#------------------------------------------------------------------------------
#$Date: 2016-02-14 05:40:26 +0100 (dom 14 de feb de 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/31/7013165.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7013165
loop_
_publ_author_name
'Fleming, Sean'
'Gutsche, C. David'
'Harrowfield, Jack M.'
'Ogden, Mark I.'
'Skelton, Brian W.'
'Stewart, Donald F.'
'White, Allan H.'
_publ_section_title
;
 Calixarenes as aryloxides: oligonuclear europium(iii) derivatives
;
_journal_issue                   17
_journal_name_full               'Dalton Transactions'
_journal_page_first              3319
_journal_paper_doi               10.1039/b305041f
_journal_year                    2003
_chemical_formula_sum            'C175 H248 Eu4 N4 O30 S6'
_chemical_formula_weight         3688.14
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 92.54(2)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   21.152(4)
_cell_length_b                   33.453(7)
_cell_length_c                   30.524(5)
_cell_measurement_reflns_used    14
_cell_measurement_temperature    293
_cell_measurement_theta_max      14.5
_cell_measurement_theta_min      12.3
_cell_volume                     21577(7)
_computing_cell_refinement       'Enraf Nonius software'
_computing_data_collection       'Enraf Nonius software'
_computing_data_reduction        xtal
_computing_molecular_graphics    xtal
_computing_publication_material  'xtal BONDLA CIFIO'
_computing_structure_refinement  'xtal CRYLSQ'
_computing_structure_solution    xtal
_diffrn_ambient_temperature      293
_diffrn_measurement_device_type  CAD4
_diffrn_measurement_method       '2θ-ω scans'
_diffrn_radiation_detector       'scintillation counter'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_sigmaI/netI    0
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       39
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            37850
_diffrn_reflns_reduction_process 'perpendicular monochr Lp'
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_min         1.3
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  60
_diffrn_standards_number         6
_exptl_absorpt_coefficient_mu    1.261
_exptl_absorpt_correction_T_max  .85
_exptl_absorpt_correction_T_min  .79
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
XTAL absorb                 
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.135
_exptl_crystal_description       block
_exptl_crystal_F_000             7184
_exptl_crystal_size_max          .24
_exptl_crystal_size_mid          .2
_exptl_crystal_size_min          .14
_refine_diff_density_max         2.86
_refine_diff_density_min         -.852
_refine_ls_goodness_of_fit_all   1.696
_refine_ls_goodness_of_fit_ref   2.402
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           atomblock
_refine_ls_number_constraints    0
_refine_ls_number_parameters     1853
_refine_ls_number_reflns         12379
_refine_ls_number_restraints     182
_refine_ls_R_factor_all          .243
_refine_ls_R_factor_gt           .093
_refine_ls_shift/su_max          .118
_refine_ls_shift/su_mean         .007
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         .143
_refine_ls_wR_factor_ref         .112
_reflns_d_resolution_high        .84
_reflns_d_resolution_low         15.673
_reflns_Friedel_coverage         0
_reflns_limit_h_max              25
_reflns_limit_h_min              0
_reflns_limit_k_max              39
_reflns_limit_k_min              0
_reflns_limit_l_max              36
_reflns_limit_l_min              -36
_reflns_number_gt                12380
_reflns_number_total             37850
_reflns_threshold_expression     'I    > 3.00 sig(I   )'
_cod_data_source_file            b305041f.txt
_cod_data_source_block           eucal7
_cod_original_sg_symbol_Hall     -p_2yn
_cod_original_sg_symbol_H-M      P_1_21/n_1
_cod_database_code               7013165
loop_
_symmetry_equiv_pos_as_xyz
+x,+y,+z
1/2-x,1/2+y,1/2-z
-x,-y,-z
1/2+x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_calc_attached_atom
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Eu1 .89050(6) .69576(4) .41236(5) .0579(9) Uani ? ? 1.00000 ? ?
Eu2 .73757(6) .64256(4) .43281(5) .0585(9) Uani ? ? 1.00000 ? ?
Eu3 .69341(6) .74308(4) .47776(5) .0618(9) Uani ? ? 1.00000 ? ?
Eu4 .73801(6) .73396(4) .36020(5) .0621(9) Uani ? ? 1.00000 ? ?
O1 .6773(7) .6999(4) .4156(5) .064(11) Uani ? ? 1.00000 ? ?
O2 .7927(7) .6741(4) .3725(5) .058(10) Uani ? ? 1.00000 ? ?
C0 .8262(11) .7388(7) .4738(9) .077(19) Uani ? ? 1.00000 ? ?
O101 .7919(6) .7211(4) .4432(5) .061(11) Uani ? ? 1.00000 ? ?
O102 .8855(7) .7347(5) .4764(5) .083(13) Uani ? ? 1.00000 ? ?
O103 .8003(7) .7604(5) .5034(6) .080(12) Uani ? ? 1.00000 ? ?
O111 .9337(7) .6687(4) .3506(5) .062(11) Uani ? ? 1.00000 ? ?
C111 .9856(11) .6794(6) .3313(7) .057(16) Uani ? ? 1.00000 ? ?
C112 1.0406(11) .6554(7) .3344(8) .065(18) Uani ? ? 1.00000 ? ?
C113 1.0978(10) .6694(7) .3162(9) .069(18) Uani ? ? 1.00000 ? ?
C114 1.1022(10) .7064(7) .2983(8) .069(18) Uani ? ? 1.00000 ? ?
C1141 1.1660(9) .7246(6) .2850(6) .09(2) Uani ? ? 1.00000 ? ?
C1142 1.193(2) .6949(13) .2528(15) .088(18) Uiso ? ? .50000 ? ?
C1143 1.160(2) .7651(13) .2633(15) .091(19) Uiso ? ? .50000 ? ?
C1144 1.208(2) .7258(13) .3245(14) .081(17) Uiso ? ? .50000 ? ?
C1142' 1.219(3) .6977(16) .2958(18) .15(3) Uiso ? ? .50000 ? ?
C1143' 1.163(2) .7347(14) .2389(15) .11(2) Uiso ? ? .50000 ? ?
C1144' 1.176(3) .7646(16) .3090(18) .14(3) Uiso ? ? .50000 ? ?
C115 1.0461(11) .7282(7) .2928(8) .08(2) Uani ? ? 1.00000 ? ?
C116 .9886(10) .7142(8) .3086(8) .08(2) Uani ? ? 1.00000 ? ?
C11 1.0346(12) .6125(8) .3512(9) .08(2) Uani ? ? 1.00000 ? ?
O121 .9053(7) .6040(4) .3211(5) .072(12) Uani ? ? 1.00000 ? ?
C121 .9495(11) .5797(7) .3063(7) .063(17) Uani ? ? 1.00000 ? ?
C122 .9305(12) .5520(7) .2756(9) .09(2) Uani ? ? 1.00000 ? ?
C123 .9717(14) .5254(8) .2587(10) .11(3) Uani ? ? 1.00000 ? ?
C124 1.0365(12) .5271(7) .2726(8) .09(2) Uani ? ? 1.00000 ? ?
C1241 1.0848(11) .4932(8) .2564(8) .13(3) Uani ? ? 1.00000 ? ?
C1242 1.1515(15) .5047(10) .2689(13) .19(4) Uani ? ? 1.00000 ? ?
C1243 1.0762(18) .4901(13) .2067(12) .23(5) Uani ? ? 1.00000 ? ?
C1244 1.072(2) .4527(9) .2783(14) .22(5) Uani ? ? 1.00000 ? ?
C125 1.0547(12) .5558(7) .3035(8) .08(2) Uani ? ? 1.00000 ? ?
C126 1.0125(11) .5829(7) .3198(8) .064(17) Uani ? ? 1.00000 ? ?
C12 .8620(13) .5495(7) .2556(10) .09(2) Uani ? ? 1.00000 ? ?
O131 .8042(9) .6253(5) .2787(5) .094(14) Uani ? ? 1.00000 ? ?
C131 .8240(11) .6196(7) .2367(9) .08(2) Uani ? ? 1.00000 ? ?
C132 .8231(11) .6484(6) .2069(8) .070(18) Uani ? ? 1.00000 ? ?
C133 .8371(14) .6418(7) .1633(9) .09(2) Uani ? ? 1.00000 ? ?
C134 .8567(14) .6049(9) .1502(8) .10(2) Uani ? ? 1.00000 ? ?
C1341 .8681(16) .5984(8) .1036(11) .13(3) Uani ? ? 1.00000 ? ?
C1342 .914(2) .5612(12) .0959(11) .19(4) Uani ? ? 1.00000 ? ?
C1343 .905(2) .6307(11) .0805(12) .22(4) Uani ? ? 1.00000 ? ?
C1344 .808(2) .5858(15) .0802(13) .24(5) Uani ? ? 1.00000 ? ?
C135 .8644(13) .5761(7) .1824(8) .08(2) Uani ? ? 1.00000 ? ?
C136 .8484(12) .5831(7) .2239(8) .07(2) Uani ? ? 1.00000 ? ?
C13 .8057(11) .6906(7) .2189(9) .08(2) Uani ? ? 1.00000 ? ?
O141 .7158(7) .6849(5) .2875(5) .074(12) Uani ? ? 1.00000 ? ?
C141 .6951(10) .6943(7) .2474(7) .062(17) Uani ? ? 1.00000 ? ?
C142 .6289(12) .7046(7) .2379(8) .07(2) Uani ? ? 1.00000 ? ?
C143 .6097(13) .7188(10) .1973(9) .11(3) Uani ? ? 1.00000 ? ?
C144 .6528(13) .7240(8) .1631(8) .10(2) Uani ? ? 1.00000 ? ?
C1441 .6315(9) .7432(7) .1154(7) .16(3) Uani ? ? 1.00000 ? ?
C1442 .678(3) .7346(18) .081(2) .20(4) Uiso ? ? .50000 ? ?
C1443 .572(3) .7260(18) .101(2) .20(4) Uiso ? ? .50000 ? ?
C1444 .627(3) .789(2) .124(2) .27(5) Uiso ? ? .50000 ? ?
C1442' .636(3) .7120(18) .081(2) .20(4) Uiso ? ? .50000 ? ?
C1443' .567(2) .7587(16) .1175(17) .14(3) Uiso ? ? .50000 ? ?
C1444' .678(3) .779(2) .104(2) .24(5) Uiso ? ? .50000 ? ?
C145 .7158(12) .7133(9) .1752(11) .11(3) Uani ? ? 1.00000 ? ?
C146 .7350(12) .6994(8) .2156(7) .08(2) Uani ? ? 1.00000 ? ?
C14 .5780(11) .6997(8) .2731(8) .08(2) Uani ? ? 1.00000 ? ?
O151 .6354(7) .7391(5) .3442(6) .089(13) Uani ? ? 1.00000 ? ?
C151 .5842(11) .7558(8) .3247(9) .08(2) Uani ? ? 1.00000 ? ?
C152 .5590(11) .7903(7) .3425(9) .08(2) Uani ? ? 1.00000 ? ?
C153 .5063(11) .8073(7) .3213(8) .074(19) Uani ? ? 1.00000 ? ?
C154 .4810(13) .7939(8) .2836(9) .09(2) Uani ? ? 1.00000 ? ?
C1541 .4230(15) .8159(10) .2596(11) .126(12) Uiso ? ? 1.00000 ? ?
C1542 .4425(18) .8282(15) .2199(13) .23(5) Uani ? ? 1.00000 ? ?
C1543 .370(2) .7890(13) .254(2) .30(6) Uani ? ? 1.00000 ? ?
C1544 .400(2) .8490(16) .282(2) .38(8) Uani ? ? 1.00000 ? ?
C155 .5019(12) .7579(9) .2695(9) .10(2) Uani ? ? 1.00000 ? ?
C156 .5546(12) .7396(7) .2889(9) .08(2) Uani ? ? 1.00000 ? ?
C15 .5871(11) .8069(6) .3835(9) .073(18) Uani ? ? 1.00000 ? ?
O161 .7138(7) .7797(4) .4137(5) .069(11) Uani ? ? 1.00000 ? ?
C161 .7087(11) .8172(6) .3964(7) .061(17) Uani ? ? 1.00000 ? ?
C162 .7614(12) .8404(7) .3903(8) .073(19) Uani ? ? 1.00000 ? ?
C163 .7503(13) .8808(7) .3730(10) .10(2) Uani ? ? 1.00000 ? ?
C164 .6909(13) .8947(8) .3577(10) .10(2) Uani ? ? 1.00000 ? ?
C1641 .6925(17) .9391(11) .3398(12) .153(15) Uiso ? ? 1.00000 ? ?
C1642 .719(2) .9666(14) .3723(15) .22(2) Uiso ? ? 1.00000 ? ?
C1643 .626(2) .9476(13) .3246(14) .21(2) Uiso ? ? 1.00000 ? ?
C1644 .730(2) .9387(12) .2990(13) .189(18) Uiso ? ? 1.00000 ? ?
C165 .6429(12) .8682(7) .3615(9) .08(2) Uani ? ? 1.00000 ? ?
C166 .6480(12) .8313(7) .3801(9) .08(2) Uani ? ? 1.00000 ? ?
C16 .8260(13) .8267(7) .4055(9) .09(2) Uani ? ? 1.00000 ? ?
O171 .8473(7) .7510(4) .3688(5) .062(11) Uani ? ? 1.00000 ? ?
C171 .8786(11) .7829(6) .3537(8) .062(17) Uani ? ? 1.00000 ? ?
C172 .8688(11) .8198(7) .3693(8) .067(18) Uani ? ? 1.00000 ? ?
C173 .8993(13) .8524(7) .3536(9) .09(2) Uani ? ? 1.00000 ? ?
C174 .9388(13) .8494(7) .3184(9) .10(2) Uani ? ? 1.00000 ? ?
C1741 .9768(10) .8873(6) .2993(7) .14(3) Uani ? ? 1.00000 ? ?
C1742 1.016(3) .9039(16) .3347(17) .15(3) Uiso ? ? .50000 ? ?
C1743 .928(3) .9168(18) .2848(19) .19(4) Uiso ? ? .50000 ? ?
C1744 1.014(2) .8776(14) .2626(15) .10(2) Uiso ? ? .50000 ? ?
C1742' 1.049(2) .8788(16) .3008(18) .14(3) Uiso ? ? .50000 ? ?
C1743' .954(3) .8917(17) .2527(18) .17(3) Uiso ? ? .50000 ? ?
C1744' .968(2) .9216(13) .3235(15) .089(19) Uiso ? ? .50000 ? ?
C175 .9489(12) .8119(7) .3022(9) .08(2) Uani ? ? 1.00000 ? ?
C176 .9182(12) .7784(6) .3178(8) .067(18) Uani ? ? 1.00000 ? ?
C17 .9288(11) .7387(7) .2967(8) .066(17) Uani ? ? 1.00000 ? ?
O211 .5870(7) .7320(5) .4837(5) .070(12) Uani ? ? 1.00000 ? ?
C211 .5509(11) .7265(7) .5187(8) .065(18) Uani ? ? 1.00000 ? ?
C212 .5062(11) .7579(7) .5283(8) .071(18) Uani ? ? 1.00000 ? ?
C213 .4709(14) .7560(8) .5655(10) .10(2) Uani ? ? 1.00000 ? ?
C214 .4721(12) .7243(7) .5904(9) .13(3) Uani ? ? 1.00000 ? ?
C2141 .4390(10) .7236(6) .6337(7) .17(4) Uani ? ? 1.00000 ? ?
C2142 .450(2) .6888(13) .6616(14) .085(18) Uiso ? ? .50000 ? ?
C2143 .370(2) .7319(13) .6242(15) .085(18) Uiso ? ? .50000 ? ?
C2144 .466(3) .7618(16) .6603(18) .14(3) Uiso ? ? .50000 ? ?
C2142' .399(3) .6860(18) .630(2) .20(4) Uiso ? ? .50000 ? ?
C2143' .398(3) .7548(17) .6385(18) .18(3) Uiso ? ? .50000 ? ?
C2144' .484(3) .7199(18) .671(2) .19(4) Uiso ? ? .50000 ? ?
C215 .5133(13) .6928(9) .5814(8) .10(2) Uani ? ? 1.00000 ? ?
C216 .5516(11) .6945(7) .5444(8) .068(18) Uani ? ? 1.00000 ? ?
C21 .4953(11) .7912(7) .4963(9) .08(2) Uani ? ? 1.00000 ? ?
O221 .5087(7) .7382(5) .4213(5) .076(12) Uani ? ? 1.00000 ? ?
C221 .4555(12) .7565(7) .4266(8) .08(2) Uani ? ? 1.00000 ? ?
C222 .4030(13) .7494(7) .3964(9) .09(2) Uani ? ? 1.00000 ? ?
C223 .3471(12) .7688(9) .4003(10) .10(2) Uani ? ? 1.00000 ? ?
C224 .3350(14) .7952(9) .4320(10) .16(3) Uani ? ? 1.00000 ? ?
C2241 .2667(11) .8155(7) .4367(7) .17(4) Uani ? ? 1.00000 ? ?
C2242 .257(2) .8415(15) .4001(17) .13(3) Uiso ? ? .50000 ? ?
C2243 .259(2) .8347(15) .4791(16) .12(2) Uiso ? ? .50000 ? ?
C2244 .220(3) .7799(18) .434(2) .20(4) Uiso ? ? .50000 ? ?
C2242' .234(2) .8176(16) .3943(17) .14(3) Uiso ? ? .50000 ? ?
C2243' .280(3) .8584(17) .450(2) .19(4) Uiso ? ? .50000 ? ?
C2244' .229(3) .794(2) .473(2) .25(5) Uiso ? ? .50000 ? ?
C225 .3877(16) .8031(9) .4624(11) .13(3) Uani ? ? 1.00000 ? ?
C226 .4467(12) .7835(7) .4592(9) .08(2) Uani ? ? 1.00000 ? ?
C22 .4120(10) .7192(8) .3626(8) .08(2) Uani ? ? 1.00000 ? ?
O231 .5237(7) .6695(5) .3880(6) .095(14) Uani ? ? 1.00000 ? ?
C231 .4634(11) .6539(7) .3960(10) .09(2) Uani ? ? 1.00000 ? ?
C232 .4623(13) .6198(8) .4196(11) .11(2) Uani ? ? 1.00000 ? ?
C233 .4057(13) .6026(10) .4267(15) .18(4) Uani ? ? 1.00000 ? ?
C234 .3534(16) .6187(10) .4059(10) .138(13) Uiso ? ? 1.00000 ? ?
C2341 .2839(12) .5929(7) .4094(8) .200(19) Uiso ? ? 1.00000 ? ?
C2342 .274(2) .5866(15) .4570(16) .11(2) Uiso ? ? .50000 ? ?
C2343 .229(2) .6147(14) .3883(16) .10(2) Uiso ? ? .50000 ? ?
C2344 .297(3) .5515(16) .3834(17) .13(3) Uiso ? ? .50000 ? ?
C2342' .286(3) .5592(18) .4427(19) .19(4) Uiso ? ? .50000 ? ?
C2343' .235(3) .623(2) .428(2) .33(7) Uiso ? ? .50000 ? ?
C2344' .271(3) .580(2) .364(2) .31(6) Uiso ? ? .50000 ? ?
C235 .3562(14) .6576(9) .3846(10) .110(11) Uiso ? ? 1.00000 ? ?
C236 .4130(11) .6764(7) .3822(9) .08(2) Uani ? ? 1.00000 ? ?
C23 .5219(11) .6016(7) .4421(10) .09(2) Uani ? ? 1.00000 ? ?
O241 .6242(7) .6163(4) .3856(6) .074(12) Uani ? ? 1.00000 ? ?
C241 .5986(11) .5780(7) .3888(8) .070(18) Uani ? ? 1.00000 ? ?
C242 .6254(12) .5484(7) .3637(8) .08(2) Uani ? ? 1.00000 ? ?
C243 .5972(13) .5087(7) .3706(10) .10(2) Uani ? ? 1.00000 ? ?
C244 .5498(11) .5008(7) .3969(9) .10(2) Uani ? ? 1.00000 ? ?
C2441 .5282(9) .4585(7) .4035(7) .13(3) Uani ? ? 1.00000 ? ?
C2442 .471(2) .4570(16) .4322(17) .14(3) Uiso ? ? .50000 ? ?
C2443 .512(2) .4402(14) .3561(15) .10(2) Uiso ? ? .50000 ? ?
C2444 .580(3) .4354(17) .4266(18) .17(3) Uiso ? ? .50000 ? ?
C2442' .460(3) .4582(16) .3979(17) .15(3) Uiso ? ? .50000 ? ?
C2443' .552(2) .4318(15) .3736(17) .14(3) Uiso ? ? .50000 ? ?
C2444' .547(3) .4456(16) .4504(17) .14(3) Uiso ? ? .50000 ? ?
C245 .5279(11) .5317(7) .4205(10) .09(2) Uani ? ? 1.00000 ? ?
C246 .5504(11) .5697(7) .4173(8) .069(18) Uani ? ? 1.00000 ? ?
C24 .6799(12) .5539(7) .3315(8) .07(2) Uani ? ? 1.00000 ? ?
O251 .7678(7) .5971(4) .3848(5) .063(11) Uani ? ? 1.00000 ? ?
C251 .7832(11) .5594(6) .3769(8) .064(17) Uani ? ? 1.00000 ? ?
C252 .8392(11) .5433(7) .3918(8) .066(18) Uani ? ? 1.00000 ? ?
C253 .8523(11) .5026(7) .3856(8) .071(18) Uani ? ? 1.00000 ? ?
C254 .8104(11) .4788(7) .3614(8) .068(18) Uani ? ? 1.00000 ? ?
C2541 .8236(14) .4349(8) .3570(10) .10(2) Uani ? ? 1.00000 ? ?
C2542 .7726(16) .4105(10) .3350(14) .17(3) Uani ? ? 1.00000 ? ?
C2543 .844(2) .4164(9) .3973(14) .22(4) Uani ? ? 1.00000 ? ?
C2544 .8793(18) .4280(10) .3279(14) .18(4) Uani ? ? 1.00000 ? ?
C255 .7566(11) .4949(7) .3444(9) .08(2) Uani ? ? 1.00000 ? ?
C256 .7418(11) .5354(7) .3523(8) .070(19) Uani ? ? 1.00000 ? ?
C25 .8876(10) .5694(7) .4141(8) .065(17) Uani ? ? 1.00000 ? ?
O261 .8438(7) .6426(5) .4542(5) .076(12) Uani ? ? 1.00000 ? ?
C261 .8605(11) .6102(7) .4812(7) .059(7) Uiso ? ? 1.00000 ? ?
C262 .8577(11) .6166(6) .5269(8) .058(17) Uani ? ? 1.00000 ? ?
C263 .8728(10) .5857(7) .5519(8) .063(17) Uani ? ? 1.00000 ? ?
C264 .8939(11) .5473(7) .5354(8) .069(18) Uani ? ? 1.00000 ? ?
C2641 .9109(11) .5137(8) .5663(8) .08(2) Uani ? ? 1.00000 ? ?
C2642 .9708(15) .5246(9) .5942(13) .15(3) Uani ? ? 1.00000 ? ?
C2643 .8608(15) .5065(9) .6010(12) .14(3) Uani ? ? 1.00000 ? ?
C2644 .9215(18) .4721(9) .5451(12) .15(3) Uani ? ? 1.00000 ? ?
C265 .8959(11) .5442(6) .4914(8) .066(18) Uani ? ? 1.00000 ? ?
C266 .8811(10) .5737(6) .4636(9) .072(18) Uani ? ? 1.00000 ? ?
C26 .8336(10) .6550(7) .5462(8) .062(17) Uani ? ? 1.00000 ? ?
O271 .7165(7) .6738(4) .4977(5) .056(10) Uani ? ? 1.00000 ? ?
C271 .7164(9) .6603(6) .5400(8) .056(16) Uani ? ? 1.00000 ? ?
C272 .6548(10) .6515(6) .5614(8) .058(16) Uani ? ? 1.00000 ? ?
C273 .6569(11) .6369(6) .6035(7) .057(16) Uani ? ? 1.00000 ? ?
C274 .7088(11) .6310(6) .6275(7) .068(18) Uani ? ? 1.00000 ? ?
C2741 .7050(9) .6160(6) .6738(7) .09(2) Uani ? ? 1.00000 ? ?
C2742 .650(2) .6384(15) .6968(16) .12(2) Uiso ? ? .50000 ? ?
C2743 .766(2) .6206(14) .7015(15) .10(2) Uiso ? ? .50000 ? ?
C2744 .691(3) .5723(16) .6708(18) .15(3) Uiso ? ? .50000 ? ?
C2742' .642(2) .6042(15) .6857(16) .12(2) Uiso ? ? .50000 ? ?
C2743' .724(3) .6497(17) .7034(19) .17(3) Uiso ? ? .50000 ? ?
C2744' .756(3) .5848(19) .683(2) .23(4) Uiso ? ? .50000 ? ?
C275 .7666(10) .6376(7) .6075(8) .063(17) Uani ? ? 1.00000 ? ?
C276 .7691(10) .6513(6) .5676(7) .054(16) Uani ? ? 1.00000 ? ?
C27 .5941(12) .6573(6) .5329(7) .062(17) Uani ? ? 1.00000 ? ?
O10 .6888(9) .7469(5) .5502(6) .106(15) Uani ? ? 1.00000 ? ?
S10 .7038(9) .7705(5) .5909(5) .102(15) Uani ? ? .49(3) ? ?
S10' .699(2) .7484(12) .5915(13) .33(2) Uiso ? ? .51(3) ? ?
C101 .760(3) .7478(18) .621(2) .31(3) Uiso ? ? 1.00000 ? ?
C102 .632(2) .7629(16) .6228(17) .26(2) Uiso ? ? 1.00000 ? ?
O20 .9801(7) .7397(5) .4107(6) .091(14) Uani ? ? 1.00000 ? ?
S20 .9857(7) .7807(4) .4282(5) .090(12) Uani ? ? .54(2) ? ?
S20' 1.0260(19) .7634(13) .4348(13) .34(5) Uani ? ? .46(2) ? ?
C201 1.051(2) .7982(12) .3976(14) .20(4) Uani ? ? 1.00000 ? ?
C202 1.024(3) .7829(15) .4817(15) .27(6) Uani ? ? 1.00000 ? ?
O30 .9769(7) .6607(5) .4511(7) .101(15) Uani ? ? 1.00000 ? ?
S30 1.0260(5) .6696(4) .4825(4) .100(9) Uani ? ? .751(16) ? ?
S30' 1.033(2) .6271(18) .488(2) .29(7) Uani ? ? .249(16) ? ?
C301 1.026(2) .6409(15) .5187(16) .24(2) Uiso ? ? 1.00000 ? ?
C302 1.093(3) .6650(17) .4537(18) .28(3) Uiso ? ? 1.00000 ? ?
O40 .6977(8) .5884(5) .4718(6) .092(14) Uani ? ? 1.00000 ? ?
S40 .6723(5) .5515(3) .4919(4) .077(8) Uani ? ? .691(12) ? ?
S40' .7316(11) .5508(7) .4967(8) .081(18) Uani ? ? .309(12) ? ?
C401 .7040(17) .5500(7) .5407(10) .13(3) Uani ? ? 1.00000 ? ?
C402 .7135(16) .5122(8) .4673(11) .13(3) Uani ? ? 1.00000 ? ?
O50 .7522(9) .7739(5) .2966(6) .100(15) Uani ? ? 1.00000 ? ?
S50 .7353(6) .8155(4) .2806(4) .112(11) Uani ? ? .692(13) ? ?
S50' .7529(11) .7927(6) .2517(7) .064(15) Uani ? ? .308(13) ? ?
C501 .6722(16) .8138(11) .2480(12) .16(3) Uani ? ? 1.00000 ? ?
C502 .787(2) .8293(15) .2531(17) .28(5) Uani ? ? 1.00000 ? ?
O60 .6655(9) .8098(5) .4900(6) .121(17) Uani ? ? 1.00000 ? ?
S60 .6797(9) .8461(6) .5168(7) .185(10) Uiso ? ? .50000 ? ?
S60' .6401(10) .8527(7) .4911(7) .233(13) Uiso ? ? .50000 ? ?
C601 .704(2) .8877(10) .4834(13) .50(5) Uiso ? ? 1.00000 ? ?
C602 .6063(19) .8616(10) .5469(13) .36(4) Uiso ? ? 1.00000 ? ?
N01 1.0833(17) .6357(12) .1627(10) .36(6) Uani ? ? 1.00000 ? ?
C011 1.0548(12) .6369(9) .1773(8) .138(13) Uiso ? ? 1.00000 ? ?
C012 1.0080(19) .6386(13) .2019(15) .41(8) Uani ? ? 1.00000 ? ?
N02 .273(3) .6962(15) .5110(11) .41(3) Uiso ? ? 1.00000 ? ?
C021 .3019(18) .6764(10) .5251(7) .197(19) Uiso ? ? 1.00000 ? ?
C022 .342(3) .6487(19) .5429(14) .46(5) Uiso ? ? 1.00000 ? ?
N03 .454(3) .9093(16) .4160(16) .44(4) Uiso ? ? 1.00000 ? ?
C031 .472(3) .9312(16) .4433(13) .38(8) Uani ? ? 1.00000 ? ?
C032 .492(4) .956(2) .4723(19) .55(14) Uani ? ? 1.00000 ? ?
N04 .664(2) .5663(14) .1635(17) .39(3) Uiso ? ? 1.00000 ? ?
C041 .629(3) .5778(13) .182(2) .44(5) Uiso ? ? 1.00000 ? ?
C042 .584(4) .590(3) .205(4) .77(10) Uiso ? ? 1.00000 ? ?
O01 .872(5) .950(3) .469(3) .88(8) Uiso ? ? 1.00000 ? ?
O02 .886(3) .8122(18) .554(2) .51(4) Uiso ? ? 1.00000 ? ?
O03 1.072(4) .896(2) .486(2) .67(5) Uiso ? ? 1.00000 ? ?
O04 .384(4) .660(2) .163(3) .67(5) Uiso ? ? 1.00000 ? ?
O05 .441(3) .5733(18) .2826(18) .49(4) Uiso ? ? 1.00000 ? ?
H113 1.13547 .65173 .31712 .09200 Uiso ? ? 1.00000 ? ?
H1142a 1.23038 .70483 .24284 .18000 Uiso ? ? .50000 ? ?
H1142b 1.16143 .69383 .22812 .18000 Uiso ? ? .50000 ? ?
H1142c 1.19650 .66961 .26510 .18000 Uiso ? ? .50000 ? ?
H1143a 1.20347 .77341 .25842 .10000 Uiso ? ? .50000 ? ?
H1143b 1.14467 .78279 .28527 .10000 Uiso ? ? .50000 ? ?
H1143c 1.13619 .76347 .23918 .10000 Uiso ? ? .50000 ? ?
H1144a 1.24926 .73422 .31678 .11100 Uiso ? ? .50000 ? ?
H1144b 1.21550 .69669 .33431 .11100 Uiso ? ? .50000 ? ?
H1144c 1.19233 .73904 .34668 .11100 Uiso ? ? .50000 ? ?
H1143'a 1.20183 .74643 .23289 .10000 Uiso ? ? .50000 ? ?
H1143'b 1.13034 .75535 .23686 .10000 Uiso ? ? .50000 ? ?
H1143'c 1.15219 .71316 .22284 .10000 Uiso ? ? .50000 ? ?
H1142'a 1.25602 .70467 .28350 .29100 Uiso ? ? .50000 ? ?
H1142'b 1.20738 .66994 .28099 .29100 Uiso ? ? .50000 ? ?
H1142'c 1.22360 .69077 .32549 .29100 Uiso ? ? .50000 ? ?
H1144'a 1.21961 .77153 .30289 .15100 Uiso ? ? .50000 ? ?
H1144'b 1.18194 .75508 .34146 .15100 Uiso ? ? .50000 ? ?
H1144'c 1.14758 .77977 .30456 .15100 Uiso ? ? .50000 ? ?
H115 1.04769 .75361 .27507 .09500 Uiso ? ? 1.00000 ? ?
H11a 1.00510 .61300 .37666 .10200 Uiso ? ? 1.00000 ? ?
H11b 1.07515 .60466 .36663 .10200 Uiso ? ? 1.00000 ? ?
H123 .96212 .50410 .23637 .13200 Uiso ? ? 1.00000 ? ?
H1242a 1.18262 .48532 .25943 .23900 Uiso ? ? 1.00000 ? ?
H1242b 1.15854 .50730 .30022 .23900 Uiso ? ? 1.00000 ? ?
H1242c 1.16406 .53013 .25632 .23900 Uiso ? ? 1.00000 ? ?
H1243a 1.10484 .47066 .19567 .29600 Uiso ? ? 1.00000 ? ?
H1243b 1.08536 .51534 .19342 .29600 Uiso ? ? 1.00000 ? ?
H1243c 1.03448 .48267 .19959 .29600 Uiso ? ? 1.00000 ? ?
H1244a 1.10166 .43339 .26675 .28100 Uiso ? ? 1.00000 ? ?
H1244b 1.03085 .44509 .26853 .28100 Uiso ? ? 1.00000 ? ?
H1244c 1.07740 .45498 .30774 .28100 Uiso ? ? 1.00000 ? ?
H125 1.10046 .55537 .31367 .09900 Uiso ? ? 1.00000 ? ?
H12a .83176 .55137 .28063 .11000 Uiso ? ? 1.00000 ? ?
H12b .85087 .52332 .24297 .11000 Uiso ? ? 1.00000 ? ?
H133 .83141 .66374 .14002 .12100 Uiso ? ? 1.00000 ? ?
H1342a .91735 .55454 .06585 .25900 Uiso ? ? 1.00000 ? ?
H1342b .88983 .53706 .10805 .25900 Uiso ? ? 1.00000 ? ?
H1342c .94963 .56393 .11131 .25900 Uiso ? ? 1.00000 ? ?
H1343a .90736 .62688 .04844 .24900 Uiso ? ? 1.00000 ? ?
H1343b .94462 .63413 .09264 .24900 Uiso ? ? 1.00000 ? ?
H1343c .88184 .65687 .08216 .24900 Uiso ? ? 1.00000 ? ?
H1344a .81228 .58018 .04775 .30100 Uiso ? ? 1.00000 ? ?
H1344b .77382 .60263 .08219 .30100 Uiso ? ? 1.00000 ? ?
H1344c .79508 .55883 .09074 .30100 Uiso ? ? 1.00000 ? ?
H135 .88284 .54922 .17442 .11500 Uiso ? ? 1.00000 ? ?
H13a .82901 .71076 .20279 .10600 Uiso ? ? 1.00000 ? ?
H13b .82087 .69642 .25054 .10600 Uiso ? ? 1.00000 ? ?
H143 .56210 .72224 .19298 .13700 Uiso ? ? 1.00000 ? ?
H1442a .65742 .73870 .05262 .25100 Uiso ? ? .50000 ? ?
H1442b .66224 .69758 .07601 .25100 Uiso ? ? .50000 ? ?
H1442c .71102 .73090 .08792 .25100 Uiso ? ? .50000 ? ?
H1443a .55574 .73180 .07235 .19800 Uiso ? ? .50000 ? ?
H1443b .53765 .72945 .12099 .19800 Uiso ? ? .50000 ? ?
H1443c .57355 .69430 .10015 .19800 Uiso ? ? .50000 ? ?
H1444a .60645 .79127 .08368 .43400 Uiso ? ? .50000 ? ?
H1444b .66252 .79485 .11797 .43400 Uiso ? ? .50000 ? ?
H1444c .59371 .79225 .13333 .43400 Uiso ? ? .50000 ? ?
H1442'a .62985 .72053 .05156 .25100 Uiso ? ? .50000 ? ?
H1442'b .62141 .68619 .08495 .25100 Uiso ? ? .50000 ? ?
H1442'c .68714 .70607 .08086 .25100 Uiso ? ? .50000 ? ?
H1443'a .55057 .77092 .08971 .13600 Uiso ? ? .50000 ? ?
H1443'b .55784 .77293 .14046 .13600 Uiso ? ? .50000 ? ?
H1443'c .53221 .73437 .11773 .13600 Uiso ? ? .50000 ? ?
H1444'a .65248 .78899 .07996 .43400 Uiso ? ? .50000 ? ?
H1444'b .70921 .76902 .10541 .43400 Uiso ? ? .50000 ? ?
H1444'c .66138 .79470 .13029 .43400 Uiso ? ? .50000 ? ?
H145 .74626 .71738 .15068 .12600 Uiso ? ? 1.00000 ? ?
H14a .59716 .68391 .29776 .09100 Uiso ? ? 1.00000 ? ?
H14b .54427 .68275 .26091 .09100 Uiso ? ? 1.00000 ? ?
H153 .48469 .83159 .33407 .09400 Uiso ? ? 1.00000 ? ?
H1542a .40985 .84294 .20278 .38200 Uiso ? ? 1.00000 ? ?
H1542b .45511 .80659 .20031 .38200 Uiso ? ? 1.00000 ? ?
H1542c .47963 .84668 .22018 .38200 Uiso ? ? 1.00000 ? ?
H1543a .33598 .80449 .23750 .39400 Uiso ? ? 1.00000 ? ?
H1543b .35500 .78220 .28068 .39400 Uiso ? ? 1.00000 ? ?
H1543c .37943 .76717 .23642 .39400 Uiso ? ? 1.00000 ? ?
H1544a .36485 .86291 .26840 .37100 Uiso ? ? 1.00000 ? ?
H1544b .42962 .86951 .29320 .37100 Uiso ? ? 1.00000 ? ?
H1544c .38119 .83964 .31138 .37100 Uiso ? ? 1.00000 ? ?
H155 .47910 .74718 .24361 .12600 Uiso ? ? 1.00000 ? ?
H15a .59851 .78471 .40316 .08900 Uiso ? ? 1.00000 ? ?
H15b .55833 .82338 .39823 .08900 Uiso ? ? 1.00000 ? ?
H163 .78713 .89857 .37617 .11700 Uiso ? ? 1.00000 ? ?
H1642a .71043 .99184 .35818 .34400 Uiso ? ? 1.00000 ? ?
H1642b .75771 .95898 .37429 .34400 Uiso ? ? 1.00000 ? ?
H1642c .69387 .96413 .39678 .34400 Uiso ? ? 1.00000 ? ?
H1643a .62118 .97494 .31499 .32400 Uiso ? ? 1.00000 ? ?
H1643b .59607 .94713 .35099 .32400 Uiso ? ? 1.00000 ? ?
H1643c .60642 .93046 .30443 .32400 Uiso ? ? 1.00000 ? ?
H1644a .72729 .96525 .28558 .32200 Uiso ? ? 1.00000 ? ?
H1644b .71585 .91997 .27763 .32200 Uiso ? ? 1.00000 ? ?
H1644c .77206 .93402 .30819 .32200 Uiso ? ? 1.00000 ? ?
H165 .60149 .87629 .34975 .10300 Uiso ? ? 1.00000 ? ?
H16a .81796 .80270 .42258 .10500 Uiso ? ? 1.00000 ? ?
H16b .83985 .84682 .42724 .10500 Uiso ? ? 1.00000 ? ?
H173 .89489 .88000 .36813 .11000 Uiso ? ? 1.00000 ? ?
H1742a 1.03240 .93096 .32658 .15500 Uiso ? ? .50000 ? ?
H1742b 1.04548 .88990 .34880 .15500 Uiso ? ? .50000 ? ?
H1742c .98552 .91405 .35959 .15500 Uiso ? ? .50000 ? ?
H1743a .94980 .93930 .27320 .19000 Uiso ? ? .50000 ? ?
H1743b .90225 .92333 .30627 .19000 Uiso ? ? .50000 ? ?
H1743c .90543 .90389 .26028 .19000 Uiso ? ? .50000 ? ?
H1744a 1.04111 .90007 .25803 .11600 Uiso ? ? .50000 ? ?
H1744b .99532 .86597 .24313 .11600 Uiso ? ? .50000 ? ?
H1744c 1.04926 .85766 .27805 .11600 Uiso ? ? .50000 ? ?
H1742'a 1.06870 .90268 .29462 .16100 Uiso ? ? .50000 ? ?
H1742'b 1.05728 .85704 .28983 .16100 Uiso ? ? .50000 ? ?
H1742'c 1.05899 .87671 .33590 .16100 Uiso ? ? .50000 ? ?
H1743'a .97789 .91050 .23690 .14000 Uiso ? ? .50000 ? ?
H1743'b .91178 .89383 .24731 .14000 Uiso ? ? .50000 ? ?
H1743'c .96603 .86473 .23652 .14000 Uiso ? ? .50000 ? ?
H1744'a .98821 .94443 .31260 .19000 Uiso ? ? .50000 ? ?
H1744'b .97578 .91968 .35433 .19000 Uiso ? ? .50000 ? ?
H1744'c .92065 .92874 .32057 .19000 Uiso ? ? .50000 ? ?
H175 .98054 .80857 .27716 .10400 Uiso ? ? 1.00000 ? ?
H17a .89097 .72238 .30090 .07800 Uiso ? ? 1.00000 ? ?
H17b .92645 .74318 .26377 .07800 Uiso ? ? 1.00000 ? ?
H213 .44389 .77890 .57170 .12700 Uiso ? ? 1.00000 ? ?
H2142a .42950 .69100 .68851 .09600 Uiso ? ? .50000 ? ?
H2142b .49667 .68847 .67026 .09600 Uiso ? ? .50000 ? ?
H2142c .44102 .66517 .64741 .09600 Uiso ? ? .50000 ? ?
H2143a .34377 .73357 .64880 .10600 Uiso ? ? .50000 ? ?
H2143b .34955 .71212 .60409 .10600 Uiso ? ? .50000 ? ?
H2143c .36333 .75755 .60805 .10600 Uiso ? ? .50000 ? ?
H2144a .44132 .76671 .68607 .17700 Uiso ? ? .50000 ? ?
H2144b .45943 .78545 .64185 .17700 Uiso ? ? .50000 ? ?
H2144c .50811 .75946 .66857 .17700 Uiso ? ? .50000 ? ?
H2142'a .37206 .68476 .65555 .24300 Uiso ? ? .50000 ? ?
H2142'b .42584 .66314 .63199 .24300 Uiso ? ? .50000 ? ?
H2142'c .37399 .68625 .60482 .24300 Uiso ? ? .50000 ? ?
H2143'a .37219 .75106 .66564 .17500 Uiso ? ? .50000 ? ?
H2143'b .36159 .75191 .61504 .17500 Uiso ? ? .50000 ? ?
H2143'c .41232 .77933 .63771 .17500 Uiso ? ? .50000 ? ?
H2144'a .46297 .71621 .69888 .17700 Uiso ? ? .50000 ? ?
H2144'b .51019 .74300 .67480 .17700 Uiso ? ? .50000 ? ?
H2144'c .51141 .69700 .66851 .17700 Uiso ? ? .50000 ? ?
H215 .51636 .66892 .60188 .11200 Uiso ? ? 1.00000 ? ?
H21a .53732 .79818 .48488 .09800 Uiso ? ? 1.00000 ? ?
H21b .48533 .81567 .51362 .09800 Uiso ? ? 1.00000 ? ?
H223 .31437 .76266 .37665 .12800 Uiso ? ? 1.00000 ? ?
H2242a .21498 .85187 .39667 .17500 Uiso ? ? .50000 ? ?
H2242b .25943 .82305 .37277 .17500 Uiso ? ? .50000 ? ?
H2242c .28722 .86003 .39751 .17500 Uiso ? ? .50000 ? ?
H2243a .21513 .83960 .48606 .12200 Uiso ? ? .50000 ? ?
H2243b .28456 .85458 .48649 .12200 Uiso ? ? .50000 ? ?
H2243c .26975 .81180 .50274 .12200 Uiso ? ? .50000 ? ?
H2244a .17491 .78964 .43682 .23900 Uiso ? ? .50000 ? ?
H2244b .22714 .76207 .45746 .23900 Uiso ? ? .50000 ? ?
H2244c .22033 .76699 .40694 .23900 Uiso ? ? .50000 ? ?
H2242'a .19830 .83578 .39380 .17500 Uiso ? ? .50000 ? ?
H2242'b .22521 .79422 .38192 .17500 Uiso ? ? .50000 ? ?
H2242'c .26477 .83250 .37457 .17500 Uiso ? ? .50000 ? ?
H2243'a .23643 .87034 .45972 .21900 Uiso ? ? .50000 ? ?
H2243'b .30215 .87199 .43916 .21900 Uiso ? ? .50000 ? ?
H2243'c .29562 .85370 .48545 .12200 Uiso ? ? .50000 ? ?
H2244'a .18157 .80457 .46916 .23900 Uiso ? ? .50000 ? ?
H2244'b .24127 .78918 .49529 .23900 Uiso ? ? .50000 ? ?
H2244'c .21470 .76566 .45473 .23900 Uiso ? ? .50000 ? ?
H225 .38423 .82172 .48756 .15000 Uiso ? ? 1.00000 ? ?
H22a .45235 .72301 .34700 .09500 Uiso ? ? 1.00000 ? ?
H22b .37977 .72107 .33743 .09500 Uiso ? ? 1.00000 ? ?
H233 .40162 .57834 .44130 .20000 Uiso ? ? 1.00000 ? ?
H2342a .23485 .58289 .46596 .31600 Uiso ? ? .50000 ? ?
H2342b .26803 .62424 .46806 .31600 Uiso ? ? .50000 ? ?
H2342c .30727 .58554 .47603 .31600 Uiso ? ? .50000 ? ?
H2343a .19408 .59694 .38606 .14300 Uiso ? ? .50000 ? ?
H2343b .24216 .61636 .35556 .14300 Uiso ? ? .50000 ? ?
H2343c .22177 .63888 .39706 .14300 Uiso ? ? .50000 ? ?
H2344a .25599 .53560 .39283 .25700 Uiso ? ? .50000 ? ?
H2344b .32459 .53649 .41300 .25700 Uiso ? ? .50000 ? ?
H2344c .31090 .55082 .36518 .25700 Uiso ? ? .50000 ? ?
H2342'a .24188 .55480 .45099 .31600 Uiso ? ? .50000 ? ?
H2342'b .29231 .58087 .47594 .31600 Uiso ? ? .50000 ? ?
H2342'c .31330 .54601 .44639 .31600 Uiso ? ? .50000 ? ?
H2343'a .19211 .61193 .42445 .17100 Uiso ? ? .50000 ? ?
H2343'b .22564 .64316 .39593 .17100 Uiso ? ? .50000 ? ?
H2343'c .24241 .64044 .44584 .17100 Uiso ? ? .50000 ? ?
H2344'a .23960 .55755 .36596 .25700 Uiso ? ? .50000 ? ?
H2344'b .31275 .55513 .36482 .25700 Uiso ? ? .50000 ? ?
H2344'c .27704 .59152 .34418 .25700 Uiso ? ? .50000 ? ?
H235 .31604 .66930 .37259 .14800 Uiso ? ? 1.00000 ? ?
H23a .51170 .59153 .47273 .10800 Uiso ? ? 1.00000 ? ?
H23b .55240 .62303 .44953 .10800 Uiso ? ? 1.00000 ? ?
H243 .61379 .48637 .35439 .12300 Uiso ? ? 1.00000 ? ?
H2442a .45580 .43014 .44246 .16800 Uiso ? ? .50000 ? ?
H2442b .43221 .46930 .41997 .16800 Uiso ? ? .50000 ? ?
H2442c .47735 .47122 .46137 .16800 Uiso ? ? .50000 ? ?
H2443a .51093 .40975 .35707 .08600 Uiso ? ? .50000 ? ?
H2443b .55367 .44335 .33963 .08600 Uiso ? ? .50000 ? ?
H2443c .48114 .44978 .34090 .08600 Uiso ? ? .50000 ? ?
H2444a .56615 .40720 .43739 .15700 Uiso ? ? .50000 ? ?
H2444b .59106 .44726 .45708 .15700 Uiso ? ? .50000 ? ?
H2444c .61597 .43183 .41314 .15700 Uiso ? ? .50000 ? ?
H2442'a .43893 .43027 .40442 .15900 Uiso ? ? .50000 ? ?
H2442'b .44077 .46735 .37399 .15900 Uiso ? ? .50000 ? ?
H2442'c .43897 .47291 .42438 .15900 Uiso ? ? .50000 ? ?
H2443'a .53838 .40324 .37959 .16900 Uiso ? ? .50000 ? ?
H2443'b .59792 .43024 .37858 .16900 Uiso ? ? .50000 ? ?
H2443'c .54114 .43767 .34567 .16900 Uiso ? ? .50000 ? ?
H2444'a .53129 .41782 .45845 .15700 Uiso ? ? .50000 ? ?
H2444'b .52980 .46229 .47276 .15700 Uiso ? ? .50000 ? ?
H2444'c .59155 .44399 .45586 .15700 Uiso ? ? .50000 ? ?
H245 .49104 .52722 .44334 .11700 Uiso ? ? 1.00000 ? ?
H24a .68693 .58243 .32354 .09100 Uiso ? ? 1.00000 ? ?
H24b .66917 .54166 .30213 .09100 Uiso ? ? 1.00000 ? ?
H253 .89297 .49016 .39843 .09000 Uiso ? ? 1.00000 ? ?
H2542a .78287 .38348 .33118 .22600 Uiso ? ? 1.00000 ? ?
H2542b .76531 .42164 .30446 .22600 Uiso ? ? 1.00000 ? ?
H2542c .73482 .41382 .34895 .22600 Uiso ? ? 1.00000 ? ?
H2543a .85456 .38832 .39546 .30800 Uiso ? ? 1.00000 ? ?
H2543b .81285 .41901 .41903 .30800 Uiso ? ? 1.00000 ? ?
H2543c .88281 .42913 .41046 .30800 Uiso ? ? 1.00000 ? ?
H2544a .89273 .40124 .32327 .23300 Uiso ? ? 1.00000 ? ?
H2544b .91852 .44258 .33862 .23300 Uiso ? ? 1.00000 ? ?
H2544c .87163 .43966 .29820 .23300 Uiso ? ? 1.00000 ? ?
H255 .72632 .47911 .32623 .09600 Uiso ? ? 1.00000 ? ?
H25a .88706 .59709 .40029 .08100 Uiso ? ? 1.00000 ? ?
H25b .93110 .56046 .40810 .08100 Uiso ? ? 1.00000 ? ?
H263 .86900 .58779 .58525 .08900 Uiso ? ? 1.00000 ? ?
H2642a .98350 .50409 .61424 .20700 Uiso ? ? 1.00000 ? ?
H2642b .96523 .54889 .61020 .20700 Uiso ? ? 1.00000 ? ?
H2642c 1.00530 .52904 .57482 .20700 Uiso ? ? 1.00000 ? ?
H2643a .86880 .48453 .62096 .18000 Uiso ? ? 1.00000 ? ?
H2643b .81771 .50022 .58720 .18000 Uiso ? ? 1.00000 ? ?
H2643c .85226 .52969 .61936 .18000 Uiso ? ? 1.00000 ? ?
H2644a .93173 .45291 .56670 .18700 Uiso ? ? 1.00000 ? ?
H2644b .95686 .47516 .52641 .18700 Uiso ? ? 1.00000 ? ?
H2644c .88548 .46487 .52805 .18700 Uiso ? ? 1.00000 ? ?
H265 .91093 .51932 .48004 .08400 Uiso ? ? 1.00000 ? ?
H26a .82838 .67491 .52151 .07900 Uiso ? ? 1.00000 ? ?
H26b .86216 .66774 .56698 .07900 Uiso ? ? 1.00000 ? ?
H273 .61508 .62956 .61530 .06700 Uiso ? ? 1.00000 ? ?
H2742a .64679 .62364 .72616 .12600 Uiso ? ? .50000 ? ?
H2742b .61023 .62762 .68118 .12600 Uiso ? ? .50000 ? ?
H2742c .65353 .66214 .69842 .12600 Uiso ? ? .50000 ? ?
H2743a .76127 .61136 .73061 .10300 Uiso ? ? .50000 ? ?
H2743b .77538 .64931 .70351 .10300 Uiso ? ? .50000 ? ?
H2743c .79971 .60793 .68865 .10300 Uiso ? ? .50000 ? ?
H2744a .69066 .55785 .69692 .13800 Uiso ? ? .50000 ? ?
H2744b .72734 .55835 .65403 .13800 Uiso ? ? .50000 ? ?
H2744c .65483 .56560 .65228 .13800 Uiso ? ? .50000 ? ?
H2742'a .64298 .58850 .71376 .14600 Uiso ? ? .50000 ? ?
H2742'b .63403 .57500 .66526 .14600 Uiso ? ? .50000 ? ?
H2742'c .60981 .61660 .67947 .14600 Uiso ? ? .50000 ? ?
H2743'a .71034 .64331 .73457 .19000 Uiso ? ? .50000 ? ?
H2743'b .69560 .67310 .69651 .19000 Uiso ? ? .50000 ? ?
H2743'c .76381 .65687 .70469 .19000 Uiso ? ? .50000 ? ?
H2744'a .76107 .57878 .71435 .13800 Uiso ? ? .50000 ? ?
H2744'b .79873 .59838 .67753 .13800 Uiso ? ? .50000 ? ?
H2744'c .75407 .56259 .66676 .13800 Uiso ? ? .50000 ? ?
H275 .80548 .63135 .62331 .07500 Uiso ? ? 1.00000 ? ?
H27a .60552 .65931 .50213 .07900 Uiso ? ? 1.00000 ? ?
H27b .56898 .63264 .53401 .07900 Uiso ? ? 1.00000 ? ?
H101a .74915 .71927 .63262 .30100 Uiso ? ? .49(3) ? ?
H101b .77103 .76063 .65059 .30100 Uiso ? ? .49(3) ? ?
H101c .80113 .74293 .60941 .30100 Uiso ? ? .49(3) ? ?
H102a .61943 .73854 .63065 .28100 Uiso ? ? .49(3) ? ?
H102b .59329 .77677 .60750 .28100 Uiso ? ? .49(3) ? ?
H102c .63431 .78027 .65073 .28100 Uiso ? ? .49(3) ? ?
H101'a .77360 .77278 .62630 .30100 Uiso ? ? .51(3) ? ?
H101'b .79529 .73118 .61027 .30100 Uiso ? ? .51(3) ? ?
H101'c .76019 .73487 .65364 .30100 Uiso ? ? .51(3) ? ?
H102'a .63519 .79375 .62466 .28100 Uiso ? ? .51(3) ? ?
H102'b .62415 .75630 .65328 .28100 Uiso ? ? .51(3) ? ?
H102'c .59017 .76012 .60738 .28100 Uiso ? ? .51(3) ? ?
H201a 1.08668 .78168 .40106 .22500 Uiso ? ? .54(2) ? ?
H201b 1.06397 .82490 .40999 .22500 Uiso ? ? .54(2) ? ?
H201c 1.03773 .80199 .36890 .22500 Uiso ? ? .54(2) ? ?
H202a 1.06154 .77304 .48407 .26700 Uiso ? ? .54(2) ? ?
H202b .99384 .77284 .50165 .26700 Uiso ? ? .54(2) ? ?
H202c 1.02509 .81292 .48899 .26700 Uiso ? ? .54(2) ? ?
H201'a 1.01415 .81492 .39485 .22500 Uiso ? ? .46(2) ? ?
H201'b 1.06252 .78843 .37145 .22500 Uiso ? ? .46(2) ? ?
H201'c 1.08515 .81597 .40992 .22500 Uiso ? ? .46(2) ? ?
H202'a .99371 .80649 .47240 .26700 Uiso ? ? .46(2) ? ?
H202'b 1.05910 .79623 .49460 .26700 Uiso ? ? .46(2) ? ?
H202'c 1.00083 .76959 .50301 .26700 Uiso ? ? .46(2) ? ?
H301a 1.02517 .61516 .51868 .44000 Uiso ? ? .751(16) ? ?
H301b .98206 .64725 .53872 .44000 Uiso ? ? .751(16) ? ?
H301c 1.05490 .64958 .54674 .44000 Uiso ? ? .751(16) ? ?
H302a 1.09274 .68547 .42673 .43600 Uiso ? ? .751(16) ? ?
H302b 1.13261 .67787 .46847 .43600 Uiso ? ? .751(16) ? ?
H302c 1.09158 .68398 .42561 .43600 Uiso ? ? .751(16) ? ?
H301'a 1.03209 .66999 .53065 .13600 Uiso ? ? .249(16) ? ?
H301'b 1.04733 .62658 .54552 .13600 Uiso ? ? .249(16) ? ?
H301'c .97838 .63848 .53180 .13600 Uiso ? ? .249(16) ? ?
H302'a 1.08772 .69547 .45404 .43600 Uiso ? ? .249(16) ? ?
H302'b 1.09525 .66076 .42097 .43600 Uiso ? ? .249(16) ? ?
H302'c 1.13931 .66315 .46290 .43600 Uiso ? ? .249(16) ? ?
H401a .74936 .55001 .54318 .14200 Uiso ? ? .691(12) ? ?
H401b .69127 .52606 .55804 .14200 Uiso ? ? .691(12) ? ?
H401c .69085 .57240 .55983 .14200 Uiso ? ? .691(12) ? ?
H402a .75744 .51644 .46618 .08900 Uiso ? ? .691(12) ? ?
H402b .69842 .51009 .43495 .14600 Uiso ? ? .691(12) ? ?
H402c .70503 .48667 .47878 .14600 Uiso ? ? .691(12) ? ?
H401'a .65971 .55189 .54144 .14200 Uiso ? ? .309(12) ? ?
H401'b .72121 .57146 .56094 .14200 Uiso ? ? .309(12) ? ?
H401'c .71590 .52528 .55797 .14200 Uiso ? ? .309(12) ? ?
H402'a .66899 .50646 .46515 .14600 Uiso ? ? .309(12) ? ?
H402'b .73563 .48843 .47523 .14600 Uiso ? ? .309(12) ? ?
H402'c .72446 .51702 .43562 .14600 Uiso ? ? .309(12) ? ?
H501a .67801 .79749 .22158 .18000 Uiso ? ? .692(13) ? ?
H501b .65734 .83929 .23766 .18000 Uiso ? ? .692(13) ? ?
H501c .63611 .80112 .26184 .18000 Uiso ? ? .692(13) ? ?
H502a .79277 .80901 .22834 .08400 Uiso ? ? .692(13) ? ?
H502b .82778 .82896 .26836 .31000 Uiso ? ? .692(13) ? ?
H502c .78030 .85358 .23907 .31000 Uiso ? ? .692(13) ? ?
H501'a .66023 .82694 .27277 .18000 Uiso ? ? .308(13) ? ?
H501'b .64082 .79143 .24238 .18000 Uiso ? ? .308(13) ? ?
H501'c .66524 .83086 .22240 .18000 Uiso ? ? .308(13) ? ?
H502'a .77586 .84542 .27362 .14400 Uiso ? ? .308(13) ? ?
H502'b .78370 .84075 .22359 .31000 Uiso ? ? .308(13) ? ?
H502'c .83256 .82145 .25658 .31000 Uiso ? ? .308(13) ? ?
H601a .67316 .89541 .46153 .40700 Uiso ? ? .50000 ? ?
H601b .74143 .87866 .46715 .40700 Uiso ? ? .50000 ? ?
H601c .71765 .91007 .50000 .40700 Uiso ? ? .50000 ? ?
H602a .57235 .87135 .52133 .33500 Uiso ? ? .50000 ? ?
H602b .61206 .88503 .56259 .33500 Uiso ? ? .50000 ? ?
H602c .58772 .84136 .55908 .33500 Uiso ? ? .50000 ? ?
H601'a .73447 .88715 .50707 .40700 Uiso ? ? .50000 ? ?
H601'b .68869 .91388 .47882 .40700 Uiso ? ? .50000 ? ?
H601'c .72755 .88075 .45675 .40700 Uiso ? ? .50000 ? ?
H602'a .63422 .86207 .56660 .33500 Uiso ? ? .50000 ? ?
H602'b .57084 .84441 .54782 .33500 Uiso ? ? .50000 ? ?
H602'c .58551 .88946 .54175 .33500 Uiso ? ? .50000 ? ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_oxidation_number
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O ? 0 120 .008 .006 'Int Tables Vol IV Tables 2.2B and 2.3.1'
N ? 0 16 .004 .003 'Int Tables Vol IV Tables 2.2B and 2.3.1'
C ? 0 700 .002 .002 'Int Tables Vol IV Tables 2.2B and 2.3.1'
H ? 0 992 0 0 'Int Tables Vol IV Tables 2.2B and 2.3.1'
Eu ? 0 16 -.542 3.669 'Int Tables Vol IV Tables 2.2B and 2.3.1'
Cl ? 0 0 .132 .159 'Int Tables Vol IV Tables 2.2B and 2.3.1'
S ? 0 24 .11 .124 'Int Tables Vol IV Tables 2.2B and 2.3.1'
loop_
_diffrn_attenuator_code
_diffrn_attenuator_scale
? ?
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
? ? ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Eu2 Eu1 Eu4 . . . 60.24(4) ?
Eu2 Eu1 O2 . . . 40.0(3) ?
Eu2 Eu1 C0 . . . 71.5(5) ?
Eu2 Eu1 O101 . . . 49.8(3) ?
Eu2 Eu1 O102 . . . 93.0(4) ?
Eu2 Eu1 O111 . . . 108.8(4) ?
Eu2 Eu1 O171 . . . 98.3(3) ?
Eu2 Eu1 O261 . . . 36.3(3) ?
Eu2 Eu1 O20 . . . 167.7(4) ?
Eu2 Eu1 O30 . . . 108.9(4) ?
Eu4 Eu1 O2 . . . 37.2(3) ?
Eu4 Eu1 C0 . . . 70.8(5) ?
Eu4 Eu1 O101 . . . 47.3(3) ?
Eu4 Eu1 O102 . . . 95.4(4) ?
Eu4 Eu1 O111 . . . 98.6(4) ?
Eu4 Eu1 O171 . . . 38.3(3) ?
Eu4 Eu1 O261 . . . 96.3(3) ?
Eu4 Eu1 O20 . . . 116.5(4) ?
Eu4 Eu1 O30 . . . 169.1(4) ?
O2 Eu1 C0 . . . 93.4(6) ?
O2 Eu1 O101 . . . 65.4(5) ?
O2 Eu1 O102 . . . 120.3(5) ?
O2 Eu1 O111 . . . 80.6(5) ?
O2 Eu1 O171 . . . 70.5(5) ?
O2 Eu1 O261 . . . 72.0(5) ?
O2 Eu1 O20 . . . 144.7(5) ?
O2 Eu1 O30 . . . 134.0(5) ?
C0 Eu1 O101 . . . 28.0(6) ?
C0 Eu1 O102 . . . 27.0(6) ?
C0 Eu1 O111 . . . 168.0(6) ?
C0 Eu1 O171 . . . 77.9(6) ?
C0 Eu1 O261 . . . 78.5(6) ?
C0 Eu1 O20 . . . 96.2(6) ?
C0 Eu1 O30 . . . 107.6(7) ?
O101 Eu1 O102 . . . 55.0(5) ?
O101 Eu1 O111 . . . 144.3(5) ?
O101 Eu1 O171 . . . 69.2(5) ?
O101 Eu1 O261 . . . 71.4(5) ?
O101 Eu1 O20 . . . 118.6(5) ?
O101 Eu1 O30 . . . 127.4(6) ?
O102 Eu1 O111 . . . 157.8(5) ?
O102 Eu1 O171 . . . 90.2(5) ?
O102 Eu1 O261 . . . 86.2(6) ?
O102 Eu1 O20 . . . 75.2(6) ?
O102 Eu1 O30 . . . 85.6(6) ?
O111 Eu1 O171 . . . 90.2(5) ?
O111 Eu1 O261 . . . 109.1(5) ?
O111 Eu1 O20 . . . 83.2(6) ?
O111 Eu1 O30 . . . 83.9(6) ?
O171 Eu1 O261 . . . 133.9(5) ?
O171 Eu1 O20 . . . 78.5(5) ?
O171 Eu1 O30 . . . 152.6(5) ?
O261 Eu1 O20 . . . 143.2(5) ?
O261 Eu1 O30 . . . 72.9(5) ?
O20 Eu1 O30 . . . 74.3(6) ?
Eu1 Eu2 Eu3 . . . 82.37(4) ?
Eu1 Eu2 Eu4 . . . 59.73(3) ?
Eu1 Eu2 O1 . . . 92.2(4) ?
Eu1 Eu2 O2 . . . 40.0(3) ?
Eu1 Eu2 O101 . . . 41.1(3) ?
Eu1 Eu2 O241 . . . 139.8(3) ?
Eu1 Eu2 O251 . . . 86.6(4) ?
Eu1 Eu2 O261 . . . 38.4(4) ?
Eu1 Eu2 O271 . . . 97.4(3) ?
Eu1 Eu2 O40 . . . 141.2(4) ?
Eu3 Eu2 Eu4 . . . 59.86(4) ?
Eu3 Eu2 O1 . . . 38.0(3) ?
Eu3 Eu2 O2 . . . 91.3(3) ?
Eu3 Eu2 O101 . . . 41.3(3) ?
Eu3 Eu2 O241 . . . 103.9(3) ?
Eu3 Eu2 O251 . . . 159.0(4) ?
Eu3 Eu2 O261 . . . 98.6(4) ?
Eu3 Eu2 O271 . . . 38.7(3) ?
Eu3 Eu2 O40 . . . 113.9(4) ?
Eu4 Eu2 O1 . . . 39.0(4) ?
Eu4 Eu2 O2 . . . 36.9(3) ?
Eu4 Eu2 O101 . . . 46.7(3) ?
Eu4 Eu2 O241 . . . 88.7(3) ?
Eu4 Eu2 O251 . . . 99.1(4) ?
Eu4 Eu2 O261 . . . 97.9(4) ?
Eu4 Eu2 O271 . . . 98.2(3) ?
Eu4 Eu2 O40 . . . 159.0(4) ?
O1 Eu2 O2 . . . 75.7(5) ?
O1 Eu2 O101 . . . 59.3(4) ?
O1 Eu2 O241 . . . 72.9(4) ?
O1 Eu2 O251 . . . 125.4(5) ?
O1 Eu2 O261 . . . 125.0(5) ?
O1 Eu2 O271 . . . 72.4(5) ?
O1 Eu2 O40 . . . 122.8(6) ?
O2 Eu2 O101 . . . 59.3(4) ?
O2 Eu2 O241 . . . 99.7(5) ?
O2 Eu2 O251 . . . 69.0(5) ?
O2 Eu2 O261 . . . 74.0(5) ?
O2 Eu2 O271 . . . 124.4(5) ?
O2 Eu2 O40 . . . 154.7(5) ?
O101 Eu2 O241 . . . 130.7(4) ?
O101 Eu2 O251 . . . 124.8(5) ?
O101 Eu2 O261 . . . 65.8(5) ?
O101 Eu2 O271 . . . 65.3(5) ?
O101 Eu2 O40 . . . 143.2(5) ?
O241 Eu2 O251 . . . 73.7(5) ?
O241 Eu2 O261 . . . 156.8(5) ?
O241 Eu2 O271 . . . 112.4(5) ?
O241 Eu2 O40 . . . 73.0(5) ?
O251 Eu2 O261 . . . 83.2(5) ?
O251 Eu2 O271 . . . 161.7(5) ?
O251 Eu2 O40 . . . 85.7(6) ?
O261 Eu2 O271 . . . 88.8(5) ?
O261 Eu2 O40 . . . 102.9(6) ?
O271 Eu2 O40 . . . 80.0(5) ?
Eu2 Eu3 Eu4 . . . 60.22(4) ?
Eu2 Eu3 O1 . . . 37.1(3) ?
Eu2 Eu3 C0 . . . 71.0(5) ?
Eu2 Eu3 O101 . . . 49.8(3) ?
Eu2 Eu3 O103 . . . 95.0(4) ?
Eu2 Eu3 O161 . . . 96.0(4) ?
Eu2 Eu3 O211 . . . 98.3(4) ?
Eu2 Eu3 O271 . . . 36.2(3) ?
Eu2 Eu3 O10 . . . 115.9(5) ?
Eu2 Eu3 O60 . . . 167.8(5) ?
Eu4 Eu3 O1 . . . 39.6(4) ?
Eu4 Eu3 C0 . . . 70.3(5) ?
Eu4 Eu3 O101 . . . 47.3(3) ?
Eu4 Eu3 O103 . . . 93.3(4) ?
Eu4 Eu3 O161 . . . 35.9(4) ?
Eu4 Eu3 O211 . . . 110.5(4) ?
Eu4 Eu3 O271 . . . 96.1(3) ?
Eu4 Eu3 O10 . . . 167.9(5) ?
Eu4 Eu3 O60 . . . 107.8(5) ?
O1 Eu3 C0 . . . 92.4(6) ?
O1 Eu3 O101 . . . 65.0(5) ?
O1 Eu3 O103 . . . 119.8(5) ?
O1 Eu3 O161 . . . 71.4(5) ?
O1 Eu3 O211 . . . 81.9(5) ?
O1 Eu3 O271 . . . 69.3(5) ?
O1 Eu3 O10 . . . 144.3(6) ?
O1 Eu3 O60 . . . 132.2(6) ?
C0 Eu3 O101 . . . 27.5(6) ?
C0 Eu3 O103 . . . 27.3(6) ?
C0 Eu3 O161 . . . 76.8(6) ?
C0 Eu3 O211 . . . 167.6(6) ?
C0 Eu3 O271 . . . 76.9(6) ?
C0 Eu3 O10 . . . 97.6(7) ?
C0 Eu3 O60 . . . 108.3(6) ?
O101 Eu3 O103 . . . 54.7(5) ?
O101 Eu3 O161 . . . 67.4(5) ?
O101 Eu3 O211 . . . 145.8(5) ?
O101 Eu3 O271 . . . 70.3(5) ?
O101 Eu3 O10 . . . 120.9(6) ?
O101 Eu3 O60 . . . 124.9(6) ?
O103 Eu3 O161 . . . 86.7(5) ?
O103 Eu3 O211 . . . 156.1(6) ?
O103 Eu3 O271 . . . 88.4(5) ?
O103 Eu3 O10 . . . 75.3(6) ?
O103 Eu3 O60 . . . 87.7(6) ?
O161 Eu3 O211 . . . 111.4(5) ?
O161 Eu3 O271 . . . 131.1(5) ?
O161 Eu3 O10 . . . 144.2(6) ?
O161 Eu3 O60 . . . 72.3(6) ?
O211 Eu3 O271 . . . 90.8(5) ?
O211 Eu3 O10 . . . 81.1(6) ?
O211 Eu3 O60 . . . 83.5(6) ?
O271 Eu3 O10 . . . 79.8(6) ?
O271 Eu3 O60 . . . 156.0(6) ?
O10 Eu3 O60 . . . 76.3(6) ?
Eu1 Eu4 Eu2 . . . 60.02(3) ?
Eu1 Eu4 Eu3 . . . 82.55(4) ?
Eu1 Eu4 O1 . . . 90.9(3) ?
Eu1 Eu4 O2 . . . 39.6(3) ?
Eu1 Eu4 O101 . . . 41.2(3) ?
Eu1 Eu4 O141 . . . 104.4(3) ?
Eu1 Eu4 O151 . . . 159.4(5) ?
Eu1 Eu4 O161 . . . 98.0(4) ?
Eu1 Eu4 O171 . . . 39.1(3) ?
Eu1 Eu4 O50 . . . 113.5(4) ?
Eu2 Eu4 Eu3 . . . 59.92(4) ?
Eu2 Eu4 O1 . . . 37.2(3) ?
Eu2 Eu4 O2 . . . 39.2(4) ?
Eu2 Eu4 O101 . . . 49.3(3) ?
Eu2 Eu4 O141 . . . 89.2(3) ?
Eu2 Eu4 O151 . . . 99.5(4) ?
Eu2 Eu4 O161 . . . 96.6(4) ?
Eu2 Eu4 O171 . . . 99.0(3) ?
Eu2 Eu4 O50 . . . 159.1(4) ?
Eu3 Eu4 O1 . . . 38.6(3) ?
Eu3 Eu4 O2 . . . 93.4(4) ?
Eu3 Eu4 O101 . . . 41.4(3) ?
Eu3 Eu4 O141 . . . 140.1(3) ?
Eu3 Eu4 O151 . . . 85.3(5) ?
Eu3 Eu4 O161 . . . 36.9(4) ?
Eu3 Eu4 O171 . . . 99.1(4) ?
Eu3 Eu4 O50 . . . 140.9(4) ?
O1 Eu4 O2 . . . 76.2(5) ?
O1 Eu4 O101 . . . 60.2(4) ?
O1 Eu4 O141 . . . 101.6(5) ?
O1 Eu4 O151 . . . 69.4(6) ?
O1 Eu4 O161 . . . 71.4(5) ?
O1 Eu4 O171 . . . 124.8(5) ?
O1 Eu4 O50 . . . 155.6(5) ?
O2 Eu4 O101 . . . 62.4(5) ?
O2 Eu4 O141 . . . 71.8(5) ?
O2 Eu4 O151 . . . 125.2(5) ?
O2 Eu4 O161 . . . 125.3(5) ?
O2 Eu4 O171 . . . 73.5(5) ?
O2 Eu4 O50 . . . 122.1(6) ?
O101 Eu4 O141 . . . 133.3(4) ?
O101 Eu4 O151 . . . 125.1(6) ?
O101 Eu4 O161 . . . 63.3(5) ?
O101 Eu4 O171 . . . 65.0(5) ?
O101 Eu4 O50 . . . 140.4(5) ?
O141 Eu4 O151 . . . 75.0(6) ?
O141 Eu4 O161 . . . 156.8(5) ?
O141 Eu4 O171 . . . 111.0(5) ?
O141 Eu4 O50 . . . 72.9(5) ?
O151 Eu4 O161 . . . 81.9(6) ?
O151 Eu4 O171 . . . 160.7(5) ?
O151 Eu4 O50 . . . 86.3(6) ?
O161 Eu4 O171 . . . 90.4(5) ?
O161 Eu4 O50 . . . 104.1(6) ?
O171 Eu4 O50 . . . 78.4(6) ?
Eu2 O1 Eu3 . . . 104.9(5) ?
Eu2 O1 Eu4 . . . 103.8(5) ?
Eu3 O1 Eu4 . . . 101.9(5) ?
Eu1 O2 Eu2 . . . 100.0(5) ?
Eu1 O2 Eu4 . . . 103.1(5) ?
Eu2 O2 Eu4 . . . 103.9(5) ?
Eu1 C0 Eu3 . . . 125.2(9) ?
Eu1 C0 O101 . . . 63.3(12) ?
Eu1 C0 O102 . . . 57.9(12) ?
Eu1 C0 O103 . . . 175.3(16) ?
Eu3 C0 O101 . . . 61.9(11) ?
Eu3 C0 O102 . . . 173.1(18) ?
Eu3 C0 O103 . . . 59.4(11) ?
O101 C0 O102 . . . 121(2) ?
O101 C0 O103 . . . 121(2) ?
O102 C0 O103 . . . 118(2) ?
Eu1 O101 Eu2 . . . 89.1(4) ?
Eu1 O101 Eu3 . . . 176.3(7) ?
Eu1 O101 Eu4 . . . 91.5(5) ?
Eu1 O101 C0 . . . 88.6(13) ?
Eu1 O101 O102 . . . 59.8(5) ?
Eu1 O101 O103 . . . 118.0(7) ?
Eu2 O101 Eu3 . . . 88.8(4) ?
Eu2 O101 Eu4 . . . 84.0(4) ?
Eu2 O101 C0 . . . 134.5(13) ?
Eu2 O101 O102 . . . 125.3(7) ?
Eu2 O101 O103 . . . 129.5(7) ?
Eu3 O101 Eu4 . . . 91.4(4) ?
Eu3 O101 C0 . . . 90.6(13) ?
Eu3 O101 O102 . . . 119.3(8) ?
Eu3 O101 O103 . . . 61.3(5) ?
Eu4 O101 C0 . . . 141.5(14) ?
Eu4 O101 O102 . . . 134.9(8) ?
Eu4 O101 O103 . . . 132.0(7) ?
Eu1 O102 C0 . . . 95.1(14) ?
Eu3 O103 C0 . . . 93.3(13) ?
Eu1 O111 C111 . . . 128.6(12) ?
O111 C111 C112 . . . 121.0(19) ?
O111 C111 C116 . . . 121(2) ?
C112 C111 C116 . . . 118(2) ?
C111 C112 C113 . . . 120(2) ?
C111 C112 C11 . . . 118(2) ?
C113 C112 C11 . . . 121(2) ?
C112 C113 C114 . . . 122(2) ?
C112 C113 H113 . . . 119 ?
C114 C113 H113 . . . 119 ?
C113 C114 C1141 . . . 122.6(19) ?
C113 C114 C115 . . . 117(2) ?
C1141 C114 C115 . . . 121(2) ?
C114 C1141 C1142 . . . 106(2) ?
C114 C1141 C1143 . . . 114(2) ?
C114 C1141 C1144 . . . 107(2) ?
C114 C1141 C1142' . . . 111(3) ?
C114 C1141 C1143' . . . 110(2) ?
C114 C1141 C1144' . . . 109(3) ?
C1142 C1141 C1143 . . . 109(3) ?
C1142 C1141 C1144 . . . 108(3) ?
C1143 C1141 C1144 . . . 112(3) ?
C1142' C1141 C1143' . . . 112(3) ?
C1142' C1141 C1144' . . . 110(3) ?
C1143' C1141 C1144' . . . 105(3) ?
C1141 C1142 H1142a . . . 109 ?
C1141 C1142 H1142b . . . 104 ?
C1141 C1142 H1142c . . . 111 ?
H1142a C1142 H1142b . . . 109 ?
H1142a C1142 H1142c . . . 115 ?
H1142b C1142 H1142c . . . 108 ?
C1141 C1143 H1143a . . . 105 ?
C1141 C1143 H1143b . . . 106 ?
C1141 C1143 H1143c . . . 110 ?
H1143a C1143 H1143b . . . 106 ?
H1143a C1143 H1143c . . . 113 ?
H1143b C1143 H1143c . . . 116 ?
C1141 C1144 H1144a . . . 109 ?
C1141 C1144 H1144b . . . 107 ?
C1141 C1144 H1144c . . . 114 ?
H1144a C1144 H1144b . . . 103 ?
H1144a C1144 H1144c . . . 115 ?
H1144b C1144 H1144c . . . 108 ?
C1141 C1142' H1142'a . . . 114 ?
C1141 C1142' H1142'b . . . 107 ?
C1141 C1142' H1142'c . . . 115 ?
H1142'a C1142' H1142'b . . . 103 ?
H1142'a C1142' H1142'c . . . 114 ?
H1142'b C1142' H1142'c . . . 102 ?
C1141 C1143' H1143'a . . . 106 ?
C1141 C1143' H1143'b . . . 103 ?
C1141 C1143' H1143'c . . . 110 ?
H1143'a C1143' H1143'b . . . 108 ?
H1143'a C1143' H1143'c . . . 115 ?
H1143'b C1143' H1143'c . . . 112 ?
C1141 C1144' H1144'a . . . 103 ?
C1141 C1144' H1144'b . . . 101 ?
C1141 C1144' H1144'c . . . 113 ?
H1144'a C1144' H1144'b . . . 100 ?
H1144'a C1144' H1144'c . . . 122 ?
H1144'b C1144' H1144'c . . . 115 ?
C114 C115 C116 . . . 122(2) ?
C114 C115 H115 . . . 117 ?
C116 C115 H115 . . . 121 ?
C111 C116 C115 . . . 121(2) ?
C111 C116 C17 . . . 121(2) ?
C115 C116 C17 . . . 117(2) ?
C112 C11 C126 . . . 117(2) ?
C112 C11 H11a . . . 108 ?
C112 C11 H11b . . . 109 ?
C126 C11 H11a . . . 109 ?
C126 C11 H11b . . . 112 ?
H11a C11 H11b . . . 101 ?
O121 C121 C122 . . . 117(2) ?
O121 C121 C126 . . . 122(2) ?
C122 C121 C126 . . . 121(2) ?
C121 C122 C123 . . . 122(2) ?
C121 C122 C12 . . . 123(2) ?
C123 C122 C12 . . . 115(2) ?
C122 C123 C124 . . . 119(2) ?
C122 C123 H123 . . . 128 ?
C124 C123 H123 . . . 113 ?
C123 C124 C1241 . . . 120(2) ?
C123 C124 C125 . . . 118(2) ?
C1241 C124 C125 . . . 122(2) ?
C124 C1241 C1242 . . . 110(2) ?
C124 C1241 C1243 . . . 108(2) ?
C124 C1241 C1244 . . . 111(2) ?
C1242 C1241 C1243 . . . 110(3) ?
C1242 C1241 C1244 . . . 107(2) ?
C1243 C1241 C1244 . . . 111(3) ?
C1241 C1242 H1242a . . . 113 ?
C1241 C1242 H1242b . . . 112 ?
C1241 C1242 H1242c . . . 113 ?
H1242a C1242 H1242b . . . 106 ?
H1242a C1242 H1242c . . . 105 ?
H1242b C1242 H1242c . . . 106 ?
C1241 C1243 H1243a . . . 110 ?
C1241 C1243 H1243b . . . 110 ?
C1241 C1243 H1243c . . . 109 ?
H1243a C1243 H1243b . . . 108 ?
H1243a C1243 H1243c . . . 110 ?
H1243b C1243 H1243c . . . 110 ?
C1241 C1244 H1244a . . . 107 ?
C1241 C1244 H1244b . . . 106 ?
C1241 C1244 H1244c . . . 110 ?
H1244a C1244 H1244b . . . 108 ?
H1244a C1244 H1244c . . . 111 ?
H1244b C1244 H1244c . . . 115 ?
C124 C125 C126 . . . 122(2) ?
C124 C125 H125 . . . 116 ?
C126 C125 H125 . . . 122 ?
C11 C126 C121 . . . 122(2) ?
C11 C126 C125 . . . 120(2) ?
C121 C126 C125 . . . 118(2) ?
C122 C12 C136 . . . 111(2) ?
C122 C12 H12a . . . 108 ?
C122 C12 H12b . . . 114 ?
C136 C12 H12a . . . 109 ?
C136 C12 H12b . . . 112 ?
H12a C12 H12b . . . 102 ?
O131 C131 C132 . . . 123(2) ?
O131 C131 C136 . . . 121(2) ?
C132 C131 C136 . . . 116(2) ?
C131 C132 C133 . . . 123(2) ?
C131 C132 C13 . . . 121(2) ?
C133 C132 C13 . . . 116(2) ?
C132 C133 C134 . . . 120(2) ?
C132 C133 H133 . . . 122 ?
C134 C133 H133 . . . 118 ?
C133 C134 C1341 . . . 119(2) ?
C133 C134 C135 . . . 117(2) ?
C1341 C134 C135 . . . 125(3) ?
C134 C1341 C1342 . . . 112(3) ?
C134 C1341 C1343 . . . 117(3) ?
C134 C1341 C1344 . . . 110(3) ?
C1342 C1341 C1343 . . . 99(3) ?
C1342 C1341 C1344 . . . 102(3) ?
C1343 C1341 C1344 . . . 115(3) ?
C1341 C1342 H1342a . . . 114 ?
C1341 C1342 H1342b . . . 105 ?
C1341 C1342 H1342c . . . 111 ?
H1342a C1342 H1342b . . . 103 ?
H1342a C1342 H1342c . . . 115 ?
H1342b C1342 H1342c . . . 108 ?
C1341 C1343 H1343a . . . 114 ?
C1341 C1343 H1343b . . . 113 ?
C1341 C1343 H1343c . . . 109 ?
H1343a C1343 H1343b . . . 110 ?
H1343a C1343 H1343c . . . 102 ?
H1343b C1343 H1343c . . . 108 ?
C1341 C1344 H1344a . . . 115 ?
C1341 C1344 H1344b . . . 117 ?
C1341 C1344 H1344c . . . 110 ?
H1344a C1344 H1344b . . . 106 ?
H1344a C1344 H1344c . . . 101 ?
H1344b C1344 H1344c . . . 107 ?
C134 C135 C136 . . . 121(2) ?
C134 C135 H135 . . . 119 ?
C136 C135 H135 . . . 120 ?
C12 C136 C131 . . . 123(2) ?
C12 C136 C135 . . . 115(2) ?
C131 C136 C135 . . . 122(2) ?
C132 C13 C146 . . . 115(2) ?
C132 C13 H13a . . . 113 ?
C132 C13 H13b . . . 110 ?
C146 C13 H13a . . . 110 ?
C146 C13 H13b . . . 107 ?
H13a C13 H13b . . . 101 ?
Eu4 O141 C141 . . . 129.5(14) ?
O141 C141 C142 . . . 121(2) ?
O141 C141 C146 . . . 121(2) ?
C142 C141 C146 . . . 117(2) ?
C141 C142 C143 . . . 120(2) ?
C141 C142 C14 . . . 122(2) ?
C143 C142 C14 . . . 118(2) ?
C142 C143 C144 . . . 122(3) ?
C142 C143 H143 . . . 114 ?
C144 C143 H143 . . . 124 ?
C143 C144 C1441 . . . 123(2) ?
C143 C144 C145 . . . 114(2) ?
C1441 C144 C145 . . . 123(2) ?
C144 C1441 C1442 . . . 113(3) ?
C144 C1441 C1443 . . . 109(3) ?
C144 C1441 C1444 . . . 105(3) ?
C144 C1441 C1442' . . . 110(3) ?
C144 C1441 C1443' . . . 109(3) ?
C144 C1441 C1444' . . . 110(3) ?
C1442 C1441 C1443 . . . 107(4) ?
C1442 C1441 C1444 . . . 110(4) ?
C1443 C1441 C1444 . . . 113(4) ?
C1442' C1441 C1443' . . . 111(3) ?
C1442' C1441 C1444' . . . 108(4) ?
C1443' C1441 C1444' . . . 109(3) ?
C1441 C1442 H1442a . . . 109 ?
C1441 C1442 H1442b . . . 95 ?
C1441 C1442 H1442c . . . 117 ?
H1442a C1442 H1442b . . . 87 ?
H1442a C1442 H1442c . . . 133 ?
H1442b C1442 H1442c . . . 96 ?
C1441 C1443 H1443a . . . 118 ?
C1441 C1443 H1443b . . . 115 ?
C1441 C1443 H1443c . . . 112 ?
H1443a C1443 H1443b . . . 108 ?
H1443a C1443 H1443c . . . 101 ?
H1443b C1443 H1443c . . . 100 ?
C1441 C1444 H1444a . . . 85 ?
C1441 C1444 H1444b . . . 97 ?
C1441 C1444 H1444c . . . 104 ?
H1444a C1444 H1444b . . . 94 ?
H1444a C1444 H1444c . . . 94 ?
H1444b C1444 H1444c . . . 158 ?
C1441 C1442' H1442'a . . . 117 ?
C1441 C1442' H1442'b . . . 121 ?
C1441 C1442' H1442'c . . . 102 ?
H1442'a C1442' H1442'b . . . 113 ?
H1442'a C1442' H1442'c . . . 99 ?
H1442'b C1442' H1442'c . . . 99 ?
C1441 C1443' H1443'a . . . 114 ?
C1441 C1443' H1443'b . . . 118 ?
C1441 C1443' H1443'c . . . 111 ?
H1443'a C1443' H1443'b . . . 112 ?
H1443'a C1443' H1443'c . . . 96 ?
H1443'b C1443' H1443'c . . . 103 ?
C1441 C1444' H1444'a . . . 96 ?
C1441 C1444' H1444'b . . . 102 ?
C1441 C1444' H1444'c . . . 89 ?
H1444'a C1444' H1444'b . . . 133 ?
H1444'a C1444' H1444'c . . . 102 ?
H1444'b C1444' H1444'c . . . 121 ?
C144 C145 C146 . . . 124(3) ?
C144 C145 H145 . . . 113 ?
C146 C145 H145 . . . 123 ?
C13 C146 C141 . . . 126(2) ?
C13 C146 C145 . . . 112(2) ?
C141 C146 C145 . . . 122(2) ?
C142 C14 C156 . . . 112(2) ?
C142 C14 H14a . . . 108 ?
C142 C14 H14b . . . 108 ?
C156 C14 H14a . . . 111 ?
C156 C14 H14b . . . 113 ?
H14a C14 H14b . . . 105 ?
Eu4 O151 C151 . . . 154.2(16) ?
O151 C151 C152 . . . 119(2) ?
O151 C151 C156 . . . 122(2) ?
C152 C151 C156 . . . 119(2) ?
C151 C152 C153 . . . 118(2) ?
C151 C152 C15 . . . 120(2) ?
C153 C152 C15 . . . 122(2) ?
C152 C153 C154 . . . 123(2) ?
C152 C153 H153 . . . 121 ?
C154 C153 H153 . . . 116 ?
C153 C154 C1541 . . . 121(2) ?
C153 C154 C155 . . . 117(2) ?
C1541 C154 C155 . . . 121(2) ?
C154 C1541 C1542 . . . 107(3) ?
C154 C1541 C1543 . . . 110(3) ?
C154 C1541 C1544 . . . 115(3) ?
C1542 C1541 C1543 . . . 110(4) ?
C1542 C1541 C1544 . . . 109(4) ?
C1543 C1541 C1544 . . . 106(4) ?
C1541 C1542 H1542a . . . 113 ?
C1541 C1542 H1542b . . . 115 ?
C1541 C1542 H1542c . . . 117 ?
H1542a C1542 H1542b . . . 104 ?
H1542a C1542 H1542c . . . 103 ?
H1542b C1542 H1542c . . . 103 ?
C1541 C1543 H1543a . . . 106 ?
C1541 C1543 H1543b . . . 111 ?
C1541 C1543 H1543c . . . 113 ?
H1543a C1543 H1543b . . . 107 ?
H1543a C1543 H1543c . . . 106 ?
H1543b C1543 H1543c . . . 114 ?
C1541 C1544 H1544a . . . 117 ?
C1541 C1544 H1544b . . . 119 ?
C1541 C1544 H1544c . . . 110 ?
H1544a C1544 H1544b . . . 106 ?
H1544a C1544 H1544c . . . 102 ?
H1544b C1544 H1544c . . . 100 ?
C154 C155 C156 . . . 122(3) ?
C154 C155 H155 . . . 115 ?
C156 C155 H155 . . . 123 ?
C14 C156 C151 . . . 118(2) ?
C14 C156 C155 . . . 122(2) ?
C151 C156 C155 . . . 120(2) ?
C152 C15 C166 . . . 117(2) ?
C152 C15 H15a . . . 108 ?
C152 C15 H15b . . . 112 ?
C166 C15 H15a . . . 105 ?
C166 C15 H15b . . . 106 ?
H15a C15 H15b . . . 107 ?
Eu3 O161 Eu4 . . . 107.2(5) ?
Eu3 O161 C161 . . . 141.5(14) ?
Eu4 O161 C161 . . . 110.6(13) ?
O161 C161 C162 . . . 121(2) ?
O161 C161 C166 . . . 119(2) ?
C162 C161 C166 . . . 119(2) ?
C161 C162 C163 . . . 117(2) ?
C161 C162 C16 . . . 121(2) ?
C163 C162 C16 . . . 122(2) ?
C162 C163 C164 . . . 124(2) ?
C162 C163 H163 . . . 114 ?
C164 C163 H163 . . . 122 ?
C163 C164 C1641 . . . 113(2) ?
C163 C164 C165 . . . 115(2) ?
C1641 C164 C165 . . . 132(3) ?
C164 C1641 C1642 . . . 112(3) ?
C164 C1641 C1643 . . . 105(3) ?
C164 C1641 C1644 . . . 107(3) ?
C1642 C1641 C1643 . . . 115(3) ?
C1642 C1641 C1644 . . . 112(3) ?
C1643 C1641 C1644 . . . 106(3) ?
C1641 C1642 H1642a . . . 101 ?
C1641 C1642 H1642b . . . 101 ?
C1641 C1642 H1642c . . . 106 ?
H1642a C1642 H1642b . . . 116 ?
H1642a C1642 H1642c . . . 110 ?
H1642b C1642 H1642c . . . 119 ?
C1641 C1643 H1643a . . . 111 ?
C1641 C1643 H1643b . . . 111 ?
C1641 C1643 H1643c . . . 119 ?
H1643a C1643 H1643b . . . 101 ?
H1643a C1643 H1643c . . . 110 ?
H1643b C1643 H1643c . . . 103 ?
C1641 C1644 H1644a . . . 108 ?
C1641 C1644 H1644b . . . 115 ?
C1641 C1644 H1644c . . . 106 ?
H1644a C1644 H1644b . . . 108 ?
H1644a C1644 H1644c . . . 108 ?
H1644b C1644 H1644c . . . 111 ?
C164 C165 C166 . . . 126(2) ?
C164 C165 H165 . . . 117 ?
C166 C165 H165 . . . 117 ?
C15 C166 C161 . . . 123(2) ?
C15 C166 C165 . . . 117(2) ?
C161 C166 C165 . . . 120(2) ?
C162 C16 C172 . . . 113(2) ?
C162 C16 H16a . . . 104 ?
C162 C16 H16b . . . 104 ?
C172 C16 H16a . . . 113 ?
C172 C16 H16b . . . 116 ?
H16a C16 H16b . . . 105 ?
Eu1 O171 Eu4 . . . 102.6(5) ?
Eu1 O171 C171 . . . 127.6(13) ?
Eu4 O171 C171 . . . 129.8(13) ?
O171 C171 C172 . . . 121(2) ?
O171 C171 C176 . . . 119.8(19) ?
C172 C171 C176 . . . 118(2) ?
C16 C172 C171 . . . 121(2) ?
C16 C172 C173 . . . 117(2) ?
C171 C172 C173 . . . 122(2) ?
C172 C173 C174 . . . 121(2) ?
C172 C173 H173 . . . 121 ?
C174 C173 H173 . . . 118 ?
C173 C174 C1741 . . . 123(2) ?
C173 C174 C175 . . . 117(2) ?
C1741 C174 C175 . . . 120(2) ?
C174 C1741 C1742 . . . 108(3) ?
C174 C1741 C1743 . . . 106(3) ?
C174 C1741 C1744 . . . 114(2) ?
C174 C1741 C1742' . . . 110(3) ?
C174 C1741 C1743' . . . 106(3) ?
C174 C1741 C1744' . . . 112(3) ?
C1742 C1741 C1743 . . . 110(3) ?
C1742 C1741 C1744 . . . 111(3) ?
C1743 C1741 C1744 . . . 108(3) ?
C1742' C1741 C1743' . . . 109(3) ?
C1742' C1741 C1744' . . . 107(3) ?
C1743' C1741 C1744' . . . 113(3) ?
C1741 C1742 H1742a . . . 111 ?
C1741 C1742 H1742b . . . 122 ?
C1741 C1742 H1742c . . . 107 ?
H1742a C1742 H1742b . . . 112 ?
H1742a C1742 H1742c . . . 96 ?
H1742b C1742 H1742c . . . 105 ?
C1741 C1743 H1743a . . . 107 ?
C1741 C1743 H1743b . . . 112 ?
C1741 C1743 H1743c . . . 104 ?
H1743a C1743 H1743b . . . 113 ?
H1743a C1743 H1743c . . . 107 ?
H1743b C1743 H1743c . . . 112 ?
C1741 C1744 H1744a . . . 107 ?
C1741 C1744 H1744b . . . 115 ?
C1741 C1744 H1744c . . . 101 ?
H1744a C1744 H1744b . . . 124 ?
H1744a C1744 H1744c . . . 98 ?
H1744b C1744 H1744c . . . 109 ?
C1741 C1742' H1742'a . . . 107 ?
C1741 C1742' H1742'b . . . 113 ?
C1741 C1742' H1742'c . . . 101 ?
H1742'a C1742' H1742'b . . . 125 ?
H1742'a C1742' H1742'c . . . 101 ?
H1742'b C1742' H1742'c . . . 108 ?
C1741 C1743' H1743'a . . . 114 ?
C1741 C1743' H1743'b . . . 117 ?
C1741 C1743' H1743'c . . . 107 ?
H1743'a C1743' H1743'b . . . 113 ?
H1743'a C1743' H1743'c . . . 101 ?
H1743'b C1743' H1743'c . . . 103 ?
C1741 C1744' H1744'a . . . 114 ?
C1741 C1744' H1744'b . . . 117 ?
C1741 C1744' H1744'c . . . 108 ?
H1744'a C1744' H1744'b . . . 110 ?
H1744'a C1744' H1744'c . . . 104 ?
H1744'b C1744' H1744'c . . . 104 ?
C174 C175 C176 . . . 122(2) ?
C174 C175 H175 . . . 119 ?
C176 C175 H175 . . . 119 ?
C171 C176 C175 . . . 119(2) ?
C171 C176 C17 . . . 122(2) ?
C175 C176 C17 . . . 119(2) ?
C116 C17 C176 . . . 120(2) ?
C116 C17 H17a . . . 110 ?
C116 C17 H17b . . . 108 ?
C176 C17 H17a . . . 107 ?
C176 C17 H17b . . . 107 ?
H17a C17 H17b . . . 102 ?
Eu3 O211 C211 . . . 132.4(13) ?
O211 C211 C212 . . . 117(2) ?
O211 C211 C216 . . . 126(2) ?
C212 C211 C216 . . . 117(2) ?
C211 C212 C213 . . . 121(2) ?
C211 C212 C21 . . . 120(2) ?
C213 C212 C21 . . . 120(2) ?
C212 C213 C214 . . . 121(3) ?
C212 C213 H213 . . . 118 ?
C214 C213 H213 . . . 121 ?
C213 C214 C2141 . . . 121(2) ?
C213 C214 C215 . . . 120(3) ?
C2141 C214 C215 . . . 118(2) ?
C214 C2141 C2142 . . . 117(2) ?
C214 C2141 C2143 . . . 108(2) ?
C214 C2141 C2144 . . . 105(3) ?
C214 C2141 C2142' . . . 103(3) ?
C214 C2141 C2143' . . . 114(3) ?
C214 C2141 C2144' . . . 112(3) ?
C2142 C2141 C2143 . . . 113(3) ?
C2142 C2141 C2144 . . . 107(3) ?
C2143 C2141 C2144 . . . 106(3) ?
C2142' C2141 C2143' . . . 106(4) ?
C2142' C2141 C2144' . . . 109(4) ?
C2143' C2141 C2144' . . . 112(4) ?
C2141 C2142 H2142a . . . 112 ?
C2141 C2142 H2142b . . . 107 ?
C2141 C2142 H2142c . . . 113 ?
H2142a C2142 H2142b . . . 105 ?
H2142a C2142 H2142c . . . 113 ?
H2142b C2142 H2142c . . . 107 ?
C2141 C2143 H2143a . . . 117 ?
C2141 C2143 H2143b . . . 113 ?
C2141 C2143 H2143c . . . 112 ?
H2143a C2143 H2143b . . . 106 ?
H2143a C2143 H2143c . . . 105 ?
H2143b C2143 H2143c . . . 103 ?
C2141 C2144 H2144a . . . 111 ?
C2141 C2144 H2144b . . . 108 ?
C2141 C2144 H2144c . . . 113 ?
H2144a C2144 H2144b . . . 105 ?
H2144a C2144 H2144c . . . 110 ?
H2144b C2144 H2144c . . . 110 ?
C2141 C2142' H2142'a . . . 108 ?
C2141 C2142' H2142'b . . . 109 ?
C2141 C2142' H2142'c . . . 111 ?
H2142'a C2142' H2142'b . . . 105 ?
H2142'a C2142' H2142'c . . . 110 ?
H2142'b C2142' H2142'c . . . 113 ?
C2141 C2143' H2143'a . . . 111 ?
C2141 C2143' H2143'b . . . 108 ?
C2141 C2143' H2143'c . . . 119 ?
H2143'a C2143' H2143'b . . . 99 ?
H2143'a C2143' H2143'c . . . 110 ?
H2143'b C2143' H2143'c . . . 108 ?
C2141 C2144' H2144'a . . . 113 ?
C2141 C2144' H2144'b . . . 112 ?
C2141 C2144' H2144'c . . . 112 ?
H2144'a C2144' H2144'b . . . 107 ?
H2144'a C2144' H2144'c . . . 106 ?
H2144'b C2144' H2144'c . . . 107 ?
C214 C215 C216 . . . 120(2) ?
C214 C215 H215 . . . 120 ?
C216 C215 H215 . . . 120(3) ?
C211 C216 C215 . . . 121(2) ?
C211 C216 C27 . . . 120(2) ?
C215 C216 C27 . . . 120(2) ?
C212 C21 C226 . . . 116(2) ?
C212 C21 H21a . . . 107 ?
C212 C21 H21b . . . 107 ?
C226 C21 H21a . . . 111 ?
C226 C21 H21b . . . 112 ?
H21a C21 H21b . . . 102 ?
O221 C221 C222 . . . 120(2) ?
O221 C221 C226 . . . 123(2) ?
C222 C221 C226 . . . 117(2) ?
C221 C222 C223 . . . 121(2) ?
C221 C222 C22 . . . 117(2) ?
C223 C222 C22 . . . 122(2) ?
C222 C223 C224 . . . 125(3) ?
C222 C223 H223 . . . 115 ?
C224 C223 H223 . . . 121 ?
C223 C224 C2241 . . . 123(2) ?
C223 C224 C225 . . . 115(3) ?
C2241 C224 C225 . . . 122(3) ?
C224 C2241 C2242 . . . 107(3) ?
C224 C2241 C2243 . . . 114(3) ?
C224 C2241 C2244 . . . 104(3) ?
C224 C2241 C2242' . . . 110(3) ?
C224 C2241 C2243' . . . 106(3) ?
C224 C2241 C2244' . . . 111(3) ?
C2242 C2241 C2243 . . . 114(3) ?
C2242 C2241 C2244 . . . 111(3) ?
C2243 C2241 C2244 . . . 107(3) ?
C2242' C2241 C2243' . . . 106(3) ?
C2242' C2241 C2244' . . . 114(3) ?
C2243' C2241 C2244' . . . 110(4) ?
C2241 C2242 H2242a . . . 114 ?
C2241 C2242 H2242b . . . 105 ?
C2241 C2242 H2242c . . . 114 ?
H2242a C2242 H2242b . . . 102 ?
H2242a C2242 H2242c . . . 114 ?
H2242b C2242 H2242c . . . 106 ?
C2241 C2243 H2243a . . . 115 ?
C2241 C2243 H2243b . . . 117 ?
C2241 C2243 H2243c . . . 105 ?
H2243a C2243 H2243b . . . 113 ?
H2243a C2243 H2243c . . . 99 ?
H2243b C2243 H2243c . . . 105 ?
C2241 C2244 H2244a . . . 110 ?
C2241 C2244 H2244b . . . 111 ?
C2241 C2244 H2244c . . . 112 ?
H2244a C2244 H2244b . . . 105 ?
H2244a C2244 H2244c . . . 106 ?
H2244b C2244 H2244c . . . 112 ?
C2241 C2242' H2242'a . . . 113 ?
C2241 C2242' H2242'b . . . 115 ?
C2241 C2242' H2242'c . . . 105 ?
H2242'a C2242' H2242'b . . . 114 ?
H2242'a C2242' H2242'c . . . 102 ?
H2242'b C2242' H2242'c . . . 108 ?
C2241 C2243' H2243'a . . . 106 ?
C2241 C2243' H2243'b . . . 125 ?
C2241 C2243' H2243'c . . . 100 ?
H2243'a C2243' H2243'b . . . 118 ?
H2243'a C2243' H2243'c . . . 90 ?
H2243'b C2243' H2243'c . . . 110 ?
C2241 C2244' H2244'a . . . 107 ?
C2241 C2244' H2244'b . . . 126 ?
C2241 C2244' H2244'c . . . 100 ?
H2244'a C2244' H2244'b . . . 117 ?
H2244'a C2244' H2244'c . . . 90 ?
H2244'b C2244' H2244'c . . . 108 ?
C224 C225 C226 . . . 122(3) ?
C224 C225 H225 . . . 122 ?
C226 C225 H225 . . . 116 ?
C21 C226 C221 . . . 123(2) ?
C21 C226 C225 . . . 116(2) ?
C221 C226 C225 . . . 120(3) ?
C222 C22 C236 . . . 112(2) ?
C222 C22 H22a . . . 113 ?
C222 C22 H22b . . . 113 ?
C236 C22 H22a . . . 108 ?
C236 C22 H22b . . . 110 ?
H22a C22 H22b . . . 101 ?
O231 C231 C232 . . . 116(2) ?
O231 C231 C236 . . . 116(2) ?
C232 C231 C236 . . . 127(2) ?
C231 C232 C233 . . . 119(3) ?
C231 C232 C23 . . . 123(2) ?
C233 C232 C23 . . . 118(3) ?
C232 C233 C234 . . . 118(3) ?
C232 C233 H233 . . . 123 ?
C234 C233 H233 . . . 118 ?
C233 C234 C2341 . . . 117(3) ?
C233 C234 C235 . . . 121(3) ?
C2341 C234 C235 . . . 122(3) ?
C234 C2341 C2342 . . . 107(3) ?
C234 C2341 C2343 . . . 113(3) ?
C234 C2341 C2344 . . . 104(3) ?
C234 C2341 C2342' . . . 115(3) ?
C234 C2341 C2343' . . . 107(3) ?
C234 C2341 C2344' . . . 103(3) ?
C2342 C2341 C2343 . . . 110(3) ?
C2342 C2341 C2344 . . . 113(3) ?
C2343 C2341 C2344 . . . 111(3) ?
C2342' C2341 C2343' . . . 104(4) ?
C2342' C2341 C2344' . . . 114(4) ?
C2343' C2341 C2344' . . . 115(4) ?
C2341 C2342 H2342a . . . 120 ?
C2341 C2342 H2342b . . . 98 ?
C2341 C2342 H2342c . . . 119 ?
H2342a C2342 H2342b . . . 88 ?
H2342a C2342 H2342c . . . 121 ?
H2342b C2342 H2342c . . . 87 ?
C2341 C2343 H2343a . . . 108 ?
C2341 C2343 H2343b . . . 101 ?
C2341 C2343 H2343c . . . 117 ?
H2343a C2343 H2343b . . . 102 ?
H2343a C2343 H2343c . . . 118 ?
H2343b C2343 H2343c . . . 107 ?
C2341 C2344 H2344a . . . 98 ?
C2341 C2344 H2344b . . . 94 ?
C2341 C2344 H2344c . . . 123 ?
H2344a C2344 H2344b . . . 88 ?
H2344a C2344 H2344c . . . 129 ?
H2344b C2344 H2344c . . . 115 ?
C2341 C2342' H2342'a . . . 106 ?
C2341 C2342' H2342'b . . . 96 ?
C2341 C2342' H2342'c . . . 124 ?
H2342'a C2342' H2342'b . . . 87 ?
H2342'a C2342' H2342'c . . . 128 ?
H2342'b C2342' H2342'c . . . 100 ?
C2341 C2343' H2343'a . . . 110 ?
C2341 C2343' H2343'b . . . 99 ?
C2341 C2343' H2343'c . . . 126 ?
H2343'a C2343' H2343'b . . . 91 ?
H2343'a C2343' H2343'c . . . 120 ?
H2343'b C2343' H2343'c . . . 99 ?
C2341 C2344' H2344'a . . . 105 ?
C2341 C2344' H2344'b . . . 94 ?
C2341 C2344' H2344'c . . . 125 ?
H2344'a C2344' H2344'b . . . 89 ?
H2344'a C2344' H2344'c . . . 127 ?
H2344'b C2344' H2344'c . . . 103 ?
C234 C235 C236 . . . 119(3) ?
C234 C235 H235 . . . 118 ?
C236 C235 H235 . . . 123 ?
C22 C236 C231 . . . 129(2) ?
C22 C236 C235 . . . 117(2) ?
C231 C236 C235 . . . 114(2) ?
C232 C23 C246 . . . 114(2) ?
C232 C23 H23a . . . 110 ?
C232 C23 H23b . . . 109 ?
C246 C23 H23a . . . 110 ?
C246 C23 H23b . . . 112 ?
H23a C23 H23b . . . 101 ?
Eu2 O241 C241 . . . 124.2(13) ?
O241 C241 C242 . . . 117(2) ?
O241 C241 C246 . . . 121(2) ?
C242 C241 C246 . . . 122(2) ?
C241 C242 C243 . . . 113(2) ?
C241 C242 C24 . . . 127(2) ?
C243 C242 C24 . . . 121(2) ?
C242 C243 C244 . . . 126(2) ?
C242 C243 H243 . . . 118 ?
C244 C243 H243 . . . 117 ?
C243 C244 C2441 . . . 120(2) ?
C243 C244 C245 . . . 117(2) ?
C2441 C244 C245 . . . 122(2) ?
C244 C2441 C2442 . . . 111(3) ?
C244 C2441 C2443 . . . 107(2) ?
C244 C2441 C2444 . . . 109(3) ?
C244 C2441 C2442' . . . 107(3) ?
C244 C2441 C2443' . . . 113(3) ?
C244 C2441 C2444' . . . 109(3) ?
C2442 C2441 C2443 . . . 112(3) ?
C2442 C2441 C2444 . . . 107(3) ?
C2443 C2441 C2444 . . . 111(3) ?
C2442' C2441 C2443' . . . 108(3) ?
C2442' C2441 C2444' . . . 109(3) ?
C2443' C2441 C2444' . . . 110(3) ?
C2441 C2442 H2442a . . . 119 ?
C2441 C2442 H2442b . . . 116 ?
C2441 C2442 H2442c . . . 114 ?
H2442a C2442 H2442b . . . 103 ?
H2442a C2442 H2442c . . . 100 ?
H2442b C2442 H2442c . . . 102 ?
C2441 C2443 H2443a . . . 111 ?
C2441 C2443 H2443b . . . 105 ?
C2441 C2443 H2443c . . . 119 ?
H2443a C2443 H2443b . . . 98 ?
H2443a C2443 H2443c . . . 112 ?
H2443b C2443 H2443c . . . 110 ?
C2441 C2444 H2444a . . . 114 ?
C2441 C2444 H2444b . . . 111 ?
C2441 C2444 H2444c . . . 119 ?
H2444a C2444 H2444b . . . 97 ?
H2444a C2444 H2444c . . . 107 ?
H2444b C2444 H2444c . . . 108 ?
C2441 C2442' H2442'a . . . 114 ?
C2441 C2442' H2442'b . . . 121 ?
C2441 C2442' H2442'c . . . 111 ?
H2442'a C2442' H2442'b . . . 107 ?
H2442'a C2442' H2442'c . . . 94 ?
H2442'b C2442' H2442'c . . . 106 ?
C2441 C2443' H2443'a . . . 112 ?
C2441 C2443' H2443'b . . . 109 ?
C2441 C2443' H2443'c . . . 113 ?
H2443'a C2443' H2443'b . . . 103 ?
H2443'a C2443' H2443'c . . . 108 ?
H2443'b C2443' H2443'c . . . 112 ?
C2441 C2444' H2444'a . . . 114 ?
C2441 C2444' H2444'b . . . 114 ?
C2441 C2444' H2444'c . . . 113 ?
H2444'a C2444' H2444'b . . . 103 ?
H2444'a C2444' H2444'c . . . 104 ?
H2444'b C2444' H2444'c . . . 108 ?
C244 C245 C246 . . . 123(2) ?
C244 C245 H245 . . . 121 ?
C246 C245 H245 . . . 116 ?
C23 C246 C241 . . . 121(2) ?
C23 C246 C245 . . . 120(2) ?
C241 C246 C245 . . . 120(2) ?
C242 C24 C256 . . . 109(2) ?
C242 C24 H24a . . . 113 ?
C242 C24 H24b . . . 112 ?
C256 C24 H24a . . . 110 ?
C256 C24 H24b . . . 111 ?
H24a C24 H24b . . . 102 ?
Eu2 O251 C251 . . . 148.1(15) ?
O251 C251 C252 . . . 122(2) ?
O251 C251 C256 . . . 120(2) ?
C252 C251 C256 . . . 118(2) ?
C251 C252 C253 . . . 121(2) ?
C251 C252 C25 . . . 120(2) ?
C253 C252 C25 . . . 120(2) ?
C252 C253 C254 . . . 120(2) ?
C252 C253 H253 . . . 121 ?
C254 C253 H253 . . . 119 ?
C253 C254 C2541 . . . 120(2) ?
C253 C254 C255 . . . 119(2) ?
C2541 C254 C255 . . . 121(2) ?
C254 C2541 C2542 . . . 116(2) ?
C254 C2541 C2543 . . . 113(3) ?
C254 C2541 C2544 . . . 110(2) ?
C2542 C2541 C2543 . . . 110(3) ?
C2542 C2541 C2544 . . . 103(3) ?
C2543 C2541 C2544 . . . 103(3) ?
C2541 C2542 H2542a . . . 115 ?
C2541 C2542 H2542b . . . 107 ?
C2541 C2542 H2542c . . . 110 ?
H2542a C2542 H2542b . . . 106 ?
H2542a C2542 H2542c . . . 112 ?
H2542b C2542 H2542c . . . 106 ?
C2541 C2543 H2543a . . . 116 ?
C2541 C2543 H2543b . . . 112 ?
C2541 C2543 H2543c . . . 112 ?
H2543a C2543 H2543b . . . 108 ?
H2543a C2543 H2543c . . . 104 ?
H2543b C2543 H2543c . . . 105 ?
C2541 C2544 H2544a . . . 118 ?
C2541 C2544 H2544b . . . 113 ?
C2541 C2544 H2544c . . . 112 ?
H2544a C2544 H2544b . . . 105 ?
H2544a C2544 H2544c . . . 106 ?
H2544b C2544 H2544c . . . 102 ?
C254 C255 C256 . . . 121(2) ?
C254 C255 H255 . . . 122 ?
C256 C255 H255 . . . 118 ?
C24 C256 C251 . . . 119(2) ?
C24 C256 C255 . . . 120(2) ?
C251 C256 C255 . . . 120(2) ?
C252 C25 C266 . . . 115(2) ?
C252 C25 H25a . . . 110 ?
C252 C25 H25b . . . 111 ?
C266 C25 H25a . . . 109 ?
C266 C25 H25b . . . 110 ?
H25a C25 H25b . . . 101 ?
Eu1 O261 Eu2 . . . 105.4(6) ?
Eu1 O261 C261 . . . 141.3(13) ?
Eu2 O261 C261 . . . 112.5(12) ?
O261 C261 C262 . . . 116.2(19) ?
O261 C261 C266 . . . 121(2) ?
C262 C261 C266 . . . 122(2) ?
C261 C262 C263 . . . 115(2) ?
C261 C262 C26 . . . 123(2) ?
C263 C262 C26 . . . 121(2) ?
C262 C263 C264 . . . 124(2) ?
C262 C263 H263 . . . 119 ?
C264 C263 H263 . . . 116 ?
C263 C264 C2641 . . . 121(2) ?
C263 C264 C265 . . . 116(2) ?
C2641 C264 C265 . . . 123(2) ?
C264 C2641 C2642 . . . 110(2) ?
C264 C2641 C2643 . . . 113(2) ?
C264 C2641 C2644 . . . 116(2) ?
C2642 C2641 C2643 . . . 103(2) ?
C2642 C2641 C2644 . . . 108(2) ?
C2643 C2641 C2644 . . . 105(2) ?
C2641 C2642 H2642a . . . 113 ?
C2641 C2642 H2642b . . . 112 ?
C2641 C2642 H2642c . . . 109 ?
H2642a C2642 H2642b . . . 109 ?
H2642a C2642 H2642c . . . 108 ?
H2642b C2642 H2642c . . . 107 ?
C2641 C2643 H2643a . . . 116 ?
C2641 C2643 H2643b . . . 112 ?
C2641 C2643 H2643c . . . 115 ?
H2643a C2643 H2643b . . . 104 ?
H2643a C2643 H2643c . . . 106 ?
H2643b C2643 H2643c . . . 103 ?
C2641 C2644 H2644a . . . 111 ?
C2641 C2644 H2644b . . . 106 ?
C2641 C2644 H2644c . . . 110 ?
H2644a C2644 H2644b . . . 109 ?
H2644a C2644 H2644c . . . 112 ?
H2644b C2644 H2644c . . . 110 ?
C264 C265 C266 . . . 124(2) ?
C264 C265 H265 . . . 117 ?
C266 C265 H265 . . . 119 ?
C25 C266 C261 . . . 120(2) ?
C25 C266 C265 . . . 122(2) ?
C261 C266 C265 . . . 118(2) ?
C262 C26 C276 . . . 114.6(18) ?
C262 C26 H26a . . . 107 ?
C262 C26 H26b . . . 115 ?
C276 C26 H26a . . . 107.4 ?
C276 C26 H26b . . . 107 ?
H26a C26 H26b . . . 104 ?
Eu2 O271 Eu3 . . . 105.1(5) ?
Eu2 O271 C271 . . . 132.2(12) ?
Eu3 O271 C271 . . . 122.7(12) ?
O271 C271 C272 . . . 120.7(17) ?
O271 C271 C276 . . . 127.1(19) ?
C272 C271 C276 . . . 112(2) ?
C271 C272 C273 . . . 119(2) ?
C271 C272 C27 . . . 116(2) ?
C273 C272 C27 . . . 125(2) ?
C272 C273 C274 . . . 125(2) ?
C272 C273 H273 . . . 116 ?
C274 C273 H273 . . . 120 ?
C273 C274 C2741 . . . 120(2) ?
C273 C274 C275 . . . 117(2) ?
C2741 C274 C275 . . . 123(2) ?
C274 C2741 C2742 . . . 109(2) ?
C274 C2741 C2743 . . . 114(2) ?
C274 C2741 C2744 . . . 107(3) ?
C274 C2741 C2742' . . . 114(2) ?
C274 C2741 C2743' . . . 107(3) ?
C274 C2741 C2744' . . . 110(3) ?
C2742 C2741 C2743 . . . 109(3) ?
C2742 C2741 C2744 . . . 111(3) ?
C2743 C2741 C2744 . . . 107(3) ?
C2742' C2741 C2743' . . . 106(3) ?
C2742' C2741 C2744' . . . 115(3) ?
C2743' C2741 C2744' . . . 104(3) ?
C2741 C2742 H2742a . . . 104 ?
C2741 C2742 H2742b . . . 104 ?
C2741 C2742 H2742c . . . 116 ?
H2742a C2742 H2742b . . . 98 ?
H2742a C2742 H2742c . . . 116 ?
H2742b C2742 H2742c . . . 116 ?
C2741 C2743 H2743a . . . 112 ?
C2741 C2743 H2743b . . . 108 ?
C2741 C2743 H2743c . . . 112 ?
H2743a C2743 H2743b . . . 107 ?
H2743a C2743 H2743c . . . 111 ?
H2743b C2743 H2743c . . . 108 ?
C2741 C2744 H2744a . . . 118 ?
C2741 C2744 H2744b . . . 109 ?
C2741 C2744 H2744c . . . 114 ?
H2744a C2744 H2744b . . . 103 ?
H2744a C2744 H2744c . . . 110 ?
H2744b C2744 H2744c . . . 101 ?
C2741 C2742' H2742'a . . . 111 ?
C2741 C2742' H2742'b . . . 102 ?
C2741 C2742' H2742'c . . . 125 ?
H2742'a C2742' H2742'b . . . 91 ?
H2742'a C2742' H2742'c . . . 118 ?
H2742'b C2742' H2742'c . . . 102 ?
C2741 C2743' H2743'a . . . 109 ?
C2741 C2743' H2743'b . . . 109 ?
C2741 C2743' H2743'c . . . 118 ?
H2743'a C2743' H2743'b . . . 100 ?
H2743'a C2743' H2743'c . . . 108 ?
H2743'b C2743' H2743'c . . . 111 ?
C2741 C2744' H2744'a . . . 112 ?
C2741 C2744' H2744'b . . . 107 ?
C2741 C2744' H2744'c . . . 118 ?
H2744'a C2744' H2744'b . . . 100 ?
H2744'a C2744' H2744'c . . . 112 ?
H2744'b C2744' H2744'c . . . 106 ?
C274 C275 C276 . . . 122(2) ?
C274 C275 H275 . . . 119 ?
C276 C275 H275 . . . 119 ?
C26 C276 C271 . . . 115(2) ?
C26 C276 C275 . . . 120(2) ?
C271 C276 C275 . . . 125(2) ?
C216 C27 C272 . . . 116.3(18) ?
C216 C27 H27a . . . 109 ?
C216 C27 H27b . . . 110 ?
C272 C27 H27a . . . 109 ?
C272 C27 H27b . . . 108.4 ?
H27a C27 H27b . . . 104 ?
Eu3 O10 S10 . . . 147.3(13) ?
Eu3 O10 S10' . . . 168(2) ?
O10 S10 C101 . . . 110(2) ?
O10 S10 C102 . . . 102(2) ?
C101 S10 C102 . . . 103(3) ?
O10 S10' C101 . . . 133(4) ?
O10 S10' C102 . . . 116(3) ?
C101 S10' C102 . . . 111(4) ?
S10 C101 H101a . . . 116 ?
S10 C101 H101b . . . 115 ?
S10 C101 H101c . . . 121 ?
S10' C101 H101'a . . . 110 ?
S10' C101 H101'b . . . 116 ?
S10' C101 H101'c . . . 121 ?
H101a C101 H101b . . . 97 ?
H101a C101 H101c . . . 101 ?
H101b C101 H101c . . . 103 ?
H101'a C101 H101'b . . . 110 ?
H101'a C101 H101'c . . . 102 ?
H101'b C101 H101'c . . . 96 ?
S10 C102 H102a . . . 122 ?
S10 C102 H102b . . . 110 ?
S10 C102 H102c . . . 110 ?
S10' C102 H102'a . . . 104 ?
S10' C102 H102'b . . . 128 ?
S10' C102 H102'c . . . 115 ?
H102a C102 H102b . . . 107 ?
H102a C102 H102c . . . 107 ?
H102b C102 H102c . . . 98 ?
H102'a C102 H102'b . . . 101 ?
H102'a C102 H102'c . . . 100 ?
H102'b C102 H102'c . . . 105 ?
Eu1 O20 S20 . . . 127.8(11) ?
Eu1 O20 S20' . . . 148(2) ?
O20 S20 C201 . . . 99.6(17) ?
O20 S20 C202 . . . 113(2) ?
C201 S20 C202 . . . 98(2) ?
O20 S20' C201 . . . 105(3) ?
O20 S20' C202 . . . 131(4) ?
C201 S20' C202 . . . 110(3) ?
S20 C201 H201a . . . 113 ?
S20 C201 H201b . . . 108 ?
S20 C201 H201c . . . 110 ?
S20' C201 H201'a . . . 101 ?
S20' C201 H201'b . . . 116 ?
S20' C201 H201'c . . . 113 ?
H201a C201 H201b . . . 105 ?
H201a C201 H201c . . . 113 ?
H201b C201 H201c . . . 108 ?
H201'a C201 H201'b . . . 113 ?
H201'a C201 H201'c . . . 105 ?
H201'b C201 H201'c . . . 108 ?
S20 C202 H202a . . . 116 ?
S20 C202 H202b . . . 106 ?
S20 C202 H202c . . . 104 ?
S20' C202 H202'a . . . 96 ?
S20' C202 H202'b . . . 122 ?
S20' C202 H202'c . . . 118 ?
H202a C202 H202b . . . 117 ?
H202a C202 H202c . . . 110 ?
H202b C202 H202c . . . 102 ?
H202'a C202 H202'b . . . 103 ?
H202'a C202 H202'c . . . 102 ?
H202'b C202 H202'c . . . 111 ?
Eu1 O30 S30 . . . 137.9(11) ?
Eu1 O30 S30' . . . 169(2) ?
O30 S30 C301 . . . 110(2) ?
O30 S30 C302 . . . 103(2) ?
C301 S30 C302 . . . 111(3) ?
O30 S30' C301 . . . 99(5) ?
O30 S30' C302 . . . 74(3) ?
C301 S30' C302 . . . 107(5) ?
S30 C301 H301a . . . 131 ?
S30 C301 H301b . . . 108 ?
S30 C301 H301c . . . 114 ?
S30' C301 H301'a . . . 134 ?
S30' C301 H301'b . . . 115 ?
S30' C301 H301'c . . . 117 ?
H301a C301 H301b . . . 100 ?
H301a C301 H301c . . . 106 ?
H301b C301 H301c . . . 89 ?
H301c C301 H301'c . . . 104 ?
H301'a C301 H301'b . . . 96 ?
H301'a C301 H301'c . . . 93 ?
H301'b C301 H301'c . . . 93 ?
S30 C302 H302a . . . 112 ?
S30 C302 H302b . . . 115 ?
S30 C302 H302c . . . 112 ?
S30' C302 H302'a . . . 122 ?
S30' C302 H302'b . . . 118 ?
S30' C302 H302'c . . . 115 ?
H302c C302 H302'c . . . 104 ?
H302'a C302 H302'b . . . 99 ?
H302'a C302 H302'c . . . 99 ?
H302'b C302 H302'c . . . 100 ?
Eu2 O40 S40 . . . 173.7(12) ?
Eu2 O40 S40' . . . 132.6(13) ?
O40 S40 C401 . . . 105.4(13) ?
O40 S40 C402 . . . 104.3(14) ?
C401 S40 C402 . . . 100.2(16) ?
O40 S40' C401 . . . 104.8(19) ?
O40 S40' C402 . . . 105.7(19) ?
C401 S40' C402 . . . 113(2) ?
S40 C401 H401a . . . 116 ?
S40 C401 H401b . . . 114 ?
S40 C401 H401c . . . 114 ?
S40' C401 H401'a . . . 117 ?
S40' C401 H401'b . . . 113 ?
S40' C401 H401'c . . . 113 ?
H401a C401 H401b . . . 105 ?
H401a C401 H401c . . . 105 ?
H401b C401 H401c . . . 102 ?
H401'a C401 H401'b . . . 106 ?
H401'a C401 H401'c . . . 106 ?
H401'b C401 H401'c . . . 101 ?
S40 C402 H402a . . . 114 ?
S40 C402 H402b . . . 109 ?
S40 C402 H402c . . . 114 ?
S40' C402 H402'a . . . 114 ?
S40' C402 H402'b . . . 115 ?
S40' C402 H402'c . . . 110 ?
H402a C402 H402b . . . 104 ?
H402a C402 H402c . . . 111 ?
H402b C402 H402c . . . 104 ?
H402'a C402 H402'b . . . 109 ?
H402'a C402 H402'c . . . 103 ?
H402'b C402 H402'c . . . 104 ?
Eu4 O50 S50 . . . 137.9(12) ?
Eu4 O50 S50' . . . 168.2(13) ?
O50 S50 C501 . . . 109.9(16) ?
O50 S50 C502 . . . 107(2) ?
C501 S50 C502 . . . 106(2) ?
O50 S50' C501 . . . 99.7(18) ?
O50 S50' C502 . . . 111(3) ?
C501 S50' C502 . . . 98(2) ?
S50 C501 H501a . . . 113 ?
S50 C501 H501b . . . 115 ?
S50 C501 H501c . . . 113 ?
S50' C501 H501'a . . . 115 ?
S50' C501 H501'b . . . 109 ?
S50' C501 H501'c . . . 112 ?
H501a C501 H501b . . . 106 ?
H501a C501 H501c . . . 104 ?
H501b C501 H501c . . . 106 ?
H501'a C501 H501'b . . . 107 ?
H501'a C501 H501'c . . . 110 ?
H501'b C501 H501'c . . . 103 ?
S50 C502 H502a . . . 109 ?
S50 C502 H502b . . . 113 ?
S50 C502 H502c . . . 115 ?
S50' C502 H502'a . . . 113 ?
S50' C502 H502'b . . . 107 ?
S50' C502 H502'c . . . 105 ?
H502a C502 H502b . . . 103 ?
H502a C502 H502c . . . 105 ?
H502b C502 H502c . . . 111 ?
H502'a C502 H502'b . . . 114 ?
H502'a C502 H502'c . . . 113 ?
H502'b C502 H502'c . . . 104 ?
Eu3 O60 S60 . . . 145.0(13) ?
Eu3 O60 S60' . . . 170.4(14) ?
O60 S60 C601 . . . 111.9(18) ?
O60 S60 C602 . . . 109.7(17) ?
C601 S60 C602 . . . 109(2) ?
O60 S60' C601 . . . 109.7(19) ?
O60 S60' C602 . . . 108.1(18) ?
C601 S60' C602 . . . 109(2) ?
S60 C601 H601a . . . 113 ?
S60 C601 H601b . . . 107 ?
S60 C601 H601c . . . 113 ?
S60' C601 H601'a . . . 112 ?
S60' C601 H601'b . . . 111 ?
S60' C601 H601'c . . . 111 ?
H601a C601 H601b . . . 106 ?
H601a C601 H601c . . . 110 ?
H601b C601 H601c . . . 107 ?
H601'a C601 H601'b . . . 111 ?
H601'a C601 H601'c . . . 106 ?
H601'b C601 H601'c . . . 106 ?
S60 C602 H602a . . . 105 ?
S60 C602 H602b . . . 113 ?
S60 C602 H602c . . . 113 ?
S60' C602 H602'a . . . 112 ?
S60' C602 H602'b . . . 105 ?
S60' C602 H602'c . . . 100 ?
H602a C602 H602b . . . 101 ?
H602a C602 H602c . . . 104 ?
H602b C602 H602c . . . 119 ?
H602'a C602 H602'b . . . 122 ?
H602'a C602 H602'c . . . 112 ?
H602'b C602 H602'c . . . 103 ?
N01 C011 C012 . . . 179(4) ?
N02 C021 C022 . . . 178(4) ?
N03 C031 C032 . . . 178(6) ?
N04 C041 C042 . . . 177(6) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Eu1 Eu2 . . 3.7682(19) ?
Eu1 Eu4 . . 3.7572(19) ?
Eu1 O2 . . 2.461(14) ?
Eu1 O101 . . 2.475(14) ?
Eu1 O102 . . 2.355(17) ?
Eu1 O111 . . 2.315(15) ?
Eu1 O171 . . 2.430(14) ?
Eu1 O261 . . 2.425(16) ?
Eu1 O20 . . 2.401(16) ?
Eu1 O30 . . 2.434(17) ?
Eu2 Eu3 . . 3.765(2) ?
Eu2 Eu4 . . 3.777(2) ?
Eu2 O1 . . 2.351(14) ?
Eu2 O2 . . 2.460(15) ?
Eu2 O101 . . 2.878(14) ?
Eu2 O241 . . 2.878(15) ?
Eu2 O251 . . 2.226(15) ?
Eu2 O261 . . 2.311(14) ?
Eu2 O271 . . 2.302(14) ?
Eu2 O40 . . 2.344(17) ?
Eu3 Eu4 . . 3.763(2) ?
Eu3 O1 . . 2.397(14) ?
Eu3 O101 . . 2.488(14) ?
Eu3 O103 . . 2.430(15) ?
Eu3 O161 . . 2.363(16) ?
Eu3 O211 . . 2.296(15) ?
Eu3 O271 . . 2.441(14) ?
Eu3 O10 . . 2.22(2) ?
Eu3 O60 . . 2.342(17) ?
Eu4 O1 . . 2.449(15) ?
Eu4 O2 . . 2.334(14) ?
Eu4 O101 . . 2.764(14) ?
Eu4 O141 . . 2.783(15) ?
Eu4 O151 . . 2.209(15) ?
Eu4 O161 . . 2.311(15) ?
Eu4 O171 . . 2.384(14) ?
Eu4 O50 . . 2.387(18) ?
C0 O101 . . 1.30(3) ?
C0 O102 . . 1.26(3) ?
C0 O103 . . 1.30(3) ?
O111 C111 . . 1.32(3) ?
C111 C112 . . 1.41(3) ?
C111 C116 . . 1.36(3) ?
C112 C113 . . 1.43(3) ?
C112 C11 . . 1.53(3) ?
C113 C114 . . 1.36(3) ?
C113 H113 . . .99 ?
C114 C1141 . . 1.55(3) ?
C114 C115 . . 1.39(3) ?
C1141 C1142 . . 1.53(5) ?
C1141 C1143 . . 1.51(5) ?
C1141 C1144 . . 1.47(5) ?
C1141 C1142' . . 1.46(6) ?
C1141 C1143' . . 1.44(5) ?
C1141 C1144' . . 1.54(6) ?
C1142 H1142a . . .92 ?
C1142 H1142b . . .99 ?
C1142 H1142c . . .93 ?
C1143 H1143a . . .98 ?
C1143 H1143b . . .96 ?
C1143 H1143c . . .87 ?
C1144 H1144a . . .96 ?
C1144 H1144b . . 1.03 ?
C1144 H1144c . . .88 ?
C1142' H1142'a . . .92 ?
C1142' H1142'b . . 1.06 ?
C1142' H1142'c . . .93 ?
C1143' H1143'a . . .94 ?
C1143' H1143'b . . .97 ?
C1143' H1143'c . . .90 ?
C1144' H1144'a . . .98 ?
C1144' H1144'b . . 1.04 ?
C1144' H1144'c . . .79 ?
C115 C116 . . 1.41(3) ?
C115 H115 . . 1.01 ?
C116 C17 . . 1.54(3) ?
C11 C126 . . 1.44(3) ?
C11 H11a . . 1.02 ?
C11 H11b . . 1.00 ?
O121 C121 . . 1.33(3) ?
C121 C122 . . 1.36(3) ?
C121 C126 . . 1.38(3) ?
C122 C123 . . 1.36(4) ?
C122 C12 . . 1.55(4) ?
C123 C124 . . 1.42(4) ?
C123 H123 . . 1.00 ?
C124 C1241 . . 1.62(3) ?
C124 C125 . . 1.39(3) ?
C1241 C1242 . . 1.50(4) ?
C1241 C1243 . . 1.52(4) ?
C1241 C1244 . . 1.54(4) ?
C1242 H1242a . . .98 ?
C1242 H1242b . . .97 ?
C1242 H1242c . . .97 ?
C1243 H1243a . . .96 ?
C1243 H1243b . . .96 ?
C1243 H1243c . . .93 ?
C1244 H1244a . . .98 ?
C1244 H1244b . . .94 ?
C1244 H1244c . . .90 ?
C125 C126 . . 1.38(3) ?
C125 H125 . . 1.00 ?
C12 C136 . . 1.50(4) ?
C12 H12a . . 1.02 ?
C12 H12b . . .98 ?
O131 C131 . . 1.38(3) ?
C131 C132 . . 1.33(3) ?
C131 C136 . . 1.39(3) ?
C132 C133 . . 1.39(4) ?
C132 C13 . . 1.51(3) ?
C133 C134 . . 1.37(4) ?
C133 H133 . . 1.03 ?
C134 C1341 . . 1.47(4) ?
C134 C135 . . 1.38(4) ?
C1341 C1342 . . 1.60(5) ?
C1341 C1343 . . 1.53(5) ?
C1341 C1344 . . 1.48(6) ?
C1342 H1342a . . .95 ?
C1342 H1342b . . 1.03 ?
C1342 H1342c . . .88 ?
C1343 H1343a . . .99 ?
C1343 H1343b . . .90 ?
C1343 H1343c . . 1.01 ?
C1344 H1344a . . 1.02 ?
C1344 H1344b . . .93 ?
C1344 H1344c . . 1.00 ?
C135 C136 . . 1.35(4) ?
C135 H135 . . 1.01 ?
C13 C146 . . 1.52(4) ?
C13 H13a . . .98 ?
C13 H13b . . 1.02 ?
O141 C141 . . 1.32(3) ?
C141 C142 . . 1.46(3) ?
C141 C146 . . 1.32(3) ?
C142 C143 . . 1.37(4) ?
C142 C14 . . 1.56(3) ?
C143 C144 . . 1.43(4) ?
C143 H143 . . 1.02 ?
C144 C1441 . . 1.64(3) ?
C144 C145 . . 1.41(4) ?
C1441 C1442 . . 1.50(7) ?
C1441 C1443 . . 1.44(6) ?
C1441 C1444 . . 1.57(7) ?
C1441 C1442' . . 1.49(6) ?
C1441 C1443' . . 1.46(6) ?
C1441 C1444' . . 1.60(7) ?
C1442 C1442' . . 1.16(9) ?
C1442 C1444' . . 1.64(9) ?
C1442 H1442a . . .94 ?
C1442 H1442b . . 1.28 ?
C1442 H1442c . . .74 ?
C1443 H1443a . . .94 ?
C1443 H1443b . . .97 ?
C1443 H1443c . . 1.06 ?
C1444 H1444a . . 1.28 ?
C1444 H1444b . . .79 ?
C1444 H1444c . . .79 ?
C1442' H1442'a . . .94 ?
C1442' H1442'b . . .92 ?
C1442' H1442'c . . 1.11 ?
C1443' H1443'a . . .99 ?
C1443' H1443'b . . .88 ?
C1443' H1443'c . . 1.10 ?
C1444' H1444'a . . .96 ?
C1444' H1444'b . . .73 ?
C1444' H1444'c . . 1.04 ?
C145 C146 . . 1.36(4) ?
C145 H145 . . 1.02 ?
C14 C156 . . 1.51(4) ?
C14 H14a . . .99 ?
C14 H14b . . .97 ?
O151 C151 . . 1.34(3) ?
C151 C152 . . 1.39(4) ?
C151 C156 . . 1.35(4) ?
C152 C153 . . 1.39(3) ?
C152 C15 . . 1.47(4) ?
C153 C154 . . 1.33(4) ?
C153 H153 . . 1.02 ?
C154 C1541 . . 1.58(4) ?
C154 C155 . . 1.36(4) ?
C1541 C1542 . . 1.36(5) ?
C1541 C1543 . . 1.43(5) ?
C1541 C1544 . . 1.40(7) ?
C1542 H1542a . . .98 ?
C1542 H1542b . . .98 ?
C1542 H1542c . . 1.00 ?
C1543 H1543a . . 1.01 ?
C1543 H1543b . . .92 ?
C1543 H1543c . . .93 ?
C1544 H1544a . . .95 ?
C1544 H1544b . . .98 ?
C1544 H1544c . . 1.05 ?
C155 C156 . . 1.38(4) ?
C155 H155 . . .98 ?
C15 C166 . . 1.53(3) ?
C15 H15a . . .98 ?
C15 H15b . . .95 ?
O161 C161 . . 1.36(3) ?
C161 C162 . . 1.38(3) ?
C161 C166 . . 1.44(3) ?
C162 C163 . . 1.47(3) ?
C162 C16 . . 1.49(4) ?
C163 C164 . . 1.40(4) ?
C163 H163 . . .98 ?
C164 C1641 . . 1.58(5) ?
C164 C165 . . 1.36(4) ?
C1641 C1642 . . 1.45(6) ?
C1641 C1643 . . 1.48(6) ?
C1641 C1644 . . 1.50(6) ?
C1642 H1642a . . .96 ?
C1642 H1642b . . .86 ?
C1642 H1642c . . .94 ?
C1643 H1643a . . .97 ?
C1643 H1643b . . 1.05 ?
C1643 H1643c . . .93 ?
C1644 H1644a . . .98 ?
C1644 H1644b . . .94 ?
C1644 H1644c . . .94 ?
C165 C166 . . 1.36(3) ?
C165 H165 . . .97 ?
C16 C172 . . 1.48(4) ?
C16 H16a . . .98 ?
C16 H16b . . .98 ?
O171 C171 . . 1.35(3) ?
C171 C172 . . 1.34(3) ?
C171 C176 . . 1.42(3) ?
C172 C173 . . 1.36(3) ?
C173 C174 . . 1.39(4) ?
C173 H173 . . 1.03 ?
C174 C1741 . . 1.62(3) ?
C174 C175 . . 1.37(3) ?
C1741 C1742 . . 1.45(6) ?
C1741 C1743 . . 1.48(6) ?
C1741 C1744 . . 1.44(5) ?
C1741 C1742' . . 1.55(6) ?
C1741 C1743' . . 1.49(6) ?
C1741 C1744' . . 1.38(5) ?
C1742 C1742' . . 1.52(8) ?
C1742 C1744' . . 1.23(7) ?
C1742 H1742a . . 1.00 ?
C1742 H1742b . . .87 ?
C1742 H1742c . . 1.08 ?
C1743 H1743a . . .96 ?
C1743 H1743b . . .90 ?
C1743 H1743c . . .97 ?
C1744 H1744a . . .96 ?
C1744 H1744b . . .80 ?
C1744 H1744c . . 1.09 ?
C1742' H1742'a . . .93 ?
C1742' H1742'b . . .82 ?
C1742' H1742'c . . 1.09 ?
C1743' H1743'a . . .95 ?
C1743' H1743'b . . .91 ?
C1743' H1743'c . . 1.06 ?
C1744' H1744'a . . .94 ?
C1744' H1744'b . . .95 ?
C1744' H1744'c . . 1.02 ?
C175 C176 . . 1.39(3) ?
C175 H175 . . 1.05 ?
C176 C17 . . 1.50(3) ?
C17 H17a . . .98 ?
C17 H17b . . 1.01 ?
O211 C211 . . 1.35(3) ?
C211 C212 . . 1.45(3) ?
C211 C216 . . 1.33(3) ?
C212 C213 . . 1.39(4) ?
C212 C21 . . 1.49(3) ?
C213 C214 . . 1.31(4) ?
C213 H213 . . .98 ?
C214 C2141 . . 1.52(4) ?
C214 C215 . . 1.40(4) ?
C2141 C2142 . . 1.46(5) ?
C2141 C2143 . . 1.50(5) ?
C2141 C2144 . . 1.60(6) ?
C2141 C2142' . . 1.52(6) ?
C2141 C2143' . . 1.37(6) ?
C2141 C2144' . . 1.46(6) ?
C2142 C2142' . . 1.43(7) ?
C2142 C2144' . . 1.29(7) ?
C2142 H2142a . . .95 ?
C2142 H2142b . . 1.01 ?
C2142 H2142c . . .92 ?
C2143 H2143a . . .96 ?
C2143 H2143b . . .99 ?
C2143 H2143c . . 1.00 ?
C2144 H2144a . . .98 ?
C2144 H2144b . . .98 ?
C2144 H2144c . . .92 ?
C2142' H2142'a . . .99 ?
C2142' H2142'b . . .96 ?
C2142' H2142'c . . .90 ?
C2143' H2143'a . . 1.02 ?
C2143' H2143'b . . 1.03 ?
C2143' H2143'c . . .88 ?
C2144' H2144'a . . .97 ?
C2144' H2144'b . . .96 ?
C2144' H2144'c . . .97 ?
C215 C216 . . 1.42(4) ?
C215 H215 . . 1.01 ?
C216 C27 . . 1.59(3) ?
C21 C226 . . 1.52(4) ?
C21 H21a . . 1.00 ?
C21 H21b . . 1.00 ?
O221 C221 . . 1.30(3) ?
C221 C222 . . 1.43(4) ?
C221 C226 . . 1.36(4) ?
C222 C223 . . 1.36(4) ?
C222 C22 . . 1.46(4) ?
C223 C224 . . 1.34(4) ?
C223 H223 . . 1.00 ?
C224 C2241 . . 1.61(4) ?
C224 C225 . . 1.44(4) ?
C2241 C2242 . . 1.42(6) ?
C2241 C2243 . . 1.46(5) ?
C2241 C2244 . . 1.55(7) ?
C2241 C2242' . . 1.44(5) ?
C2241 C2243' . . 1.51(6) ?
C2241 C2244' . . 1.56(7) ?
C2242 C2242' . . .95(7) ?
C2242 C2243' . . 1.67(8) ?
C2242 H2242a . . .95 ?
C2242 H2242b . . 1.04 ?
C2242 H2242c . . .90 ?
C2243 H2243a . . .97 ?
C2243 H2243b . . .88 ?
C2243 H2243c . . 1.07 ?
C2244 H2244a . . 1.01 ?
C2244 H2244b . . .94 ?
C2244 H2244c . . .93 ?
C2242' H2242'a . . .97 ?
C2242' H2242'b . . .88 ?
C2242' H2242'c . . 1.03 ?
C2243' H2243'a . . 1.06 ?
C2243' H2243'b . . .74 ?
C2243' H2243'c . . 1.13 ?
C2244' H2244'a . . 1.05 ?
C2244' H2244'b . . .75 ?
C2244' H2244'c . . 1.14 ?
C225 C226 . . 1.42(4) ?
C225 H225 . . .99 ?
C22 C236 . . 1.55(4) ?
C22 H22a . . 1.00 ?
C22 H22b . . 1.01 ?
O231 C231 . . 1.41(3) ?
C231 C232 . . 1.35(4) ?
C231 C236 . . 1.36(3) ?
C232 C233 . . 1.35(4) ?
C232 C23 . . 1.53(4) ?
C233 C234 . . 1.36(5) ?
C233 H233 . . .93 ?
C234 C2341 . . 1.71(4) ?
C234 C235 . . 1.46(4) ?
C2341 C2342 . . 1.50(5) ?
C2341 C2343 . . 1.50(5) ?
C2341 C2344 . . 1.63(6) ?
C2341 C2342' . . 1.52(6) ?
C2341 C2343' . . 1.57(8) ?
C2341 C2344' . . 1.47(7) ?
C2342 C2342' . . 1.06(8) ?
C2342 C2343' . . 1.70(9) ?
C2342 H2342a . . .89 ?
C2342 H2342b . . 1.31 ?
C2342 H2342c . . .90 ?
C2343 H2343a . . .94 ?
C2343 H2343b . . 1.05 ?
C2343 H2343c . . .87 ?
C2344 H2344a . . 1.07 ?
C2344 H2344b . . 1.17 ?
C2344 H2344c . . .64 ?
C2342' H2342'a . . .99 ?
C2342' H2342'b . . 1.25 ?
C2342' H2342'c . . .73 ?
C2343' H2343'a . . .97 ?
C2343' H2343'b . . 1.20 ?
C2343' H2343'c . . .82 ?
C2344' H2344'a . . 1.00 ?
C2344' H2344'b . . 1.21 ?
C2344' H2344'c . . .73 ?
C235 C236 . . 1.36(4) ?
C235 H235 . . .99 ?
C23 C246 . . 1.46(3) ?
C23 H23a . . 1.03 ?
C23 H23b . . .98 ?
O241 C241 . . 1.40(3) ?
C241 C242 . . 1.39(3) ?
C241 C246 . . 1.40(3) ?
C242 C243 . . 1.47(3) ?
C242 C24 . . 1.56(4) ?
C243 C244 . . 1.34(4) ?
C243 H243 . . .97 ?
C244 C2441 . . 1.50(3) ?
C244 C245 . . 1.35(4) ?
C2441 C2442 . . 1.52(6) ?
C2441 C2443 . . 1.59(5) ?
C2441 C2444 . . 1.49(6) ?
C2441 C2442' . . 1.45(6) ?
C2441 C2443' . . 1.39(6) ?
C2441 C2444' . . 1.53(6) ?
C2442 C2442' . . 1.06(7) ?
C2442 C2444' . . 1.72(8) ?
C2442 H2442a . . 1.01 ?
C2442 H2442b . . .98 ?
C2442 H2442c . . 1.01 ?
C2443 H2443a . . 1.02 ?
C2443 H2443b . . 1.04 ?
C2443 H2443c . . .85 ?
C2444 H2444a . . 1.05 ?
C2444 H2444b . . 1.03 ?
C2444 H2444c . . .88 ?
C2442' H2442'a . . 1.06 ?
C2442' H2442'b . . .87 ?
C2442' H2442'c . . 1.06 ?
C2443' H2443'a . . 1.02 ?
C2443' H2443'b . . .97 ?
C2443' H2443'c . . .90 ?
C2444' H2444'a . . 1.02 ?
C2444' H2444'b . . .97 ?
C2444' H2444'c . . .95 ?
C245 C246 . . 1.36(3) ?
C245 H245 . . 1.08 ?
C24 C256 . . 1.56(3) ?
C24 H24a . . 1.00 ?
C24 H24b . . 1.00 ?
O251 C251 . . 1.33(3) ?
C251 C252 . . 1.36(3) ?
C251 C256 . . 1.38(3) ?
C252 C253 . . 1.40(3) ?
C252 C25 . . 1.49(3) ?
C253 C254 . . 1.38(3) ?
C253 H253 . . 1.02 ?
C254 C2541 . . 1.50(4) ?
C254 C255 . . 1.34(3) ?
C2541 C2542 . . 1.49(4) ?
C2541 C2543 . . 1.42(5) ?
C2541 C2544 . . 1.52(5) ?
C2542 H2542a . . .94 ?
C2542 H2542b . . 1.01 ?
C2542 H2542c . . .93 ?
C2543 H2543a . . .97 ?
C2543 H2543b . . .95 ?
C2543 H2543c . . 1.00 ?
C2544 H2544a . . .95 ?
C2544 H2544b . . 1.00 ?
C2544 H2544c . . .99 ?
C255 C256 . . 1.42(3) ?
C255 H255 . . .98 ?
C25 C266 . . 1.53(4) ?
C25 H25a . . 1.02 ?
C25 H25b . . .99 ?
O261 C261 . . 1.40(3) ?
C261 C262 . . 1.42(3) ?
C261 C266 . . 1.41(3) ?
C262 C263 . . 1.32(3) ?
C262 C26 . . 1.51(3) ?
C263 C264 . . 1.46(3) ?
C263 H263 . . 1.03 ?
C264 C2641 . . 1.50(3) ?
C264 C265 . . 1.35(3) ?
C2641 C2642 . . 1.54(4) ?
C2641 C2643 . . 1.55(4) ?
C2641 C2644 . . 1.55(4) ?
C2642 H2642a . . .95 ?
C2642 H2642b . . .96 ?
C2642 H2642c . . .97 ?
C2643 H2643a . . .96 ?
C2643 H2643b . . 1.01 ?
C2643 H2643c . . .98 ?
C2644 H2644a . . .94 ?
C2644 H2644b . . .96 ?
C2644 H2644c . . .93 ?
C265 C266 . . 1.33(3) ?
C265 H265 . . .96 ?
C26 C276 . . 1.54(3) ?
C26 H26a . . 1.01 ?
C26 H26b . . .96 ?
O271 C271 . . 1.37(3) ?
C271 C272 . . 1.51(3) ?
C271 C276 . . 1.40(3) ?
C272 C273 . . 1.37(3) ?
C272 C27 . . 1.53(3) ?
C273 C274 . . 1.31(3) ?
C273 H273 . . 1.00 ?
C274 C2741 . . 1.51(3) ?
C274 C275 . . 1.41(3) ?
C2741 C2742 . . 1.57(5) ?
C2741 C2743 . . 1.51(5) ?
C2741 C2744 . . 1.49(6) ?
C2741 C2742' . . 1.46(5) ?
C2741 C2743' . . 1.49(6) ?
C2741 C2744' . . 1.51(7) ?
C2742 C2742' . . 1.20(7) ?
C2742 C2743' . . 1.60(8) ?
C2742 H2742a . . 1.03 ?
C2742 H2742b . . 1.02 ?
C2742 H2742c . . .80 ?
C2743 H2743a . . .95 ?
C2743 H2743b . . .98 ?
C2743 H2743c . . .94 ?
C2744 H2744a . . .93 ?
C2744 H2744b . . 1.05 ?
C2744 H2744c . . .96 ?
C2742' H2742'a . . 1.00 ?
C2742' H2742'b . . 1.17 ?
C2742' H2742'c . . .80 ?
C2743' H2743'a . . 1.03 ?
C2743' H2743'b . . 1.00 ?
C2743' H2743'c . . .88 ?
C2744' H2744'a . . .98 ?
C2744' H2744'b . . 1.04 ?
C2744' H2744'c . . .89 ?
C275 C276 . . 1.30(3) ?
C275 H275 . . .96 ?
C27 H27a . . .98 ?
C27 H27b . . .98 ?
O10 S10 . . 1.49(2) ?
O10 S10' . . 1.27(4) ?
S10 C101 . . 1.66(6) ?
S10 C102 . . 1.86(6) ?
S10' C101 . . 1.54(7) ?
S10' C102 . . 1.81(7) ?
C101 H101a . . 1.05 ?
C101 H101b . . 1.02 ?
C101 H101c . . .97 ?
C101 H101'a . . .90 ?
C101 H101'b . . 1.00 ?
C101 H101'c . . 1.09 ?
C102 H102a . . .89 ?
C102 H102b . . 1.03 ?
C102 H102c . . 1.03 ?
C102 H102'a . . 1.04 ?
C102 H102'b . . .97 ?
C102 H102'c . . .98 ?
O20 S20 . . 1.47(2) ?
O20 S20' . . 1.43(4) ?
S20 C201 . . 1.79(5) ?
S20 C202 . . 1.79(5) ?
S20' C201 . . 1.72(6) ?
S20' C202 . . 1.58(6) ?
C201 H201a . . .95 ?
C201 H201b . . 1.01 ?
C201 H201c . . .91 ?
C201 H201'a . . .95 ?
C201 H201'b . . .91 ?
C201 H201'c . . 1.00 ?
C202 H202a . . .86 ?
C202 H202b . . .96 ?
C202 H202c . . 1.03 ?
C202 H202'a . . 1.05 ?
C202 H202'b . . .94 ?
C202 H202'c . . .94 ?
O30 S30 . . 1.41(2) ?
O30 S30' . . 1.95(6) ?
S30 C301 . . 1.46(5) ?
S30 C302 . . 1.70(6) ?
S30' C301 . . 1.06(9) ?
S30' C302 . . 2.11(8) ?
S30' H301a . . 1.04 ?
C301 H301a . . .86 ?
C301 H301b . . 1.15 ?
C301 H301c . . 1.07 ?
C301 H301'a . . 1.05 ?
C301 H301'b . . 1.04 ?
C301 H301'c . . 1.09 ?
C302 H302a . . 1.07 ?
C302 H302b . . 1.03 ?
C302 H302c . . 1.07 ?
C302 H302'a . . 1.02 ?
C302 H302'b . . 1.01 ?
C302 H302'c . . 1.01 ?
O40 S40 . . 1.49(2) ?
O40 S40' . . 1.62(3) ?
S40 C401 . . 1.61(3) ?
S40 C402 . . 1.76(3) ?
S40' C401 . . 1.49(4) ?
S40' C402 . . 1.61(4) ?
S40' H401a . . 1.45 ?
S40' H402a . . 1.59 ?
C401 H401a . . .96 ?
C401 H401b . . 1.00 ?
C401 H401c . . 1.00 ?
C401 H401'a . . .94 ?
C401 H401'b . . 1.00 ?
C401 H401'c . . 1.01 ?
C402 H402a . . .94 ?
C402 H402b . . 1.03 ?
C402 H402c . . .94 ?
C402 H402'a . . .96 ?
C402 H402'b . . .95 ?
C402 H402'c . . 1.02 ?
O50 S50 . . 1.51(2) ?
O50 S50' . . 1.51(3) ?
S50 C501 . . 1.63(4) ?
S50 C502 . . 1.49(5) ?
S50' C501 . . 1.85(4) ?
S50' C502 . . 1.43(5) ?
S50' H502a . . 1.25 ?
C501 H501a . . .99 ?
C501 H501b . . .96 ?
C501 H501c . . .98 ?
C501 H501'a . . .92 ?
C501 H501'b . . 1.01 ?
C501 H501'c . . .97 ?
C502 H502a . . 1.02 ?
C502 H502b . . .95 ?
C502 H502c . . .93 ?
C502 H502'a . . .87 ?
C502 H502'b . . .98 ?
C502 H502'c . . .99 ?
O60 S60 . . 1.49(3) ?
O60 S60' . . 1.53(3) ?
S60 C601 . . 1.81(4) ?
S60 C602 . . 1.91(4) ?
S60' C601 . . 1.82(5) ?
S60' C602 . . 1.90(5) ?
C601 H601a . . .95 ?
C601 H601b . . .99 ?
C601 H601c . . .94 ?
C601 H601'a . . .94 ?
C601 H601'b . . .94 ?
C601 H601'c . . 1.00 ?
C602 H602a . . 1.09 ?
C602 H602b . . .92 ?
C602 H602c . . .87 ?
C602 H602'a . . .82 ?
C602 H602'b . . .95 ?
C602 H602'c . . 1.04 ?
N01 C011 . . .77(4) ?
C011 C012 . . 1.27(5) ?
N02 C021 . . .99(6) ?
C021 C022 . . 1.35(7) ?
N03 C031 . . 1.16(7) ?
C031 C032 . . 1.28(8) ?
N04 C041 . . 1.02(8) ?
C041 C042 . . 1.30(11) ?
