Information card for entry 7032802

Structure parameters

• Formula: C46 H43 Cl N6 Ni O6 P2
• Calculated formula: C46 H43 Cl N6 Ni O6 P2
• Title of publication: P,C-bond cleavage in the ligand sphere of a nickel(II) complex.
• Authors of publication: Walg, Simon P.; Schmidt, Alexandra D.; Schmitz, Marcus; Farsadpour, Saeid; Lang, Johannes; Niebergall, Mark; Sun, Yu; Roesky, Peter W.; Niedner-Schatteburg, Gereon; Thiel, Werner R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 3
• Pages of publication: 1317 - 1322
• a: 11.6115 ± 0.0007 Å
• b: 13.4918 ± 0.0009 Å
• c: 14.9171 ± 0.001 Å
• α: 87.203 ± 0.005°
• β: 75.689 ± 0.006°
• γ: 70.567 ± 0.006°
• Cell volume: 2134 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0599
• Residual factor for significantly intense reflections: 0.0516
• Weighted residual factors for significantly intense reflections: 0.131
• Weighted residual factors for all reflections included in the refinement: 0.1386
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No