#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:05:10 +0100 (vie 25 de mar de 2016) $
#$Revision: 180059 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/05/7050597.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7050597
loop_
_publ_author_name
'Kay Lee, Hung'
'Suet Lam, Tung'
'Lam, Chi-Keung'
'Li, Hung-Wing'
'Man Fung, Sze'
_publ_section_title
;
 Synthesis and structural characterisation of divalent transition metal
 complexes containing an unsymmetrical benzamidinate ligandElectronic
 supplementary information (ESI) available: inclination angles in
 complexes 1?6. See http://www.rsc.org/suppdata/nj/b3/b303527a//
;
_journal_issue                   9
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              1310
_journal_paper_doi               10.1039/b303527a
_journal_volume                  27
_journal_year                    2003
_chemical_formula_sum            'C78 H108 Co2 N10 Si4'
_chemical_formula_weight         1415.96
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.250(2)
_cell_angle_beta                 104.354(2)
_cell_angle_gamma                95.475(2)
_cell_formula_units_Z            1
_cell_length_a                   10.9563(9)
_cell_length_b                   11.6745(9)
_cell_length_c                   17.633(1)
_cell_measurement_temperature    293(2)
_cell_volume                     2038.1(3)
_computing_cell_refinement       'Bruker SMART CCD Diffractometer'
_computing_data_collection       'Bruker SMART CCD Diffractometer'
_computing_data_reduction        'Bruker SMART CCD Diffractometer'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.973
_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'Bruker SMART CCD Diffractometer'
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0215
_diffrn_reflns_av_sigmaI/netI    0.0553
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            13501
_diffrn_reflns_theta_full        28.03
_diffrn_reflns_theta_max         28.03
_diffrn_reflns_theta_min         1.27
_exptl_absorpt_coefficient_mu    0.511
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.6742
_exptl_absorpt_correction_type   SADABS
_exptl_crystal_colour            Blue
_exptl_crystal_density_diffrn    1.154
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             756
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.43
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.312
_refine_diff_density_min         -0.349
_refine_diff_density_rms         0.047
_refine_ls_extinction_coef       0.0002(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.943
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     425
_refine_ls_number_reflns         9622
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.943
_refine_ls_R_factor_all          0.0802
_refine_ls_R_factor_gt           0.0465
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0673P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1172
_refine_ls_wR_factor_ref         0.1312
_reflns_number_gt                6064
_reflns_number_total             9622
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b303527a.txt
_cod_data_source_block           Compound_5
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7050597
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.51755(3) 0.02918(3) 0.715548(18) 0.04106(11) Uani 1 1 d . . .
Si1 Si 0.39126(7) -0.31095(7) 0.62218(5) 0.0574(2) Uani 1 1 d . . .
Si2 Si 0.59688(8) 0.36430(7) 0.81087(6) 0.0609(2) Uani 1 1 d . . .
N1 N 0.32748(17) 0.02409(17) 0.70203(12) 0.0438(5) Uani 1 1 d . . .
N2 N 0.38818(18) -0.15592(17) 0.65317(12) 0.0444(5) Uani 1 1 d . . .
N3 N 0.65085(17) 0.04126(16) 0.82105(11) 0.0413(4) Uani 1 1 d . . .
N4 N 0.61216(18) 0.21549(17) 0.80163(12) 0.0453(5) Uani 1 1 d . . .
N5 N 0.59628(18) 0.02425(18) 0.61405(11) 0.0467(5) Uani 1 1 d . . .
C1 C 0.2938(2) -0.0971(2) 0.66669(14) 0.0415(5) Uani 1 1 d . . .
C2 C 0.1583(2) -0.1630(2) 0.64550(16) 0.0487(6) Uani 1 1 d . . .
C3 C 0.1007(3) -0.1589(3) 0.7068(2) 0.0678(8) Uani 1 1 d . . .
H3A H 0.1437 -0.1103 0.7619 0.081 Uiso 1 1 calc R . .
C4 C -0.0208(3) -0.2266(3) 0.6875(3) 0.0963(12) Uani 1 1 d . . .
H4A H -0.0590 -0.2239 0.7295 0.116 Uiso 1 1 calc R . .
C5 C -0.0845(3) -0.2977(3) 0.6062(3) 0.0998(13) Uani 1 1 d . . .
H5A H -0.1658 -0.3437 0.5933 0.120 Uiso 1 1 calc R . .
C6 C -0.0303(3) -0.3016(3) 0.5445(3) 0.0883(11) Uani 1 1 d . . .
H6A H -0.0749 -0.3489 0.4894 0.106 Uiso 1 1 calc R . .
C7 C 0.0922(3) -0.2349(2) 0.56361(19) 0.0666(8) Uani 1 1 d . . .
H7A H 0.1298 -0.2385 0.5213 0.080 Uiso 1 1 calc R . .
C8 C 0.2395(2) 0.1040(2) 0.71899(17) 0.0500(6) Uani 1 1 d . . .
C9 C 0.2440(3) 0.1644(2) 0.8020(2) 0.0637(8) Uani 1 1 d . . .
C10 C 0.1643(4) 0.2490(3) 0.8182(3) 0.0906(11) Uani 1 1 d . . .
H10A H 0.1677 0.2910 0.8733 0.109 Uiso 1 1 calc R . .
C11 C 0.0810(4) 0.2719(3) 0.7554(3) 0.1028(14) Uani 1 1 d . . .
H11A H 0.0266 0.3270 0.7675 0.123 Uiso 1 1 calc R . .
C12 C 0.0782(3) 0.2129(3) 0.6738(3) 0.0877(11) Uani 1 1 d . . .
H12A H 0.0213 0.2286 0.6311 0.105 Uiso 1 1 calc R . .
C13 C 0.1583(2) 0.1305(2) 0.6541(2) 0.0600(7) Uani 1 1 d . . .
C14 C 0.1629(3) 0.0778(3) 0.5668(2) 0.0775(9) Uani 1 1 d . . .
H14A H 0.2234 0.0234 0.5641 0.116 Uiso 1 1 calc R . .
H14B H 0.1889 0.1429 0.5484 0.116 Uiso 1 1 calc R . .
H14C H 0.0795 0.0331 0.5312 0.116 Uiso 1 1 calc R . .
C15 C 0.3325(3) 0.1390(3) 0.8721(2) 0.0857(10) Uani 1 1 d . . .
H15A H 0.3224 0.1883 0.9243 0.129 Uiso 1 1 calc R . .
H15B H 0.4195 0.1588 0.8721 0.129 Uiso 1 1 calc R . .
H15C H 0.3122 0.0537 0.8648 0.129 Uiso 1 1 calc R . .
C16 C 0.2778(3) -0.4046(3) 0.6532(3) 0.0900(11) Uani 1 1 d . . .
H16A H 0.1915 -0.3971 0.6292 0.135 Uiso 1 1 calc R . .
H16B H 0.2976 -0.3756 0.7130 0.135 Uiso 1 1 calc R . .
H16C H 0.2860 -0.4892 0.6334 0.135 Uiso 1 1 calc R . .
C17 C 0.3578(4) -0.3776(3) 0.5064(2) 0.0972(12) Uani 1 1 d . . .
H17A H 0.2734 -0.3686 0.4796 0.146 Uiso 1 1 calc R . .
H17B H 0.3628 -0.4631 0.4904 0.146 Uiso 1 1 calc R . .
H17C H 0.4200 -0.3352 0.4897 0.146 Uiso 1 1 calc R . .
C18 C 0.5565(3) -0.3294(3) 0.6711(2) 0.0729(9) Uani 1 1 d . . .
H18A H 0.5764 -0.2954 0.7308 0.109 Uiso 1 1 calc R . .
H18B H 0.6171 -0.2872 0.6532 0.109 Uiso 1 1 calc R . .
H18C H 0.5610 -0.4151 0.6544 0.109 Uiso 1 1 calc R . .
C21 C 0.6711(2) 0.1631(2) 0.85280(14) 0.0406(5) Uani 1 1 d . . .
C22 C 0.7470(2) 0.2332(2) 0.94199(15) 0.0472(6) Uani 1 1 d . . .
C23 C 0.7153(3) 0.2051(3) 1.00574(16) 0.0650(8) Uani 1 1 d . . .
H23A H 0.6496 0.1393 0.9932 0.078 Uiso 1 1 calc R . .
C24 C 0.7802(3) 0.2739(3) 1.08863(19) 0.0846(10) Uani 1 1 d . . .
H24A H 0.7571 0.2546 1.1311 0.102 Uiso 1 1 calc R . .
C25 C 0.8774(3) 0.3694(3) 1.1080(2) 0.0920(11) Uani 1 1 d . . .
H25A H 0.9203 0.4160 1.1635 0.110 Uiso 1 1 calc R . .
C26 C 0.9111(3) 0.3961(3) 1.0457(2) 0.0957(13) Uani 1 1 d . . .
H26A H 0.9785 0.4605 1.0587 0.115 Uiso 1 1 calc R . .
C27 C 0.8468(3) 0.3291(3) 0.96333(19) 0.0703(9) Uani 1 1 d . . .
H27A H 0.8713 0.3490 0.9215 0.084 Uiso 1 1 calc R . .
C28 C 0.7194(2) -0.0327(2) 0.86059(14) 0.0459(6) Uani 1 1 d . . .
C29 C 0.8508(3) -0.0292(2) 0.86962(16) 0.0565(7) Uani 1 1 d . . .
C30 C 0.9107(3) -0.1075(3) 0.9049(2) 0.0840(10) Uani 1 1 d . . .
H30A H 0.9984 -0.1037 0.9131 0.101 Uiso 1 1 calc R . .
C31 C 0.8466(5) -0.1888(3) 0.9276(2) 0.1017(14) Uani 1 1 d . . .
H31A H 0.8897 -0.2412 0.9499 0.122 Uiso 1 1 calc R . .
C32 C 0.7180(4) -0.1947(3) 0.91791(19) 0.0855(11) Uani 1 1 d . . .
H32A H 0.6741 -0.2511 0.9338 0.103 Uiso 1 1 calc R . .
C33 C 0.6520(3) -0.1166(2) 0.88422(16) 0.0609(7) Uani 1 1 d . . .
C34 C 0.5115(3) -0.1232(3) 0.8746(2) 0.0846(10) Uani 1 1 d . . .
H34A H 0.4812 -0.0641 0.8507 0.127 Uiso 1 1 calc R . .
H34B H 0.4974 -0.1058 0.9284 0.127 Uiso 1 1 calc R . .
H34C H 0.4659 -0.2041 0.8386 0.127 Uiso 1 1 calc R . .
C35 C 0.9263(3) 0.0554(3) 0.8416(2) 0.0742(9) Uani 1 1 d . . .
H35A H 0.8711 0.1028 0.8185 0.111 Uiso 1 1 calc R . .
H35B H 0.9613 0.0079 0.7998 0.111 Uiso 1 1 calc R . .
H35C H 0.9949 0.1096 0.8884 0.111 Uiso 1 1 calc R . .
C36 C 0.5687(5) 0.4549(3) 0.9107(3) 0.1178(15) Uani 1 1 d . . .
H36A H 0.4963 0.4114 0.9181 0.177 Uiso 1 1 calc R . .
H36B H 0.5519 0.5333 0.9088 0.177 Uiso 1 1 calc R . .
H36C H 0.6433 0.4666 0.9565 0.177 Uiso 1 1 calc R . .
C37 C 0.4572(3) 0.3537(3) 0.7223(3) 0.0989(13) Uani 1 1 d . . .
H37A H 0.3817 0.3101 0.7263 0.148 Uiso 1 1 calc R . .
H37B H 0.4728 0.3108 0.6705 0.148 Uiso 1 1 calc R . .
H37C H 0.4450 0.4349 0.7244 0.148 Uiso 1 1 calc R . .
C38 C 0.7391(3) 0.4499(3) 0.7969(2) 0.0800(10) Uani 1 1 d . . .
H38A H 0.8139 0.4600 0.8422 0.120 Uiso 1 1 calc R . .
H38B H 0.7232 0.5291 0.7963 0.120 Uiso 1 1 calc R . .
H38C H 0.7529 0.4044 0.7450 0.120 Uiso 1 1 calc R . .
C41 C 0.6912(3) 0.1355(3) 0.63364(17) 0.0708(9) Uani 1 1 d . . .
H41A H 0.7235 0.1288 0.5868 0.106 Uiso 1 1 calc R . .
H41B H 0.7607 0.1441 0.6817 0.106 Uiso 1 1 calc R . .
H41C H 0.6511 0.2061 0.6451 0.106 Uiso 1 1 calc R . .
C42 C 0.6596(3) -0.0829(3) 0.60023(17) 0.0676(8) Uani 1 1 d . . .
H42A H 0.6964 -0.0897 0.5553 0.101 Uiso 1 1 calc R . .
H42B H 0.5976 -0.1558 0.5861 0.101 Uiso 1 1 calc R . .
H42C H 0.7259 -0.0730 0.6502 0.101 Uiso 1 1 calc R . .
C43 C 0.4851(2) 0.0092(2) 0.54135(13) 0.0474(6) Uani 1 1 d . . .
H43A H 0.4459 0.0812 0.5545 0.057 Uiso 1 1 calc R . .
H43B H 0.4222 -0.0609 0.5338 0.057 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N3 Co1 N1 125.32(8) . . ?
N3 Co1 N5 113.26(7) . . ?
N1 Co1 N5 121.41(7) . . ?
N3 Co1 N4 63.66(7) . . ?
N1 Co1 N4 105.29(7) . . ?
N5 Co1 N4 98.96(7) . . ?
N3 Co1 N2 112.63(7) . . ?
N1 Co1 N2 62.96(7) . . ?
N5 Co1 N2 96.92(7) . . ?
N4 Co1 N2 163.76(7) . . ?
N3 Co1 C21 32.02(7) . . ?
N1 Co1 C21 117.52(7) . . ?
N5 Co1 C21 111.09(7) . . ?
N4 Co1 C21 31.79(7) . . ?
N2 Co1 C21 141.35(7) . . ?
N2 Si1 C18 107.78(12) . . ?
N2 Si1 C17 110.48(13) . . ?
C18 Si1 C17 107.75(16) . . ?
N2 Si1 C16 115.26(14) . . ?
C18 Si1 C16 107.14(15) . . ?
C17 Si1 C16 108.14(18) . . ?
N4 Si2 C37 106.19(12) . . ?
N4 Si2 C36 114.24(14) . . ?
C37 Si2 C36 108.9(2) . . ?
N4 Si2 C38 111.81(13) . . ?
C37 Si2 C38 106.10(16) . . ?
C36 Si2 C38 109.21(18) . . ?
C1 N1 C8 123.91(19) . . ?
C1 N1 Co1 95.48(14) . . ?
C8 N1 Co1 140.60(15) . . ?
C1 N2 Si1 130.33(17) . . ?
C1 N2 Co1 86.12(13) . . ?
Si1 N2 Co1 141.94(11) . . ?
C21 N3 C28 123.86(18) . . ?
C21 N3 Co1 94.42(14) . . ?
C28 N3 Co1 141.64(15) . . ?
C21 N4 Si2 134.43(17) . . ?
C21 N4 Co1 86.76(13) . . ?
Si2 N4 Co1 137.71(11) . . ?
C42 N5 C41 109.2(2) . . ?
C42 N5 C43 111.9(2) . . ?
C41 N5 C43 111.31(19) . . ?
C42 N5 Co1 105.86(15) . . ?
C41 N5 Co1 112.64(16) . . ?
C43 N5 Co1 105.81(14) . . ?
N2 C1 N1 115.4(2) . . ?
N2 C1 C2 122.5(2) . . ?
N1 C1 C2 122.2(2) . . ?
C3 C2 C7 118.8(2) . . ?
C3 C2 C1 121.0(2) . . ?
C7 C2 C1 120.1(2) . . ?
C2 C3 C4 120.7(3) . . ?
C5 C4 C3 119.6(4) . . ?
C6 C5 C4 120.7(3) . . ?
C5 C6 C7 119.9(3) . . ?
C2 C7 C6 120.2(3) . . ?
C9 C8 C13 120.5(3) . . ?
C9 C8 N1 118.9(2) . . ?
C13 C8 N1 120.3(2) . . ?
C10 C9 C8 118.4(3) . . ?
C10 C9 C15 120.6(3) . . ?
C8 C9 C15 121.0(3) . . ?
C11 C10 C9 121.7(4) . . ?
C10 C11 C12 119.5(3) . . ?
C11 C12 C13 121.3(4) . . ?
C12 C13 C8 118.5(3) . . ?
C12 C13 C14 120.2(3) . . ?
C8 C13 C14 121.2(2) . . ?
N4 C21 N3 114.6(2) . . ?
N4 C21 C22 123.3(2) . . ?
N3 C21 C22 121.9(2) . . ?
N4 C21 Co1 61.45(12) . . ?
N3 C21 Co1 53.55(11) . . ?
C22 C21 Co1 169.44(16) . . ?
C27 C22 C23 117.7(2) . . ?
C27 C22 C21 122.0(2) . . ?
C23 C22 C21 120.3(2) . . ?
C22 C23 C24 120.7(3) . . ?
C25 C24 C23 120.4(3) . . ?
C26 C25 C24 119.4(3) . . ?
C25 C26 C27 120.8(3) . . ?
C22 C27 C26 121.0(3) . . ?
C33 C28 C29 119.9(2) . . ?
C33 C28 N3 119.0(2) . . ?
C29 C28 N3 120.9(2) . . ?
C30 C29 C28 118.2(3) . . ?
C30 C29 C35 119.9(3) . . ?
C28 C29 C35 121.9(2) . . ?
C31 C30 C29 122.3(4) . . ?
C30 C31 C32 120.1(3) . . ?
C31 C32 C33 120.5(3) . . ?
C28 C33 C32 118.9(3) . . ?
C28 C33 C34 121.1(3) . . ?
C32 C33 C34 120.0(3) . . ?
N5 C43 C43 115.8(2) . 2_656 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 N3 2.0157(18) . ?
Co1 N1 2.0294(19) . ?
Co1 N5 2.159(2) . ?
Co1 N4 2.1980(19) . ?
Co1 N2 2.2456(19) . ?
Co1 C21 2.498(2) . ?
Si1 N2 1.725(2) . ?
Si1 C18 1.867(3) . ?
Si1 C17 1.867(3) . ?
Si1 C16 1.869(4) . ?
Si2 N4 1.722(2) . ?
Si2 C37 1.858(3) . ?
Si2 C36 1.865(4) . ?
Si2 C38 1.881(3) . ?
N1 C1 1.327(3) . ?
N1 C8 1.424(3) . ?
N2 C1 1.324(3) . ?
N3 C21 1.329(3) . ?
N3 C28 1.428(3) . ?
N4 C21 1.318(3) . ?
N5 C42 1.470(3) . ?
N5 C41 1.473(3) . ?
N5 C43 1.484(3) . ?
C1 C2 1.504(3) . ?
C2 C3 1.372(4) . ?
C2 C7 1.386(4) . ?
C3 C4 1.386(4) . ?
C4 C5 1.371(5) . ?
C5 C6 1.355(6) . ?
C6 C7 1.390(4) . ?
C8 C9 1.398(4) . ?
C8 C13 1.402(4) . ?
C9 C10 1.389(4) . ?
C9 C15 1.498(4) . ?
C10 C11 1.365(5) . ?
C11 C12 1.378(5) . ?
C12 C13 1.386(4) . ?
C13 C14 1.484(4) . ?
C21 C22 1.500(3) . ?
C22 C27 1.374(3) . ?
C22 C23 1.377(4) . ?
C23 C24 1.388(4) . ?
C24 C25 1.359(5) . ?
C25 C26 1.354(5) . ?
C26 C27 1.376(4) . ?
C28 C33 1.396(4) . ?
C28 C29 1.403(4) . ?
C29 C30 1.387(4) . ?
C29 C35 1.503(4) . ?
C30 C31 1.343(5) . ?
C31 C32 1.369(6) . ?
C32 C33 1.400(4) . ?
C33 C34 1.497(4) . ?
C43 C43 1.528(4) 2_656 ?
