#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:21:42 +0100 (vie 25 de mar de 2016) $
#$Revision: 179812 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/08/7010835.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7010835
loop_
_publ_author_name
'Fletcher, Nicholas C.'
'Nieuwenhuyzen, Mark'
'Rainey, Sharon'
_publ_section_title
;
 The isolation and purification of tris-2,2'-bipyridine complexes of
 ruthenium(ii) containing unsymmetrical ligands
;
_journal_issue                   18
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2641
_journal_paper_doi               10.1039/b104365j
_journal_year                    2001
_chemical_formula_sum            'C33 H30 F12 N6 P2 Ru'
_chemical_formula_weight         901.64
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 105.815(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   10.5990(15)
_cell_length_b                   13.5789(18)
_cell_length_c                   13.3087(18)
_cell_measurement_temperature    153(2)
_cell_volume                     1842.9(4)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      153(2)
_diffrn_measured_fraction_theta_full 0.908
_diffrn_measured_fraction_theta_max 0.908
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0531
_diffrn_reflns_av_sigmaI/netI    0.0704
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            14232
_diffrn_reflns_theta_full        28.48
_diffrn_reflns_theta_max         28.48
_diffrn_reflns_theta_min         1.59
_exptl_absorpt_coefficient_mu    0.607
_exptl_absorpt_correction_T_max  0.8484
_exptl_absorpt_correction_T_min  0.7593
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.625
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             904
_exptl_crystal_size_max          0.48
_exptl_crystal_size_mid          0.37
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.993
_refine_diff_density_min         -0.628
_refine_diff_density_rms         0.100
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.03(4)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     501
_refine_ls_number_reflns         8088
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.023
_refine_ls_R_factor_all          0.0643
_refine_ls_R_factor_gt           0.0509
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0801P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1249
_refine_ls_wR_factor_ref         0.1328
_reflns_number_gt                6728
_reflns_number_total             8088
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b104365j.txt
_cod_data_source_block           ncf79m
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)
_cod_database_code               7010835
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.10199(3) 0.85010(3) 0.22925(2) 0.02853(10) Uani 1 1 d . . .
N1A N -0.0021(4) 0.8329(4) 0.0756(3) 0.0361(12) Uani 1 1 d . E .
C2A C 0.0339(6) 0.7793(4) 0.0029(4) 0.0405(12) Uani 1 1 d . . .
H2A H 0.1120 0.7414 0.0242 0.049 Uiso 1 1 calc R A 1
C4A C -0.1528(6) 0.8295(5) -0.1297(5) 0.060(2) Uani 1 1 d . . .
H4A H -0.2040 0.8293 -0.2004 0.072 Uiso 1 1 calc R B 1
C5A C -0.1935(6) 0.8817(4) -0.0577(5) 0.0499(16) Uani 1 1 d . E .
H5A H -0.2742 0.9165 -0.0778 0.060 Uiso 1 1 calc R . .
C6A C -0.1181(5) 0.8846(4) 0.0453(5) 0.0406(13) Uani 1 1 d . . .
C7A C -0.1512(5) 0.9402(4) 0.1290(5) 0.0434(13) Uani 1 1 d . E .
C8A C -0.2609(6) 0.9999(5) 0.1150(6) 0.0573(17) Uani 1 1 d . . .
H8A H -0.3200 1.0076 0.0476 0.069 Uiso 1 1 calc R E .
C9A C -0.2834(7) 1.0483(6) 0.2000(8) 0.073(2) Uani 1 1 d . E .
H9A H -0.3600 1.0874 0.1910 0.088 Uiso 1 1 calc R C 1
C11A C -0.0883(7) 0.9812(6) 0.3048(7) 0.0493(17) Uani 1 1 d . . .
H11A H -0.0269 0.9756 0.3715 0.059 Uiso 1 1 calc R D 1
N12A N -0.0639(4) 0.9314(3) 0.2248(4) 0.0380(10) Uani 1 1 d . E .
C13A C -0.2230(15) 1.0916(9) 0.3813(11) 0.080(4) Uani 0.636(11) 1 d P E 2
H13A H -0.2450 1.1603 0.3615 0.120 Uiso 0.636(11) 1 calc PR E 2
H13B H -0.1449 1.0894 0.4412 0.120 Uiso 0.636(11) 1 calc PR E 2
H13C H -0.2967 1.0604 0.4003 0.120 Uiso 0.636(11) 1 calc PR E 2
C3A C -0.0364(7) 0.7764(5) -0.1007(5) 0.0518(18) Uani 0.636(11) 1 d P E 2
H3A H -0.0065 0.7396 -0.1503 0.062 Uiso 0.636(11) 1 calc PR E 2
C10A C -0.1975(8) 1.0404(5) 0.2959(7) 0.067(2) Uani 0.636(11) 1 d P E 2
C3' C -0.0364(7) 0.7764(5) -0.1007(5) 0.0518(18) Uani 0.36 1 d P E 1
C13' C 0.0011(13) 0.7177(11) -0.1758(10) 0.035(4) Uani 0.364(11) 1 d P E 1
H13D' H 0.0966 0.7201 -0.1630 0.053 Uiso 0.364(11) 1 calc PR E 1
H13E' H -0.0409 0.7430 -0.2460 0.053 Uiso 0.364(11) 1 calc PR E 1
H13F' H -0.0264 0.6495 -0.1704 0.053 Uiso 0.364(11) 1 calc PR E 1
C10' C -0.1975(8) 1.0404(5) 0.2959(7) 0.067(2) Uani 0.36 1 d P E 1
H10' H -0.2115 1.0740 0.3545 0.081 Uiso 0.364(11) 1 calc PR E 1
N1B N 0.2027(4) 0.8873(3) 0.3787(3) 0.0332(9) Uani 1 1 d . . .
C2B C 0.2003(6) 0.8384(6) 0.4653(4) 0.0457(14) Uani 1 1 d . . .
H2B H 0.1476 0.7809 0.4588 0.055 Uiso 1 1 calc R . .
C3B C 0.2718(7) 0.8682(6) 0.5646(4) 0.062(2) Uani 1 1 d . . .
H3B H 0.2670 0.8323 0.6247 0.074 Uiso 1 1 calc R . .
C4B C 0.3489(8) 0.9499(5) 0.5737(5) 0.0609(18) Uani 1 1 d . . .
H4B H 0.3989 0.9718 0.6405 0.073 Uiso 1 1 calc R . .
C5B C 0.3534(6) 1.0011(5) 0.4838(5) 0.0538(15) Uani 1 1 d . . .
H5B H 0.4070 1.0580 0.4890 0.065 Uiso 1 1 calc R . .
C6B C 0.2809(5) 0.9693(4) 0.3888(4) 0.0371(11) Uani 1 1 d . . .
C7B C 0.2783(5) 1.0164(4) 0.2889(4) 0.0331(11) Uani 1 1 d . . .
C8B C 0.3552(6) 1.0974(5) 0.2808(5) 0.0437(16) Uani 1 1 d . . .
H8B H 0.4090 1.1280 0.3418 0.052 Uiso 1 1 calc R . .
C9B C 0.3523(6) 1.1328(4) 0.1828(6) 0.0480(15) Uani 1 1 d . . .
H9B H 0.4078 1.1861 0.1765 0.058 Uiso 1 1 calc R . .
C10B C 0.2696(6) 1.0919(4) 0.0935(5) 0.0409(13) Uani 1 1 d . . .
C11B C 0.1923(5) 1.0127(4) 0.1082(4) 0.0364(11) Uani 1 1 d . . .
H11B H 0.1342 0.9834 0.0485 0.044 Uiso 1 1 calc R . .
N12B N 0.1963(4) 0.9762(3) 0.2032(3) 0.0299(9) Uani 1 1 d . . .
C13B C 0.2626(7) 1.1280(5) -0.0138(5) 0.0541(16) Uani 1 1 d . . .
H13D H 0.3031 1.1933 -0.0094 0.081 Uiso 1 1 calc R . .
H13E H 0.1707 1.1322 -0.0547 0.081 Uiso 1 1 calc R . .
H13F H 0.3095 1.0821 -0.0477 0.081 Uiso 1 1 calc R . .
N1C N 0.0360(4) 0.7161(3) 0.2701(3) 0.0365(10) Uani 1 1 d . . .
C2C C -0.0728(7) 0.7018(5) 0.3010(6) 0.0441(16) Uani 1 1 d . . .
H2C H -0.1266 0.7569 0.3048 0.053 Uiso 1 1 calc R . .
C3C C -0.1097(7) 0.6098(5) 0.3275(6) 0.0529(16) Uani 1 1 d . . .
H3C H -0.1888 0.6018 0.3471 0.063 Uiso 1 1 calc R . .
C4C C -0.0313(7) 0.5307(5) 0.3251(6) 0.0586(17) Uani 1 1 d . . .
H4C H -0.0554 0.4668 0.3424 0.070 Uiso 1 1 calc R . .
C5C C 0.0844(7) 0.5450(4) 0.2969(6) 0.0553(16) Uani 1 1 d . . .
H5C H 0.1412 0.4911 0.2962 0.066 Uiso 1 1 calc R . .
C6C C 0.1161(5) 0.6380(4) 0.2699(4) 0.0394(12) Uani 1 1 d . . .
C7C C 0.2396(6) 0.6619(4) 0.2440(4) 0.0375(12) Uani 1 1 d . . .
C8C C 0.3362(7) 0.5952(5) 0.2405(5) 0.0473(17) Uani 1 1 d . . .
H8C H 0.3246 0.5274 0.2529 0.057 Uiso 1 1 calc R . .
C9C C 0.4496(7) 0.6268(5) 0.2190(5) 0.0539(16) Uani 1 1 d . . .
H9C H 0.5153 0.5804 0.2154 0.065 Uiso 1 1 calc R . .
C10C C 0.4683(5) 0.7236(5) 0.2029(4) 0.0405(13) Uani 1 1 d . . .
C11C C 0.3660(5) 0.7880(4) 0.2040(4) 0.0371(12) Uani 1 1 d . . .
H11C H 0.3762 0.8558 0.1901 0.044 Uiso 1 1 calc R . .
N12C N 0.2546(4) 0.7593(3) 0.2236(3) 0.0298(9) Uani 1 1 d . . .
C13C C 0.5925(6) 0.7647(6) 0.1854(5) 0.0553(17) Uani 1 1 d . . .
H13G H 0.6517 0.7104 0.1807 0.083 Uiso 1 1 calc R . .
H13H H 0.6352 0.8078 0.2438 0.083 Uiso 1 1 calc R . .
H13I H 0.5714 0.8025 0.1202 0.083 Uiso 1 1 calc R . .
P1 P 0.37454(14) 0.85668(16) 0.88273(10) 0.0463(3) Uani 1 1 d . . .
F11 F 0.4661(7) 0.9257(5) 0.9640(5) 0.128(3) Uani 1 1 d . . .
F12 F 0.4731(6) 0.8477(8) 0.8116(5) 0.149(3) Uani 1 1 d . . .
F13 F 0.3182(5) 0.9511(4) 0.8141(4) 0.0779(13) Uani 1 1 d . . .
F14 F 0.2807(9) 0.7923(4) 0.7972(4) 0.135(3) Uani 1 1 d . . .
F15 F 0.2766(7) 0.8700(6) 0.9466(5) 0.130(3) Uani 1 1 d . . .
F16 F 0.4361(14) 0.7659(5) 0.9399(5) 0.223(7) Uani 1 1 d . . .
P2 P 0.6886(2) 0.81965(14) 0.51238(14) 0.0611(5) Uani 1 1 d . . .
F21 F 0.5616(6) 0.7630(4) 0.5187(5) 0.1078(18) Uani 1 1 d . . .
F22 F 0.7069(6) 0.7392(5) 0.4312(5) 0.114(2) Uani 1 1 d . . .
F23 F 0.6006(6) 0.8842(4) 0.4220(4) 0.111(2) Uani 1 1 d . . .
F24 F 0.6682(6) 0.8952(6) 0.5957(5) 0.135(3) Uani 1 1 d . . .
F25 F 0.8168(6) 0.8696(6) 0.5042(6) 0.135(3) Uani 1 1 d . . .
F26 F 0.7720(6) 0.7523(6) 0.6028(5) 0.130(3) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1B Ru1 N12C 88.66(16) . . ?
N1B Ru1 N1A 172.24(18) . . ?
N12C Ru1 N1A 96.31(17) . . ?
N1B Ru1 N12B 79.03(17) . . ?
N12C Ru1 N12B 93.98(19) . . ?
N1A Ru1 N12B 94.64(17) . . ?
N1B Ru1 N12A 96.33(18) . . ?
N12C Ru1 N12A 174.15(19) . . ?
N1A Ru1 N12A 79.06(19) . . ?
N12B Ru1 N12A 89.98(16) . . ?
N1B Ru1 N1C 94.90(17) . . ?
N12C Ru1 N1C 78.94(18) . . ?
N1A Ru1 N1C 91.91(18) . . ?
N12B Ru1 N1C 170.86(17) . . ?
N12A Ru1 N1C 97.53(18) . . ?
C2A N1A C6A 118.1(5) . . ?
C2A N1A Ru1 126.6(4) . . ?
C6A N1A Ru1 115.3(4) . . ?
N1A C2A C3A 123.5(6) . . ?
C5A C4A C3A 120.3(6) . . ?
C4A C5A C6A 120.4(6) . . ?
N1A C6A C5A 120.2(6) . . ?
N1A C6A C7A 114.8(5) . . ?
C5A C6A C7A 125.0(5) . . ?
N12A C7A C8A 120.5(6) . . ?
N12A C7A C6A 115.1(5) . . ?
C8A C7A C6A 124.4(6) . . ?
C9A C8A C7A 119.5(7) . . ?
C10A C9A C8A 120.7(6) . . ?
N12A C11A C10A 124.0(8) . . ?
C11A N12A C7A 118.0(5) . . ?
C11A N12A Ru1 126.3(5) . . ?
C7A N12A Ru1 115.5(4) . . ?
C2A C3A C4A 117.5(6) . . ?
C9A C10A C11A 117.2(8) . . ?
C9A C10A C13A 119.4(8) . . ?
C11A C10A C13A 123.4(10) . . ?
C2B N1B C6B 118.1(5) . . ?
C2B N1B Ru1 126.0(4) . . ?
C6B N1B Ru1 115.9(3) . . ?
N1B C2B C3B 122.8(6) . . ?
C4B C3B C2B 118.6(6) . . ?
C3B C4B C5B 119.3(6) . . ?
C6B C5B C4B 119.7(6) . . ?
C5B C6B N1B 121.5(5) . . ?
C5B C6B C7B 124.7(5) . . ?
N1B C6B C7B 113.8(5) . . ?
N12B C7B C8B 120.8(5) . . ?
N12B C7B C6B 116.0(5) . . ?
C8B C7B C6B 123.2(5) . . ?
C9B C8B C7B 119.0(6) . . ?
C8B C9B C10B 121.1(5) . . ?
C9B C10B C11B 116.5(6) . . ?
C9B C10B C13B 122.9(6) . . ?
C11B C10B C13B 120.5(6) . . ?
N12B C11B C10B 123.0(5) . . ?
C7B N12B C11B 119.5(5) . . ?
C7B N12B Ru1 115.2(4) . . ?
C11B N12B Ru1 124.8(4) . . ?
C2C N1C C6C 118.5(5) . . ?
C2C N1C Ru1 126.0(4) . . ?
C6C N1C Ru1 115.4(4) . . ?
N1C C2C C3C 122.4(6) . . ?
C4C C3C C2C 119.2(6) . . ?
C3C C4C C5C 119.0(6) . . ?
C6C C5C C4C 119.5(6) . . ?
N1C C6C C5C 121.2(5) . . ?
N1C C6C C7C 115.0(5) . . ?
C5C C6C C7C 123.8(5) . . ?
N12C C7C C8C 120.1(6) . . ?
N12C C7C C6C 114.7(5) . . ?
C8C C7C C6C 125.3(6) . . ?
C7C C8C C9C 120.0(6) . . ?
C10C C9C C8C 120.6(6) . . ?
C9C C10C C11C 117.3(5) . . ?
C9C C10C C13C 123.8(5) . . ?
C11C C10C C13C 119.0(6) . . ?
N12C C11C C10C 123.4(5) . . ?
C11C N12C C7C 118.6(5) . . ?
C11C N12C Ru1 125.4(4) . . ?
C7C N12C Ru1 116.0(4) . . ?
F16 P1 F15 94.8(6) . . ?
F16 P1 F11 92.3(5) . . ?
F15 P1 F11 86.0(4) . . ?
F16 P1 F14 90.7(5) . . ?
F15 P1 F14 94.5(5) . . ?
F11 P1 F14 176.9(4) . . ?
F16 P1 F13 174.1(5) . . ?
F15 P1 F13 91.1(4) . . ?
F11 P1 F13 88.8(3) . . ?
F14 P1 F13 88.1(3) . . ?
F16 P1 F12 88.5(6) . . ?
F15 P1 F12 176.7(4) . . ?
F11 P1 F12 94.2(5) . . ?
F14 P1 F12 85.1(5) . . ?
F13 P1 F12 85.7(4) . . ?
F25 P2 F24 93.2(4) . . ?
F25 P2 F21 176.6(4) . . ?
F24 P2 F21 89.8(3) . . ?
F25 P2 F23 92.9(4) . . ?
F24 P2 F23 90.5(4) . . ?
F21 P2 F23 88.6(4) . . ?
F25 P2 F26 89.3(4) . . ?
F24 P2 F26 89.8(4) . . ?
F21 P2 F26 89.2(3) . . ?
F23 P2 F26 177.8(4) . . ?
F25 P2 F22 89.0(4) . . ?
F24 P2 F22 177.2(4) . . ?
F21 P2 F22 88.0(4) . . ?
F23 P2 F22 91.1(3) . . ?
F26 P2 F22 88.5(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 N1B 2.048(4) . ?
Ru1 N12C 2.052(4) . ?
Ru1 N1A 2.055(4) . ?
Ru1 N12B 2.059(4) . ?
Ru1 N12A 2.063(4) . ?
Ru1 N1C 2.074(5) . ?
N1A C2A 1.346(7) . ?
N1A C6A 1.378(7) . ?
C2A C3A 1.377(8) . ?
C4A C5A 1.353(10) . ?
C4A C3A 1.390(10) . ?
C5A C6A 1.386(8) . ?
C6A C7A 1.464(9) . ?
C7A N12A 1.362(7) . ?
C7A C8A 1.388(8) . ?
C8A C9A 1.384(12) . ?
C9A C10A 1.355(12) . ?
C11A N12A 1.344(9) . ?
C11A C10A 1.388(10) . ?
C13A C10A 1.420(14) . ?
N1B C2B 1.336(7) . ?
N1B C6B 1.373(7) . ?
C2B C3B 1.392(8) . ?
C3B C4B 1.364(11) . ?
C4B C5B 1.396(10) . ?
C5B C6B 1.359(8) . ?
C6B C7B 1.469(8) . ?
C7B N12B 1.347(7) . ?
C7B C8B 1.391(9) . ?
C8B C9B 1.383(9) . ?
C9B C10B 1.385(9) . ?
C10B C11B 1.398(8) . ?
C10B C13B 1.492(9) . ?
C11B N12B 1.349(7) . ?
N1C C2C 1.340(8) . ?
N1C C6C 1.359(7) . ?
C2C C3C 1.384(9) . ?
C3C C4C 1.363(10) . ?
C4C C5C 1.391(10) . ?
C5C C6C 1.379(8) . ?
C6C C7C 1.478(8) . ?
C7C N12C 1.368(7) . ?
C7C C8C 1.377(9) . ?
C8C C9C 1.379(10) . ?
C9C C10C 1.354(9) . ?
C10C C11C 1.397(7) . ?
C10C C13C 1.504(8) . ?
C11C N12C 1.335(7) . ?
P1 F16 1.501(6) . ?
P1 F15 1.521(5) . ?
P1 F11 1.555(5) . ?
P1 F14 1.560(6) . ?
P1 F13 1.593(5) . ?
P1 F12 1.594(5) . ?
P2 F25 1.548(6) . ?
P2 F24 1.568(6) . ?
P2 F21 1.572(6) . ?
P2 F23 1.572(6) . ?
P2 F26 1.576(6) . ?
P2 F22 1.585(6) . ?
