#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:07:58 +0100 (vie 25 de mar de 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029818.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029818
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.199(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.0020(8)
_cell_length_b                   16.7356(6)
_cell_length_c                   25.5607(14)
_cell_measurement_reflns_used    13001
_cell_measurement_temperature    440.00(10)
_cell_measurement_theta_max      28.7640
_cell_measurement_theta_min      3.1980
_cell_volume                     8516.2(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      440.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0299
_diffrn_reflns_av_sigmaI/netI    0.0327
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            19710
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    2.124
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.54231
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.234
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.220
_refine_diff_density_min         -0.855
_refine_diff_density_rms         0.150
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7308
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.067
_refine_ls_R_factor_all          0.0627
_refine_ls_R_factor_gt           0.0501
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0916P)²+54.8402P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1486
_refine_ls_wR_factor_ref         0.1619
_reflns_number_gt                5865
_reflns_number_total             7308
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           A_440K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029818.cif.
;
_cod_original_cell_volume        8516.2(6)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029818
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.0000 -0.03343(7) 0.2500 0.0624(3) Uani 1 2 d S
Mo2 Mo 0.00132(3) 0.09014(4) 0.13900(3) 0.03950(19) Uani 1 1 d .
Mo3 Mo 0.00803(3) 0.29018(4) 0.14242(3) 0.04164(19) Uani 1 1 d .
Mo4 Mo 0.0000 0.40691(8) 0.2500 0.0599(3) Uani 1 2 d S
Mo5 Mo 0.09227(3) 0.19249(4) 0.29003(3) 0.03916(19) Uani 1 1 d .
O1 O -0.0631(7) -0.0959(8) 0.2085(8) 0.194(7) Uani 1 1 d .
O2 O 0.0340(4) 0.0157(4) 0.2054(3) 0.0739(18) Uani 1 1 d .
O3 O -0.0531(4) 0.0298(5) 0.0853(3) 0.096(3) Uani 1 1 d .
O4 O 0.0725(4) 0.0819(5) 0.1302(3) 0.084(2) Uani 1 1 d .
O5 O 0.0519(4) 0.1863(4) 0.2144(3) 0.077(2) Uani 1 1 d .
O6 O 0.0763(4) 0.1042(5) 0.3232(3) 0.082(2) Uani 1 1 d .
O7 O 0.1762(3) 0.1959(4) 0.3173(3) 0.076(2) Uani 1 1 d .
O8 O 0.0663(4) 0.2802(4) 0.3169(3) 0.0752(19) Uani 1 1 d .
O9 O -0.0330(3) 0.1892(4) 0.1062(3) 0.0672(17) Uani 1 1 d .
O10 O 0.0775(4) 0.2874(5) 0.1289(4) 0.090(2) Uani 1 1 d .
O11 O -0.0443(4) 0.3495(6) 0.0912(3) 0.102(3) Uani 1 1 d .
O12 O 0.0463(4) 0.3579(4) 0.2108(3) 0.082(2) Uani 1 1 d .
O13 O -0.0589(5) 0.4658(6) 0.2024(4) 0.117(3) Uani 1 1 d .
Ag1 Ag -0.15577(3) -0.04333(5) -0.63317(3) 0.0598(2) Uani 1 1 d .
Ag2 Ag -0.17829(4) 0.25616(5) -0.13356(3) 0.0677(3) Uani 1 1 d .
C9 C 0.0976(3) 0.4716(4) -0.0009(3) 0.0343(15) Uani 1 1 d .
C12 C -0.4674(4) 0.3103(5) -0.5910(3) 0.0476(19) Uani 1 1 d .
H12A H -0.4460 0.2896 -0.6124 0.057 Uiso 1 1 calc R
C14 C -0.3766(3) 0.2557(4) -0.4997(3) 0.0332(14) Uani 1 1 d .
C16 C 0.0037(3) 0.3850(5) -0.0054(3) 0.0427(17) Uani 1 1 d .
H16A H 0.0235 0.3834 0.0348 0.051 Uiso 1 1 calc R
C18 C -0.4403(3) 0.3002(4) -0.5320(3) 0.0359(15) Uani 1 1 d .
C19 C 0.1817(3) 0.5526(4) 0.0053(3) 0.0366(15) Uani 1 1 d .
C20 C 0.0331(3) 0.4274(4) -0.0350(3) 0.0344(14) Uani 1 1 d .
C23 C -0.2025(3) 0.0837(4) -0.4963(3) 0.0409(16) Uani 1 1 d .
H23A H -0.1803 0.0877 -0.4563 0.049 Uiso 1 1 calc R
C24 C -0.2906(3) 0.2251(4) -0.4142(3) 0.0371(15) Uani 1 1 d .
C25 C -0.0558(4) 0.3448(5) -0.0371(3) 0.0449(17) Uani 1 1 d .
H25A H -0.0754 0.3169 -0.0168 0.054 Uiso 1 1 calc R
C27 C 0.2770(4) 0.6385(4) 0.0083(3) 0.0457(18) Uani 1 1 d .
H27A H 0.2978 0.6348 0.0485 0.055 Uiso 1 1 calc R
C29 C 0.2202(4) 0.6527(4) -0.1092(3) 0.0430(17) Uani 1 1 d .
H29A H 0.2004 0.6574 -0.1492 0.052 Uiso 1 1 calc R
C32 C -0.2573(4) 0.2367(5) -0.3505(3) 0.0417(16) Uani 1 1 d .
C33 C -0.2648(4) 0.1212(4) -0.5270(3) 0.0398(16) Uani 1 1 d .
C34 C 0.1788(4) 0.4558(6) 0.1790(4) 0.058(2) Uani 1 1 d .
H34A H 0.1348 0.4380 0.1587 0.069 Uiso 1 1 calc R
C35 C 0.2141(3) 0.6015(4) -0.0242(3) 0.0368(15) Uani 1 1 d .
C36 C -0.2646(4) 0.0643(5) -0.6126(3) 0.0462(18) Uani 1 1 d .
H36A H -0.2862 0.0573 -0.6524 0.055 Uiso 1 1 calc R
C38 C 0.2121(4) 0.4914(5) 0.1506(3) 0.0422(17) Uani 1 1 d .
C39 C -0.4742(4) 0.3343(5) -0.5024(3) 0.049(2) Uani 1 1 d .
H39A H -0.4568 0.3304 -0.4624 0.059 Uiso 1 1 calc R
C40 C -0.5328(4) 0.3735(6) -0.5325(4) 0.055(2) Uani 1 1 d .
H40A H -0.5547 0.3959 -0.5120 0.066 Uiso 1 1 calc R
C41 C 0.1799(3) 0.5021(4) 0.0862(3) 0.0385(16) Uani 1 1 d .
C43 C 0.1863(3) 0.6097(4) -0.0829(3) 0.0414(16) Uani 1 1 d .
H43A H 0.1448 0.5867 -0.1054 0.050 Uiso 1 1 calc R
C44 C 0.3068(4) 0.6807(5) -0.0218(4) 0.0496(19) Uani 1 1 d .
H44A H 0.3478 0.7055 -0.0007 0.059 Uiso 1 1 calc R
C45 C -0.2962(4) 0.1094(5) -0.5863(3) 0.0467(18) Uani 1 1 d .
H45A H -0.3381 0.1317 -0.6081 0.056 Uiso 1 1 calc R
C46 C -0.2949(3) 0.1718(4) -0.4966(3) 0.0364(15) Uani 1 1 d .
C47 C -0.5271(4) 0.3519(5) -0.6178(3) 0.0500(19) Uani 1 1 d .
H47A H -0.5444 0.3594 -0.6576 0.060 Uiso 1 1 calc R
C48 C -0.1750(4) 0.0406(5) -0.5271(3) 0.0448(17) Uani 1 1 d .
H48A H -0.1330 0.0175 -0.5066 0.054 Uiso 1 1 calc R
C50 C 0.0015(4) 0.4277(5) -0.0946(3) 0.0484(18) Uani 1 1 d .
H50A H 0.0192 0.4571 -0.1158 0.058 Uiso 1 1 calc R
C51 C 0.3056(4) 0.5048(6) 0.2405(4) 0.064(2) Uani 1 1 d .
H51A H 0.3495 0.5223 0.2615 0.077 Uiso 1 1 calc R
C53 C 0.2114(4) 0.4468(7) 0.2385(4) 0.066(3) Uani 1 1 d .
H53A H 0.1882 0.4232 0.2576 0.079 Uiso 1 1 calc R
C54 C -0.0562(4) 0.3843(5) -0.1222(3) 0.054(2) Uani 1 1 d .
H54A H -0.0755 0.3826 -0.1624 0.065 Uiso 1 1 calc R
C56 C -0.2552(5) 0.2948(6) -0.2650(4) 0.064(2) Uani 1 1 d .
H56A H -0.2738 0.3300 -0.2476 0.077 Uiso 1 1 calc R
C57 C 0.2777(4) 0.5165(5) 0.1818(4) 0.055(2) Uani 1 1 d .
H57A H 0.3019 0.5403 0.1638 0.066 Uiso 1 1 calc R
C58 C -0.2858(4) 0.2869(6) -0.3238(4) 0.058(2) Uani 1 1 d .
H58A H -0.3251 0.3146 -0.3456 0.069 Uiso 1 1 calc R
C59 C -0.1975(4) 0.1994(6) -0.3164(4) 0.058(2) Uani 1 1 d .
H59A H -0.1750 0.1683 -0.3327 0.070 Uiso 1 1 calc R
C60 C -0.1725(5) 0.2098(7) -0.2579(4) 0.072(3) Uani 1 1 d .
H60A H -0.1330 0.1830 -0.2352 0.086 Uiso 1 1 calc R
N1 N -0.2045(3) 0.0300(4) -0.5837(3) 0.0441(15) Uani 1 1 d .
N2 N -0.5610(3) 0.3817(4) -0.5900(3) 0.0476(16) Uani 1 1 d .
N3 N -0.1994(4) 0.2542(5) -0.2310(3) 0.0605(19) Uani 1 1 d .
N4 N -0.3522(3) 0.2101(4) -0.5292(3) 0.0392(13) Uani 1 1 d .
N5 N -0.3475(3) 0.2660(4) -0.4426(3) 0.0432(14) Uani 1 1 d .
N6 N -0.2625(3) 0.1774(4) -0.4391(3) 0.0403(14) Uani 1 1 d .
N7 N 0.2793(3) 0.6872(4) -0.0794(3) 0.0465(15) Uani 1 1 d .
N8 N -0.0866(3) 0.3437(4) -0.0944(3) 0.0469(15) Uani 1 1 d .
N9 N 0.2749(4) 0.4704(5) 0.2698(3) 0.0593(19) Uani 1 1 d .
N10 N 0.1255(3) 0.5129(3) -0.0282(2) 0.0372(13) Uani 1 1 d .
N11 N 0.1230(3) 0.4630(4) 0.0569(3) 0.0429(14) Uani 1 1 d .
N12 N 0.2109(3) 0.5490(4) 0.0631(3) 0.0433(14) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Mo1 O1 104.1(12) 2 .
O1 Mo1 O2 103.1(5) 2 .
O1 Mo1 O2 109.5(6) . .
O1 Mo1 O2 109.5(6) 2 2
O1 Mo1 O2 103.1(5) . 2
O2 Mo1 O2 125.8(4) . 2
O3 Mo2 O4 102.6(4) . .
O3 Mo2 O9 98.8(4) . .
O4 Mo2 O9 103.6(3) . .
O3 Mo2 O2 101.0(4) . .
O4 Mo2 O2 92.5(3) . .
O9 Mo2 O2 151.1(3) . .
O3 Mo2 O6 90.3(3) . 2
O4 Mo2 O6 164.6(3) . 2
O9 Mo2 O6 82.4(3) . 2
O2 Mo2 O6 76.6(3) . 2
O3 Mo2 O5 165.6(3) . .
O4 Mo2 O5 91.3(3) . .
O9 Mo2 O5 74.0(3) . .
O2 Mo2 O5 81.9(3) . .
O6 Mo2 O5 76.5(3) 2 .
O11 Mo3 O10 103.7(4) . .
O11 Mo3 O12 104.5(4) . .
O10 Mo3 O12 96.6(4) . .
O11 Mo3 O9 96.8(4) . .
O10 Mo3 O9 98.8(4) . .
O12 Mo3 O9 149.8(3) . .
O11 Mo3 O8 90.7(3) . 2
O10 Mo3 O8 165.0(3) . 2
O12 Mo3 O8 75.8(3) . 2
O9 Mo3 O8 82.9(3) . 2
O11 Mo3 O5 162.2(4) . .
O10 Mo3 O5 91.9(4) . .
O12 Mo3 O5 81.7(3) . .
O9 Mo3 O5 72.1(2) . .
O8 Mo3 O5 74.5(3) 2 .
O13 Mo4 O13 107.6(7) 2 .
O13 Mo4 O12 102.5(4) 2 .
O13 Mo4 O12 107.1(4) . .
O13 Mo4 O12 107.1(4) 2 2
O13 Mo4 O12 102.5(4) . 2
O12 Mo4 O12 128.7(4) . 2
O7 Mo5 O5 114.4(4) . .
O7 Mo5 O6 103.4(4) . .
O5 Mo5 O6 111.1(3) . .
O7 Mo5 O8 106.5(3) . .
O5 Mo5 O8 111.8(3) . .
O6 Mo5 O8 109.1(3) . .
Mo1 O2 Mo2 137.1(4) . .
Mo5 O5 Mo2 140.5(4) . .
Mo5 O5 Mo3 130.4(3) . .
Mo2 O5 Mo3 88.4(2) . .
Mo5 O6 Mo2 127.3(3) . 2
Mo5 O8 Mo3 129.3(4) . 2
Mo2 O9 Mo3 122.6(3) . .
Mo4 O12 Mo3 127.0(4) . .
N2 Ag1 N9 128.8(3) 3_545 3_444
N2 Ag1 N1 124.5(2) 3_545 .
N9 Ag1 N1 106.6(3) 3_444 .
N7 Ag2 N8 123.8(2) 3_445 .
N7 Ag2 N3 133.9(3) 3_445 .
N8 Ag2 N3 102.0(2) . .
N11 C9 N10 125.0(6) . .
N11 C9 C20 115.5(6) . .
N10 C9 C20 119.4(6) . .
C47 C12 C18 119.0(7) . .
N4 C14 N5 124.8(6) . .
N4 C14 C18 118.8(6) . .
N5 C14 C18 116.4(6) . .
C25 C16 C20 118.3(7) . .
C39 C18 C12 117.5(7) . .
C39 C18 C14 120.0(6) . .
C12 C18 C14 122.5(6) . .
N12 C19 N10 124.1(6) . .
N12 C19 C35 118.5(6) . .
N10 C19 C35 117.5(6) . .
C50 C20 C16 118.4(6) . .
C50 C20 C9 123.0(6) . .
C16 C20 C9 118.6(6) . .
C48 C23 C33 118.3(7) . .
N6 C24 N5 124.6(6) . .
N6 C24 C32 119.5(6) . .
N5 C24 C32 115.9(6) . .
N8 C25 C16 124.3(7) . .
C44 C27 C35 117.8(7) . .
N7 C29 C43 122.9(7) . .
C59 C32 C58 118.1(7) . .
C59 C32 C24 121.7(7) . .
C58 C32 C24 120.2(7) . .
C23 C33 C46 120.6(7) . .
C23 C33 C45 117.5(7) . .
C46 C33 C45 121.9(6) . .
C53 C34 C38 119.0(8) . .
C27 C35 C43 118.0(7) . .
C27 C35 C19 120.2(6) . .
C43 C35 C19 121.7(6) . .
C45 C36 N1 123.4(7) . .
C57 C38 C41 119.2(7) . .
C57 C38 C34 119.2(7) . .
C41 C38 C34 121.6(7) . .
C18 C39 C40 119.3(7) . .
C39 C40 N2 123.9(7) . .
N11 C41 N12 125.3(7) . .
N11 C41 C38 116.9(6) . .
N12 C41 C38 117.7(6) . .
C29 C43 C35 119.9(7) . .
C27 C44 N7 123.5(7) . .
C36 C45 C33 119.4(7) . .
N6 C46 N4 124.7(6) . .
N6 C46 C33 118.0(6) . .
N4 C46 C33 117.3(6) . .
C12 C47 N2 123.6(7) . .
N1 C48 C23 124.4(7) . .
C20 C50 C54 119.1(7) . .
C57 C51 N9 125.3(8) . .
N9 C53 C34 123.0(8) . .
N8 C54 C50 123.7(7) . .
C58 C56 N3 123.1(8) . .
C51 C57 C38 117.4(8) . .
C56 C58 C32 119.1(8) . .
C32 C59 C60 117.7(8) . .
N3 C60 C59 125.8(9) . .
C48 N1 C36 117.0(6) . .
C48 N1 Ag1 122.8(5) . .
C36 N1 Ag1 120.2(5) . .
C47 N2 C40 116.5(6) . .
C47 N2 Ag1 123.7(5) . 3_455
C40 N2 Ag1 119.4(5) . 3_455
C60 N3 C56 115.9(7) . .
C60 N3 Ag2 129.7(6) . .
C56 N3 Ag2 113.2(6) . .
C14 N4 C46 114.8(6) . .
C14 N5 C24 115.5(6) . .
C24 N6 C46 115.5(6) . .
C29 N7 C44 117.9(7) . .
C29 N7 Ag2 115.2(5) . 3
C44 N7 Ag2 126.8(5) . 3
C25 N8 C54 116.1(6) . .
C25 N8 Ag2 115.0(5) . .
C54 N8 Ag2 128.3(5) . .
C53 N9 C51 116.1(7) . .
C53 N9 Ag1 131.1(6) . 3_556
C51 N9 Ag1 112.7(5) . 3_556
C9 N10 C19 115.8(6) . .
C9 N11 C41 114.7(6) . .
C19 N12 C41 114.9(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O1 1.701(11) 2
Mo1 O1 1.701(11) .
Mo1 O2 1.806(7) .
Mo1 O2 1.806(7) 2
Mo2 O3 1.713(7) .
Mo2 O4 1.679(7) .
Mo2 O9 1.866(7) .
Mo2 O2 1.977(7) .
Mo2 O6 2.305(7) 2
Mo2 O5 2.391(7) .
Mo3 O11 1.655(7) .
Mo3 O10 1.704(7) .
Mo3 O12 1.948(7) .
Mo3 O9 1.954(7) .
Mo3 O8 2.287(7) 2
Mo3 O5 2.413(7) .
Mo4 O13 1.670(9) 2
Mo4 O13 1.670(9) .
Mo4 O12 1.894(8) .
Mo4 O12 1.894(7) 2
Mo5 O7 1.675(6) .
Mo5 O5 1.754(7) .
Mo5 O6 1.810(7) .
Mo5 O8 1.813(7) .
O6 Mo2 2.305(7) 2
O8 Mo3 2.287(7) 2
Ag1 N2 2.276(6) 3_545
Ag1 N9 2.304(7) 3_444
Ag1 N1 2.325(6) .
Ag2 N7 2.283(6) 3_445
Ag2 N8 2.345(6) .
Ag2 N3 2.330(7) .
C9 N11 1.347(9) .
C9 N10 1.306(9) .
C9 C20 1.508(9) .
C12 C47 1.382(11) .
C12 C18 1.375(10) .
C14 N4 1.337(9) .
C14 N5 1.332(9) .
C14 C18 1.487(9) .
C16 C25 1.385(10) .
C16 C20 1.382(10) .
C18 C39 1.391(10) .
C19 N12 1.338(9) .
C19 N10 1.343(9) .
C19 C35 1.483(10) .
C20 C50 1.379(10) .
C23 C48 1.380(10) .
C23 C33 1.405(10) .
C24 N6 1.325(9) .
C24 N5 1.338(9) .
C24 C32 1.486(10) .
C25 N8 1.328(10) .
C27 C44 1.397(10) .
C27 C35 1.418(10) .
C29 N7 1.328(10) .
C29 C43 1.397(10) .
C32 C59 1.379(11) .
C32 C58 1.388(11) .
C33 C46 1.483(10) .
C33 C45 1.385(11) .
C34 C53 1.385(11) .
C34 C38 1.370(11) .
C35 C43 1.365(10) .
C36 C45 1.377(10) .
C36 N1 1.340(10) .
C38 C57 1.384(11) .
C38 C41 1.499(10) .
C39 C40 1.356(11) .
C40 N2 1.335(10) .
C41 N11 1.325(9) .
C41 N12 1.333(9) .
C44 N7 1.336(10) .
C46 N6 1.337(9) .
C46 N4 1.342(9) .
C47 N2 1.329(10) .
C48 N1 1.322(10) .
C50 C54 1.370(11) .
C51 C57 1.370(12) .
C51 N9 1.335(12) .
C53 N9 1.341(11) .
C54 N8 1.348(10) .
C56 C58 1.367(12) .
C56 N3 1.349(12) .
C59 C60 1.368(12) .
C60 N3 1.313(12) .
N2 Ag1 2.276(6) 3_455
N7 Ag2 2.283(6) 3
N9 Ag1 2.304(7) 3_556
