#------------------------------------------------------------------------------
#$Date: 2019-03-05 09:52:05 +0100 (mar 05 de mar de 2019) $
#$Revision: 213973 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/05/7050572.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7050572
loop_
_publ_author_name
'Patra, Goutam Kumar'
'Goldberg, Israel'
_publ_section_title
;
 The synthesis and characterization of a series of bis-bidentate Schiff
 base ligands and their coordination complexes with silver(i),
 copper(i) and zinc(ii) d10 metal ionsElectronic supplementary
 information (ESI) available: Views of the crystal structures of
 ligands of 1, 2 and 3. See http://www.rsc.org/suppdata/nj/b3/b301632c/
;
_journal_issue                   7
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              1124
_journal_paper_doi               10.1039/b301632c
_journal_volume                  27
_journal_year                    2003
_chemical_formula_moiety         '(C34 H24 N6), (Ag Cl O4), (C H2 Cl2)'
_chemical_formula_sum            'C35 H26 Ag Cl3 N6 O4'
_chemical_formula_weight         808.84
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 125.8021(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   27.9900(3)
_cell_length_b                   12.7440(2)
_cell_length_c                   22.6650(3)
_cell_measurement_reflns_used    5654
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      27.90
_cell_measurement_theta_min      2.22
_cell_volume                     6557.04(16)
_computing_cell_refinement       Denzo
_computing_data_collection       'Collect, Nonius B.V.'
_computing_data_reduction        Denzo
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    DIRDIF-96
_diffrn_ambient_temperature      110(2)
_diffrn_detector_area_resol_mean '56 microns'
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       '1 deg. Phi scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0620
_diffrn_reflns_limit_h_max       36
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            7695
_diffrn_reflns_theta_full        27.90
_diffrn_reflns_theta_max         27.90
_diffrn_reflns_theta_min         2.22
_exptl_absorpt_coefficient_mu    0.910
_exptl_absorpt_correction_T_max  0.9145
_exptl_absorpt_correction_T_min  0.8044
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Blessing, 1995'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.639
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prisms
_exptl_crystal_F_000             3264
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.598
_refine_diff_density_min         -0.719
_refine_diff_density_rms         0.099
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     442
_refine_ls_number_reflns         7695
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.0710
_refine_ls_R_factor_gt           0.0415
_refine_ls_shift/su_max          0.040
_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0436P)²+12.7901P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0911
_refine_ls_wR_factor_ref         0.1026
_reflns_number_gt                5654
_reflns_number_total             7695
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b301632c.txt
_cod_data_source_block           Complex-2a
_cod_original_cell_volume        6557.04(15)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7050572
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
N1 N 0.01107(11) 0.12905(19) 0.35132(13) 0.0179(5) Uani 1 1 d . . .
C2 C -0.02295(13) 0.0884(2) 0.37081(16) 0.0215(7) Uani 1 1 d . . .
C3 C -0.05600(15) 0.1573(3) 0.38292(18) 0.0298(8) Uani 1 1 d . . .
H3 H -0.0552 0.2307 0.3762 0.036 Uiso 1 1 calc R . .
C4 C -0.08914(17) 0.1184(3) 0.4043(2) 0.0376(9) Uani 1 1 d . . .
H4 H -0.1117 0.1649 0.4116 0.045 Uiso 1 1 calc R . .
C5 C -0.09012(17) 0.0097(3) 0.4155(2) 0.0395(9) Uani 1 1 d . . .
H5 H -0.1123 -0.0162 0.4319 0.047 Uiso 1 1 calc R . .
C6 C -0.05968(16) -0.0578(3) 0.4031(2) 0.0378(9) Uani 1 1 d . . .
H6 H -0.0612 -0.1308 0.4102 0.045 Uiso 1 1 calc R . .
C7 C -0.02551(15) -0.0210(3) 0.37948(18) 0.0285(8) Uani 1 1 d . . .
C8 C 0.00553(16) -0.0871(3) 0.3640(2) 0.0360(9) Uani 1 1 d . . .
H8 H 0.0029 -0.1610 0.3667 0.043 Uiso 1 1 calc R . .
C9 C 0.03986(15) -0.0458(2) 0.34479(19) 0.0290(8) Uani 1 1 d . . .
H9 H 0.0616 -0.0902 0.3349 0.035 Uiso 1 1 calc R . .
C10 C 0.04203(13) 0.0633(2) 0.34024(16) 0.0185(6) Uani 1 1 d . . .
C11 C 0.08058(13) 0.1079(2) 0.32239(15) 0.0184(6) Uani 1 1 d . . .
H11 H 0.1023 0.0622 0.3131 0.022 Uiso 1 1 calc R . .
N12 N 0.08546(10) 0.20706(18) 0.31912(13) 0.0167(5) Uani 1 1 d . . .
N13 N 0.12468(11) 0.23130(19) 0.30138(13) 0.0175(5) Uani 1 1 d . . .
C14 C 0.14299(13) 0.3268(2) 0.31377(15) 0.0168(6) Uani 1 1 d . . .
C15 C 0.12576(12) 0.4075(2) 0.34704(15) 0.0157(6) Uani 1 1 d . . .
N16 N 0.08164(10) 0.46976(18) 0.30796(13) 0.0170(5) Uani 1 1 d . . .
N17 N 0.04759(10) 0.45011(19) 0.23283(12) 0.0160(5) Uani 1 1 d . . .
C18 C 0.03233(13) 0.5320(2) 0.19373(16) 0.0188(6) Uani 1 1 d . . .
H18 H 0.0460 0.5989 0.2160 0.023 Uiso 1 1 calc R . .
C19 C -0.00654(13) 0.5234(2) 0.11400(16) 0.0181(6) Uani 1 1 d . . .
C20 C -0.01680(15) 0.6125(2) 0.07121(17) 0.0240(7) Uani 1 1 d . . .
H20 H 0.0011 0.6778 0.0935 0.029 Uiso 1 1 calc R . .
C21 C -0.05298(15) 0.6035(2) -0.00311(18) 0.0267(7) Uani 1 1 d . . .
H21 H -0.0608 0.6631 -0.0326 0.032 Uiso 1 1 calc R . .
C22 C -0.07864(14) 0.5060(2) -0.03581(17) 0.0236(7) Uani 1 1 d . . .
C23 C -0.11508(15) 0.4892(3) -0.11155(18) 0.0290(8) Uani 1 1 d . . .
H23 H -0.1243 0.5463 -0.1436 0.035 Uiso 1 1 calc R . .
C24 C -0.13716(15) 0.3922(3) -0.13928(18) 0.0324(8) Uani 1 1 d . . .
H24 H -0.1612 0.3818 -0.1904 0.039 Uiso 1 1 calc R . .
C25 C -0.12470(14) 0.3075(3) -0.09272(17) 0.0265(7) Uani 1 1 d . . .
H25 H -0.1408 0.2404 -0.1129 0.032 Uiso 1 1 calc R . .
C26 C -0.08964(13) 0.3197(2) -0.01858(17) 0.0223(7) Uani 1 1 d . . .
H26 H -0.0814 0.2616 0.0123 0.027 Uiso 1 1 calc R . .
C27 C -0.06593(13) 0.4196(2) 0.01148(16) 0.0184(6) Uani 1 1 d . . .
N28 N -0.03060(11) 0.43028(19) 0.08529(13) 0.0176(5) Uani 1 1 d . . .
C29 C 0.18388(13) 0.3589(2) 0.29607(15) 0.0203(6) Uani 1 1 d . . .
C30 C 0.20786(13) 0.4587(3) 0.31255(16) 0.0228(7) Uani 1 1 d . . .
H30 H 0.1970 0.5083 0.3340 0.027 Uiso 1 1 calc R . .
C31 C 0.24817(14) 0.4868(3) 0.29759(18) 0.0293(8) Uani 1 1 d . . .
H31 H 0.2647 0.5552 0.3093 0.035 Uiso 1 1 calc R . .
C32 C 0.26403(14) 0.4157(3) 0.26605(18) 0.0320(8) Uani 1 1 d . . .
H32 H 0.2920 0.4346 0.2569 0.038 Uiso 1 1 calc R . .
C33 C 0.23897(15) 0.3163(3) 0.24769(18) 0.0311(8) Uani 1 1 d . . .
H33 H 0.2486 0.2681 0.2241 0.037 Uiso 1 1 calc R . .
C34 C 0.20014(15) 0.2873(3) 0.26365(17) 0.0248(7) Uani 1 1 d . . .
H34 H 0.1843 0.2183 0.2526 0.030 Uiso 1 1 calc R . .
C35 C 0.16199(12) 0.4204(2) 0.42656(15) 0.0159(6) Uani 1 1 d . . .
C36 C 0.19039(13) 0.3335(2) 0.47195(16) 0.0201(6) Uani 1 1 d . . .
H36 H 0.1868 0.2665 0.4514 0.024 Uiso 1 1 calc R . .
C37 C 0.22379(14) 0.3450(3) 0.54699(17) 0.0247(7) Uani 1 1 d . . .
H37 H 0.2423 0.2857 0.5776 0.030 Uiso 1 1 calc R . .
C38 C 0.23008(14) 0.4428(3) 0.57708(17) 0.0273(7) Uani 1 1 d . . .
H38 H 0.2538 0.4508 0.6285 0.033 Uiso 1 1 calc R . .
C39 C 0.20198(14) 0.5294(3) 0.53268(17) 0.0251(7) Uani 1 1 d . . .
H39 H 0.2062 0.5962 0.5539 0.030 Uiso 1 1 calc R . .
C40 C 0.16774(13) 0.5192(2) 0.45758(16) 0.0208(7) Uani 1 1 d . . .
H40 H 0.1483 0.5786 0.4273 0.025 Uiso 1 1 calc R . .
Ag41 Ag 0.015036(10) 0.303141(17) 0.332414(13) 0.02136(8) Uani 1 1 d . . .
Cl42 Cl 0.35811(4) 0.28000(6) 0.19851(4) 0.02498(18) Uani 1 1 d . . .
O43 O 0.34717(12) 0.38973(18) 0.18346(15) 0.0418(7) Uani 1 1 d . . .
O44 O 0.38557(15) 0.2608(2) 0.27359(15) 0.0550(8) Uani 1 1 d . . .
O45 O 0.30413(14) 0.2235(2) 0.1578(2) 0.0749(11) Uani 1 1 d . . .
O46 O 0.39622(17) 0.2455(2) 0.1802(2) 0.0666(10) Uani 1 1 d . . .
C47 C 0.30220(17) 0.3882(3) 0.0029(2) 0.0365(9) Uani 1 1 d . . .
H47A H 0.3055 0.3766 0.0483 0.044 Uiso 1 1 calc R . .
H47B H 0.2610 0.3733 -0.0386 0.044 Uiso 1 1 calc R . .
Cl48 Cl 0.34988(4) 0.30062(7) 0.00017(6) 0.0417(2) Uani 1 1 d . . .
Cl49 Cl 0.31880(4) 0.52085(7) -0.00114(5) 0.0365(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C10 N1 C2 118.5(3) . . ?
C10 N1 Ag41 118.0(2) . . ?
C2 N1 Ag41 123.5(2) . . ?
N1 C2 C7 121.4(3) . . ?
N1 C2 C3 119.1(3) . . ?
C7 C2 C3 119.5(3) . . ?
C4 C3 C2 120.0(3) . . ?
C4 C3 H3 120.0 . . ?
C2 C3 H3 120.0 . . ?
C3 C4 C5 120.6(4) . . ?
C3 C4 H4 119.7 . . ?
C5 C4 H4 119.7 . . ?
C6 C5 C4 120.4(3) . . ?
C6 C5 H5 119.8 . . ?
C4 C5 H5 119.8 . . ?
C5 C6 C7 121.0(3) . . ?
C5 C6 H6 119.5 . . ?
C7 C6 H6 119.5 . . ?
C8 C7 C2 118.0(3) . . ?
C8 C7 C6 123.5(3) . . ?
C2 C7 C6 118.5(3) . . ?
C9 C8 C7 120.3(3) . . ?
C9 C8 H8 119.9 . . ?
C7 C8 H8 119.9 . . ?
C8 C9 C10 118.3(3) . . ?
C8 C9 H9 120.9 . . ?
C10 C9 H9 120.9 . . ?
N1 C10 C9 123.4(3) . . ?
N1 C10 C11 118.2(3) . . ?
C9 C10 C11 118.4(3) . . ?
N12 C11 C10 121.3(3) . . ?
N12 C11 H11 119.4 . . ?
C10 C11 H11 119.4 . . ?
C11 N12 N13 111.2(2) . . ?
C11 N12 Ag41 111.2(2) . . ?
N13 N12 Ag41 137.20(17) . . ?
C14 N13 N12 115.1(2) . . ?
N13 C14 C29 118.5(3) . . ?
N13 C14 C15 123.4(3) . . ?
C29 C14 C15 118.1(3) . . ?
N16 C15 C35 118.1(3) . . ?
N16 C15 C14 122.2(3) . . ?
C35 C15 C14 119.6(2) . . ?
C15 N16 N17 114.9(2) . . ?
C18 N17 N16 114.3(2) . . ?
C18 N17 Ag41 112.7(2) . 2 ?
N16 N17 Ag41 128.36(17) . 2 ?
N17 C18 C19 120.1(3) . . ?
N17 C18 H18 120.0 . . ?
C19 C18 H18 120.0 . . ?
N28 C19 C20 122.7(3) . . ?
N28 C19 C18 117.8(3) . . ?
C20 C19 C18 119.5(3) . . ?
C21 C20 C19 119.0(3) . . ?
C21 C20 H20 120.5 . . ?
C19 C20 H20 120.5 . . ?
C20 C21 C22 120.2(3) . . ?
C20 C21 H21 119.9 . . ?
C22 C21 H21 119.9 . . ?
C21 C22 C23 123.9(3) . . ?
C21 C22 C27 117.3(3) . . ?
C23 C22 C27 118.9(3) . . ?
C24 C23 C22 120.7(3) . . ?
C24 C23 H23 119.7 . . ?
C22 C23 H23 119.7 . . ?
C23 C24 C25 120.4(3) . . ?
C23 C24 H24 119.8 . . ?
C25 C24 H24 119.8 . . ?
C26 C25 C24 121.2(3) . . ?
C26 C25 H25 119.4 . . ?
C24 C25 H25 119.4 . . ?
C25 C26 C27 119.4(3) . . ?
C25 C26 H26 120.3 . . ?
C27 C26 H26 120.3 . . ?
N28 C27 C26 118.7(3) . . ?
N28 C27 C22 121.8(3) . . ?
C26 C27 C22 119.5(3) . . ?
C19 N28 C27 119.0(3) . . ?
C19 N28 Ag41 115.32(19) . 2 ?
C27 N28 Ag41 125.4(2) . 2 ?
C30 C29 C34 119.0(3) . . ?
C30 C29 C14 120.9(3) . . ?
C34 C29 C14 120.2(3) . . ?
C29 C30 C31 120.1(3) . . ?
C29 C30 H30 119.9 . . ?
C31 C30 H30 120.0 . . ?
C32 C31 C30 120.5(3) . . ?
C32 C31 H31 119.8 . . ?
C30 C31 H31 119.8 . . ?
C31 C32 C33 119.7(3) . . ?
C31 C32 H32 120.2 . . ?
C33 C32 H32 120.2 . . ?
C34 C33 C32 120.2(3) . . ?
C34 C33 H33 119.9 . . ?
C32 C33 H33 119.9 . . ?
C33 C34 C29 120.6(3) . . ?
C33 C34 H34 119.7 . . ?
C29 C34 H34 119.7 . . ?
C36 C35 C40 119.5(3) . . ?
C36 C35 C15 120.0(3) . . ?
C40 C35 C15 120.5(3) . . ?
C37 C36 C35 120.1(3) . . ?
C37 C36 H36 119.9 . . ?
C35 C36 H36 119.9 . . ?
C38 C37 C36 120.0(3) . . ?
C38 C37 H37 120.0 . . ?
C36 C37 H37 120.0 . . ?
C37 C38 C39 120.3(3) . . ?
C37 C38 H38 119.8 . . ?
C39 C38 H38 119.8 . . ?
C40 C39 C38 120.5(3) . . ?
C40 C39 H39 119.8 . . ?
C38 C39 H39 119.8 . . ?
C39 C40 C35 119.5(3) . . ?
C39 C40 H40 120.2 . . ?
C35 C40 H40 120.2 . . ?
N1 Ag41 N28 122.59(8) . 2 ?
N1 Ag41 N17 141.31(8) . 2 ?
N28 Ag41 N17 71.00(8) 2 2 ?
N1 Ag41 N12 70.83(8) . . ?
N28 Ag41 N12 130.92(8) 2 . ?
N17 Ag41 N12 131.05(8) 2 . ?
N1 Ag41 Ag41 101.78(6) . 2 ?
N28 Ag41 Ag41 135.50(6) 2 2 ?
N17 Ag41 Ag41 72.09(6) 2 2 ?
N12 Ag41 Ag41 63.87(5) . 2 ?
O46 Cl42 O44 108.9(2) . . ?
O46 Cl42 O45 110.4(2) . . ?
O44 Cl42 O45 108.4(2) . . ?
O46 Cl42 O43 109.00(17) . . ?
O44 Cl42 O43 110.17(17) . . ?
O45 Cl42 O43 110.04(19) . . ?
Cl48 C47 Cl49 112.0(2) . . ?
Cl48 C47 H47A 109.2 . . ?
Cl49 C47 H47A 109.2 . . ?
Cl48 C47 H47B 109.2 . . ?
Cl49 C47 H47B 109.2 . . ?
H47A C47 H47B 107.9 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
N1 C10 1.330(4) . ?
N1 C2 1.365(4) . ?
N1 Ag41 2.275(2) . ?
C2 C7 1.416(5) . ?
C2 C3 1.414(5) . ?
C3 C4 1.366(5) . ?
C3 H3 0.9500 . ?
C4 C5 1.411(5) . ?
C4 H4 0.9500 . ?
C5 C6 1.351(5) . ?
C5 H5 0.9500 . ?
C6 C7 1.420(5) . ?
C6 H6 0.9500 . ?
C7 C8 1.394(5) . ?
C8 C9 1.370(5) . ?
C8 H8 0.9500 . ?
C9 C10 1.399(4) . ?
C9 H9 0.9500 . ?
C10 C11 1.470(4) . ?
C11 N12 1.277(4) . ?
C11 H11 0.9500 . ?
N12 N13 1.407(3) . ?
N12 Ag41 2.484(2) . ?
N13 C14 1.286(4) . ?
C14 C29 1.475(4) . ?
C14 C15 1.512(4) . ?
C15 N16 1.288(4) . ?
C15 C35 1.472(4) . ?
N16 N17 1.404(3) . ?
N17 C18 1.271(4) . ?
N17 Ag41 2.395(2) 2 ?
C18 C19 1.470(4) . ?
C18 H18 0.9500 . ?
C19 N28 1.331(4) . ?
C19 C20 1.409(4) . ?
C20 C21 1.371(5) . ?
C20 H20 0.9500 . ?
C21 C22 1.409(5) . ?
C21 H21 0.9500 . ?
C22 C23 1.408(5) . ?
C22 C27 1.429(4) . ?
C23 C24 1.360(5) . ?
C23 H23 0.9500 . ?
C24 C25 1.404(5) . ?
C24 H24 0.9500 . ?
C25 C26 1.372(4) . ?
C25 H25 0.9500 . ?
C26 C27 1.412(4) . ?
C26 H26 0.9500 . ?
C27 N28 1.364(4) . ?
N28 Ag41 2.312(2) 2 ?
C29 C30 1.384(4) . ?
C29 C34 1.404(4) . ?
C30 C31 1.401(5) . ?
C30 H30 0.9500 . ?
C31 C32 1.378(5) . ?
C31 H31 0.9500 . ?
C32 C33 1.389(5) . ?
C32 H32 0.9500 . ?
C33 C34 1.381(5) . ?
C33 H33 0.9500 . ?
C34 H34 0.9500 . ?
C35 C36 1.400(4) . ?
C35 C40 1.405(4) . ?
C36 C37 1.389(4) . ?
C36 H36 0.9500 . ?
C37 C38 1.381(5) . ?
C37 H37 0.9500 . ?
C38 C39 1.387(5) . ?
C38 H38 0.9500 . ?
C39 C40 1.387(4) . ?
C39 H39 0.9500 . ?
C40 H40 0.9500 . ?
Ag41 N28 2.312(2) 2 ?
Ag41 N17 2.395(2) 2 ?
Ag41 Ag41 3.3145(5) 2 ?
Cl42 O46 1.421(3) . ?
Cl42 O44 1.420(3) . ?
Cl42 O45 1.422(3) . ?
Cl42 O43 1.430(2) . ?
C47 Cl48 1.769(4) . ?
C47 Cl49 1.769(4) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
