Information card for entry 7033069

Structure parameters

• Formula: C36.5 H44 Ca O
• Calculated formula: C36.5 H44 Ca O
• Title of publication: Unprecedented silicon(II)→calcium complexes with N-heterocyclic silylenes.
• Authors of publication: Blom, Burgert; Klatt, Günter; Gallego, Daniel; Tan, Gengwen; Driess, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 639 - 644
• a: 9.9184 ± 0.0001 Å
• b: 14.1228 ± 0.0001 Å
• c: 23.6163 ± 0.0003 Å
• α: 90°
• β: 101.909 ± 0.001°
• γ: 90°
• Cell volume: 3236.87 ± 0.06 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1442
• Weighted residual factors for all reflections included in the refinement: 0.1445
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No