max  0.746
_exptl_absorpt_correction_T_min  0.565
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
 G. M. Sheldrick. 
 SADABS: A program for absorption correction with the Siemens SMART system; 
 University of Göttingen: Germany, 1996.
;
_exptl_crystal_colour            'dark red'
_exptl_crystal_density_diffrn    2.223
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1060
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.30
_refine_diff_density_max         1.015
_refine_diff_density_min         -1.433
_refine_diff_density_rms         0.130
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.882
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         7545
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.882
_refine_ls_R_factor_all          0.0368
_refine_ls_R_factor_gt           0.0288
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0276P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0636
_refine_ls_wR_factor_ref         0.0647
_reflns_number_gt                5893
_reflns_number_total             7545
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b006146h.txt
_cod_data_source_block           12
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1667.2(12)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7010115
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.22609(3) 0.24105(2) 0.65463(2) 0.02068(8) Uani 1 1 d . . .
Ru2 Ru 0.39330(3) 0.21855(2) 0.83078(2) 0.02065(8) Uani 1 1 d . . .
Ru3 Ru 0.45510(3) 0.15750(2) 0.66077(2) 0.02046(8) Uani 1 1 d . . .
Ru4 Ru 0.69371(3) 0.30534(2) 0.82510(2) 0.02125(8) Uani 1 1 d . . .
Ru5 Ru 0.54551(4) 0.07427(3) 0.81984(2) 0.02493(8) Uani 1 1 d . . .
C1 C 0.1525(4) 0.2492(3) 0.5274(3) 0.0294(9) Uani 1 1 d . . .
C2 C 0.1158(4) 0.3223(3) 0.6916(3) 0.0328(10) Uani 1 1 d . . .
C3 C 0.0588(4) 0.0892(3) 0.6269(3) 0.0276(9) Uani 1 1 d . . .
C4 C 0.2033(5) 0.1030(3) 0.8292(3) 0.0305(9) Uani 1 1 d . . .
C5 C 0.3471(4) 0.3434(4) 0.8795(3) 0.0308(9) Uani 1 1 d . . .
C6 C 0.4968(5) 0.2150(4) 0.9570(3) 0.0350(10) Uani 1 1 d . . .
C7 C 0.3562(5) -0.0537(4) 0.7945(3) 0.0335(10) Uani 1 1 d . . .
C8 C 0.6438(5) 0.0581(4) 0.9391(3) 0.0342(10) Uani 1 1 d . . .
C9 C 0.6322(5) -0.0150(4) 0.7629(3) 0.0410(11) Uani 1 1 d . . .
C10 C 0.8354(5) 0.2339(3) 0.8352(3) 0.0310(10) Uani 1 1 d . . .
C11 C 0.7898(4) 0.3906(3) 0.9552(3) 0.0299(9) Uani 1 1 d . . .
C12 C 0.8129(4) 0.4346(3) 0.7869(3) 0.0256(9) Uani 1 1 d . . .
C13 C 0.3034(5) 0.0021(3) 0.6025(3) 0.0307(9) Uani 1 1 d . . .
C14 C 0.4282(5) 0.2059(3) 0.5447(3) 0.0299(9) Uani 1 1 d . . .
C15 C 0.6243(5) 0.1318(4) 0.6396(3) 0.0350(10) Uani 1 1 d . . .
C16 C 0.4945(4) 0.3195(3) 0.7467(3) 0.0207(8) Uani 1 1 d . . .
C17 C 0.4351(4) 0.3909(3) 0.7055(2) 0.0200(8) Uani 1 1 d . . .
C18 C 0.4754(4) 0.5023(3) 0.7049(3) 0.0228(8) Uani 1 1 d . . .
C19 C 0.6265(4) 0.5942(3) 0.7685(3) 0.0264(9) Uani 1 1 d . . .
C24 C 0.6811(4) 0.6020(3) 0.8656(3) 0.0325(10) Uani 1 1 d . . .
H24 H 0.6232 0.5470 0.8924 0.039 Uiso 1 1 calc R . .
C23 C 0.8203(5) 0.6904(4) 0.9233(3) 0.0463(13) Uani 1 1 d . . .
H23 H 0.8570 0.6963 0.9896 0.056 Uiso 1 1 calc R . .
C22 C 0.9053(5) 0.7698(4) 0.8842(4) 0.0551(15) Uani 1 1 d . . .
H22 H 1.0011 0.8295 0.9235 0.066 Uiso 1 1 calc R . .
C21 C 0.8517(5) 0.7627(4) 0.7888(4) 0.0506(14) Uani 1 1 d . . .
H21 H 0.9110 0.8174 0.7623 0.061 Uiso 1 1 calc R . .
C20 C 0.7118(5) 0.6763(3) 0.7306(3) 0.0348(10) Uani 1 1 d . . .
H20 H 0.6741 0.6732 0.6649 0.042 Uiso 1 1 calc R . .
C25 C 0.3722(4) 0.5400(3) 0.6410(3) 0.0275(9) Uani 1 1 d . . .
C26 C 0.3351(5) 0.5049(3) 0.5426(3) 0.0348(10) Uani 1 1 d . . .
H26 H 0.3760 0.4561 0.5162 0.042 Uiso 1 1 calc R . .
C27 C 0.2393(6) 0.5397(4) 0.4821(4) 0.0522(14) Uani 1 1 d . . .
H27 H 0.2135 0.5137 0.4149 0.063 Uiso 1 1 calc R . .
C28 C 0.1822(6) 0.6110(4) 0.5191(4) 0.0665(19) Uani 1 1 d . . .
H28 H 0.1178 0.6357 0.4776 0.080 Uiso 1 1 calc R . .
C29 C 0.2169(6) 0.6471(4) 0.6152(4) 0.0656(18) Uani 1 1 d . . .
H29 H 0.1748 0.6957 0.6405 0.079 Uiso 1 1 calc R . .
C30 C 0.3133(5) 0.6137(4) 0.6765(4) 0.0474(13) Uani 1 1 d . . .
H30 H 0.3394 0.6415 0.7436 0.057 Uiso 1 1 calc R . .
O1 O 0.1045(3) 0.2506(2) 0.4505(2) 0.0411(8) Uani 1 1 d . . .
O2 O 0.0514(4) 0.3738(3) 0.7146(3) 0.0520(9) Uani 1 1 d . . .
O3 O -0.0433(3) 0.0038(2) 0.6077(2) 0.0405(8) Uani 1 1 d . . .
O4 O 0.0922(3) 0.0392(2) 0.8316(2) 0.0437(8) Uani 1 1 d . . .
O5 O 0.3298(4) 0.4209(3) 0.9120(2) 0.0449(8) Uani 1 1 d . . .
O6 O 0.5447(4) 0.2238(3) 1.0366(2) 0.0455(8) Uani 1 1 d . . .
O7 O 0.2454(4) -0.1319(3) 0.7811(2) 0.0514(9) Uani 1 1 d . . .
O8 O 0.7006(4) 0.0445(3) 1.0101(2) 0.0543(10) Uani 1 1 d . . .
O9 O 0.6812(5) -0.0706(3) 0.7285(3) 0.0675(11) Uani 1 1 d . . .
O10 O 0.9355(3) 0.2082(3) 0.8414(2) 0.0423(8) Uani 1 1 d . . .
O11 O 0.8485(3) 0.4439(3) 1.0319(2) 0.0488(9) Uani 1 1 d . . .
O12 O 0.8904(3) 0.5074(2) 0.7650(2) 0.0361(7) Uani 1 1 d . . .
O13 O 0.2137(3) -0.0888(2) 0.5680(2) 0.0410(8) Uani 1 1 d . . .
O14 O 0.4214(4) 0.2302(3) 0.4740(2) 0.0452(8) Uani 1 1 d . . .
O15 O 0.7209(4) 0.1186(3) 0.6163(2) 0.0553(10) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 Ru1 C1 89.24(19) . . ?
C2 Ru1 C3 95.14(17) . . ?
C1 Ru1 C3 91.22(18) . . ?
C2 Ru1 C17 91.85(16) . . ?
C1 Ru1 C17 99.46(16) . . ?
C3 Ru1 C17 167.31(15) . . ?
C2 Ru1 C16 115.14(16) . . ?
C1 Ru1 C16 123.54(16) . . ?
C3 Ru1 C16 132.02(15) . . ?
C17 Ru1 C16 35.44(13) . . ?
C2 Ru1 Ru3 161.22(13) . . ?
C1 Ru1 Ru3 106.72(14) . . ?
C3 Ru1 Ru3 94.36(12) . . ?
C17 Ru1 Ru3 76.09(11) . . ?
C16 Ru1 Ru3 47.69(9) . . ?
C2 Ru1 Ru2 103.84(14) . . ?
C1 Ru1 Ru2 166.05(13) . . ?
C3 Ru1 Ru2 92.40(14) . . ?
C17 Ru1 Ru2 75.63(12) . . ?
C16 Ru1 Ru2 46.32(10) . . ?
Ru3 Ru1 Ru2 59.57(4) . . ?
C5 Ru2 C4 94.12(18) . . ?
C5 Ru2 C6 92.90(19) . . ?
C4 Ru2 C6 90.94(19) . . ?
C5 Ru2 C16 86.55(16) . . ?
C4 Ru2 C16 142.71(16) . . ?
C6 Ru2 C16 126.30(16) . . ?
C5 Ru2 Ru4 108.93(13) . . ?
C4 Ru2 Ru4 156.08(12) . . ?
C6 Ru2 Ru4 81.82(14) . . ?
C16 Ru2 Ru4 48.60(10) . . ?
C5 Ru2 Ru5 159.93(12) . . ?
C4 Ru2 Ru5 95.65(13) . . ?
C6 Ru2 Ru5 69.47(14) . . ?
C16 Ru2 Ru5 96.11(11) . . ?
Ru4 Ru2 Ru5 60.46(4) . . ?
C5 Ru2 Ru3 131.23(13) . . ?
C4 Ru2 Ru3 109.62(14) . . ?
C6 Ru2 Ru3 127.19(14) . . ?
C16 Ru2 Ru3 48.94(10) . . ?
Ru4 Ru2 Ru3 59.62(7) . . ?
Ru5 Ru2 Ru3 60.74(4) . . ?
C5 Ru2 Ru1 80.44(13) . . ?
C4 Ru2 Ru1 88.00(14) . . ?
C6 Ru2 Ru1 173.16(14) . . ?
C16 Ru2 Ru1 55.29(10) . . ?
Ru4 Ru2 Ru1 101.74(6) . . ?
Ru5 Ru2 Ru1 117.36(4) . . ?
Ru3 Ru2 Ru1 59.38(3) . . ?
C15 Ru3 C14 88.07(19) . . ?
C15 Ru3 C13 96.41(19) . . ?
C14 Ru3 C13 95.45(18) . . ?
C15 Ru3 C16 119.43(17) . . ?
C14 Ru3 C16 93.09(16) . . ?
C13 Ru3 C16 143.40(16) . . ?
C15 Ru3 Ru4 78.94(13) . . ?
C14 Ru3 Ru4 119.02(12) . . ?
C13 Ru3 Ru4 144.77(13) . . ?
C16 Ru3 Ru4 48.47(10) . . ?
C15 Ru3 Ru1 161.93(14) . . ?
C14 Ru3 Ru1 75.24(13) . . ?
C13 Ru3 Ru1 92.11(13) . . ?
C16 Ru3 Ru1 56.01(11) . . ?
Ru4 Ru3 Ru1 102.91(5) . . ?
C15 Ru3 Ru2 131.39(13) . . ?
C14 Ru3 Ru2 132.57(13) . . ?
C13 Ru3 Ru2 103.26(14) . . ?
C16 Ru3 Ru2 48.06(11) . . ?
Ru4 Ru3 Ru2 59.57(4) . . ?
Ru1 Ru3 Ru2 61.06(5) . . ?
C15 Ru3 Ru5 79.27(14) . . ?
C14 Ru3 Ru5 167.28(13) . . ?
C13 Ru3 Ru5 84.88(14) . . ?
C16 Ru3 Ru5 94.17(11) . . ?
Ru4 Ru3 Ru5 59.90(4) . . ?
Ru1 Ru3 Ru5 117.47(4) . . ?
Ru2 Ru3 Ru5 59.18(3) . . ?
C11 Ru4 C10 91.69(18) . . ?
C11 Ru4 C12 90.00(18) . . ?
C10 Ru4 C12 96.67(17) . . ?
C11 Ru4 C16 117.84(17) . . ?
C10 Ru4 C16 150.20(16) . . ?
C12 Ru4 C16 87.73(15) . . ?
C11 Ru4 Ru2 96.72(14) . . ?
C10 Ru4 Ru2 128.76(13) . . ?
C12 Ru4 Ru2 133.59(12) . . ?
C16 Ru4 Ru2 48.80(11) . . ?
C11 Ru4 Ru3 157.48(12) . . ?
C10 Ru4 Ru3 101.33(13) . . ?
C12 Ru4 Ru3 106.41(12) . . ?
C16 Ru4 Ru3 49.57(10) . . ?
Ru2 Ru4 Ru3 60.81(5) . . ?
C11 Ru4 Ru5 108.08(14) . . ?
C10 Ru4 Ru5 69.39(13) . . ?
C12 Ru4 Ru5 156.98(12) . . ?
C16 Ru4 Ru5 95.82(11) . . ?
Ru2 Ru4 Ru5 59.93(4) . . ?
Ru3 Ru4 Ru5 60.96(5) . . ?
C9 Ru5 C8 88.0(2) . . ?
C9 Ru5 C7 92.9(2) . . ?
C8 Ru5 C7 95.57(19) . . ?
C9 Ru5 Ru2 157.02(15) . . ?
C8 Ru5 Ru2 114.52(15) . . ?
C7 Ru5 Ru2 89.56(14) . . ?
C9 Ru5 Ru4 111.40(15) . . ?
C8 Ru5 Ru4 106.11(14) . . ?
C7 Ru5 Ru4 147.49(13) . . ?
Ru2 Ru5 Ru4 59.62(4) . . ?
C9 Ru5 Ru3 96.96(15) . . ?
C8 Ru5 Ru3 165.24(13) . . ?
C7 Ru5 Ru3 98.04(15) . . ?
Ru2 Ru5 Ru3 60.08(4) . . ?
Ru4 Ru5 Ru3 59.14(6) . . ?
O1 C1 Ru1 177.7(3) . . ?
O2 C2 Ru1 178.5(4) . . ?
O3 C3 Ru1 176.0(4) . . ?
O4 C4 Ru2 176.8(4) . . ?
O5 C5 Ru2 175.4(4) . . ?
O6 C6 Ru2 167.9(4) . . ?
O7 C7 Ru5 177.9(4) . . ?
O8 C8 Ru5 177.7(4) . . ?
O9 C9 Ru5 178.4(4) . . ?
O10 C10 Ru4 169.1(4) . . ?
O11 C11 Ru4 178.2(4) . . ?
O12 C12 Ru4 175.2(3) . . ?
O13 C13 Ru3 179.6(4) . . ?
O14 C14 Ru3 173.5(4) . . ?
O15 C15 Ru3 171.8(4) . . ?
C17 C16 Ru4 145.8(3) . . ?
C17 C16 Ru2 123.3(3) . . ?
Ru4 C16 Ru2 82.60(14) . . ?
C17 C16 Ru3 120.0(2) . . ?
Ru4 C16 Ru3 81.96(15) . . ?
Ru2 C16 Ru3 83.00(13) . . ?
C17 C16 Ru1 61.44(19) . . ?
Ru4 C16 Ru1 152.59(18) . . ?
Ru2 C16 Ru1 78.39(12) . . ?
Ru3 C16 Ru1 76.30(12) . . ?
C18 C17 C16 141.1(3) . . ?
C18 C17 Ru1 135.3(3) . . ?
C16 C17 Ru1 83.1(2) . . ?
C17 C18 C25 122.1(3) . . ?
C17 C18 C19 121.9(3) . . ?
C25 C18 C19 116.0(3) . . ?
C20 C19 C24 119.3(4) . . ?
C20 C19 C18 119.2(4) . . ?
C24 C19 C18 121.5(4) . . ?
C23 C24 C19 120.0(4) . . ?
C22 C23 C24 120.0(5) . . ?
C21 C22 C23 120.2(4) . . ?
C22 C21 C20 120.6(4) . . ?
C21 C20 C19 119.9(4) . . ?
C30 C25 C26 117.5(4) . . ?
C30 C25 C18 122.0(4) . . ?
C26 C25 C18 120.5(4) . . ?
C27 C26 C25 121.1(5) . . ?
C28 C27 C26 120.0(5) . . ?
C27 C28 C29 120.2(5) . . ?
C28 C29 C30 120.4(5) . . ?
C29 C30 C25 120.8(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 C2 1.877(5) . ?
Ru1 C1 1.897(4) . ?
Ru1 C3 1.966(4) . ?
Ru1 C17 2.124(4) . ?
Ru1 C16 2.401(4) . ?
Ru1 Ru3 2.8139(13) . ?
Ru1 Ru2 2.8615(18) . ?
Ru2 C5 1.923(5) . ?
Ru2 C4 1.924(4) . ?
Ru2 C6 1.929(5) . ?
Ru2 C16 2.113(4) . ?
Ru2 Ru4 2.7847(16) . ?
Ru2 Ru5 2.7934(12) . ?
Ru2 Ru3 2.8194(12) . ?
Ru3 C15 1.895(5) . ?
Ru3 C14 1.925(5) . ?
Ru3 C13 1.933(4) . ?
Ru3 C16 2.142(4) . ?
Ru3 Ru4 2.786(3) . ?
Ru3 Ru5 2.8379(14) . ?
Ru4 C11 1.899(4) . ?
Ru4 C10 1.919(4) . ?
Ru4 C12 1.931(4) . ?
Ru4 C16 2.106(4) . ?
Ru4 Ru5 2.8082(15) . ?
Ru5 C9 1.885(5) . ?
Ru5 C8 1.892(5) . ?
Ru5 C7 1.903(5) . ?
C1 O1 1.137(5) . ?
C2 O2 1.143(5) . ?
C3 O3 1.134(4) . ?
C4 O4 1.122(5) . ?
C5 O5 1.137(5) . ?
C6 O6 1.140(5) . ?
C7 O7 1.139(5) . ?
C8 O8 1.143(5) . ?
C9 O9 1.129(5) . ?
C10 O10 1.134(5) . ?
C11 O11 1.131(5) . ?
C12 O12 1.133(4) . ?
C13 O13 1.135(4) . ?
C14 O14 1.142(5) . ?
C15 O15 1.145(5) . ?
C16 C17 1.403(5) . ?
C17 C18 1.360(5) . ?
C18 C25 1.485(5) . ?
C18 C19 1.494(5) . ?
C19 C20 1.392(5) . ?
C19 C24 1.394(6) . ?
C24 C23 1.391(6) . ?
C23 C22 1.381(7) . ?
C22 C21 1.371(7) . ?
C21 C20 1.387(6) . ?
C25 C30 1.386(6) . ?
C25 C26 1.387(6) . ?
C26 C27 1.386(6) . ?
C27 C28 1.358(8) . ?
C28 C29 1.358(8) . ?
C29 C30 1.384(6) . ?
