#------------------------------------------------------------------------------
#$Date: 2019-03-05 09:52:05 +0100 (mar 05 de mar de 2019) $
#$Revision: 213973 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/09/7050911.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7050911
loop_
_publ_author_name
'Durran, Sean E.'
'Elsegood, Mark R. J.'
'Smith, Martin B.'
_publ_section_title
;
 New complexes of functionalised ligands bearing P/N/Se or P2Se donor
 sets
;
_journal_issue                   10
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              1402
_journal_paper_doi               10.1039/b204005k
_journal_volume                  26
_journal_year                    2002
_chemical_formula_sum            'C36 H37 Cl2 N P2 Pt Se'
_chemical_formula_weight         890.56
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                100.185(2)
_cell_angle_beta                 90.251(2)
_cell_angle_gamma                99.638(2)
_cell_formula_units_Z            4
_cell_length_a                   11.2388(7)
_cell_length_b                   14.3914(8)
_cell_length_c                   21.7918(13)
_cell_measurement_reflns_used    14801
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      28.77
_cell_measurement_theta_min      2.26
_cell_volume                     3418.0(4)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL and local programs'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker SMART 1000 CCD diffractometer'
_diffrn_measurement_method       'ω rotation with narrow frames'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0234
_diffrn_reflns_av_sigmaI/netI    0.0359
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            24506
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.84
_diffrn_standards_decay_%        0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    5.447
_exptl_absorpt_correction_T_max  0.736
_exptl_absorpt_correction_T_min  0.283
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.731
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1744
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.06
_refine_diff_density_max         2.665
_refine_diff_density_min         -0.972
_refine_diff_density_rms         0.129
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.045
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     785
_refine_ls_number_reflns         11930
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.045
_refine_ls_R_factor_all          0.0417
_refine_ls_R_factor_gt           0.0326
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0273P)²+18.2824P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0751
_refine_ls_wR_factor_ref         0.0792
_reflns_number_gt                10135
_reflns_number_total             11930
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            b204005k.txt
_cod_data_source_block           3b
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7050911
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.750388(19) 0.366785(15) 0.221569(9) 0.01785(6) Uani 1 1 d . A .
Cl1 Cl 0.62057(13) 0.28738(12) 0.28715(7) 0.0316(3) Uani 1 1 d . . .
Cl2 Cl 0.58130(13) 0.40304(10) 0.17111(7) 0.0260(3) Uani 1 1 d . . .
P1 P 0.89794(13) 0.31342(10) 0.26614(6) 0.0180(3) Uani 1 1 d . . .
P2 P 0.87055(13) 0.43843(10) 0.15618(6) 0.0189(3) Uani 1 1 d . . .
N1 N 1.0718(4) 0.3778(3) 0.1925(2) 0.0213(10) Uani 1 1 d . . .
C1 C 1.0523(5) 0.3747(4) 0.2572(3) 0.0241(12) Uani 1 1 d . A 1
H1A H 1.0641 0.4407 0.2816 0.029 Uiso 1 1 calc R A 1
H1B H 1.1112 0.3401 0.2733 0.029 Uiso 1 1 calc R A 1
C2 C 1.0328(5) 0.4626(4) 0.1750(3) 0.0234(12) Uani 1 1 d . A 1
H2A H 1.0775 0.4798 0.1384 0.028 Uiso 1 1 calc R A 1
H2B H 1.0515 0.5175 0.2100 0.028 Uiso 1 1 calc R A 1
C3 C 1.1932(6) 0.3661(5) 0.1713(3) 0.0332(15) Uani 1 1 d . A 1
H3A H 1.2290 0.3282 0.1979 0.040 Uiso 1 1 calc R A 1
H3B H 1.2451 0.4299 0.1760 0.040 Uiso 1 1 calc R A 1
C4 C 1.1907(7) 0.3158(6) 0.1031(3) 0.0453(19) Uani 1 1 d . . .
H4A H 1.2739 0.3088 0.0909 0.054 Uiso 1 1 calc R A 1
H4B H 1.1599 0.3557 0.0761 0.054 Uiso 1 1 calc R A 1
C5 C 1.1103(8) 0.2164(5) 0.0930(3) 0.0484(19) Uani 1 1 d . A .
H5A H 1.1381 0.1796 0.1230 0.058 Uiso 1 1 calc R . .
H5B H 1.0268 0.2252 0.1035 0.058 Uiso 1 1 calc R . .
C6 C 1.1066(8) 0.1558(7) 0.0277(4) 0.059(2) Uani 1 1 d U . .
H6A H 1.0760 0.1908 -0.0026 0.071 Uiso 0.820(4) 1 calc PR A 1
H6B H 1.0491 0.0954 0.0266 0.071 Uiso 0.820(4) 1 calc PR A 1
H6C H 1.1366 0.2005 -0.0007 0.071 Uiso 0.180(4) 1 d PR A 2
H6D H 1.0208 0.1304 0.0154 0.071 Uiso 0.180(4) 1 d PR A 2
Se1 Se 1.26338(12) 0.12525(9) 0.00175(4) 0.0486(4) Uani 0.820(4) 1 d PU A 1
Se1X Se 1.1793(8) 0.0665(5) 0.0124(3) 0.081(3) Uani 0.180(4) 1 d PU A 2
C7 C 1.3135(7) 0.0842(6) 0.0763(3) 0.0468(18) Uani 1 1 d U . .
C8 C 1.4118(9) 0.1420(7) 0.1105(5) 0.071(3) Uani 1 1 d . A .
H8 H 1.4503 0.1991 0.0978 0.085 Uiso 1 1 calc R . .
C9 C 1.4517(11) 0.1147(10) 0.1630(6) 0.098(4) Uani 1 1 d . . .
H9 H 1.5187 0.1530 0.1871 0.117 Uiso 1 1 calc R A .
C10 C 1.3943(11) 0.0313(8) 0.1807(5) 0.082(3) Uani 1 1 d . A .
H10 H 1.4233 0.0120 0.2167 0.098 Uiso 1 1 calc R . .
C11 C 1.2981(11) -0.0226(7) 0.1479(5) 0.076(3) Uani 1 1 d . . .
H11 H 1.2592 -0.0796 0.1606 0.091 Uiso 1 1 calc R A .
C12 C 1.2557(8) 0.0048(6) 0.0955(4) 0.054(2) Uani 1 1 d . A .
H12 H 1.1860 -0.0321 0.0729 0.065 Uiso 1 1 calc R B 2
C13 C 0.9041(5) 0.1896(4) 0.2315(2) 0.0201(12) Uani 1 1 d . A .
C14 C 0.8173(6) 0.1385(4) 0.1873(3) 0.0326(15) Uani 1 1 d . . .
H14 H 0.7481 0.1650 0.1792 0.039 Uiso 1 1 calc R A .
C15 C 0.8307(7) 0.0489(5) 0.1550(3) 0.0412(17) Uani 1 1 d . A .
H15 H 0.7706 0.0142 0.1249 0.049 Uiso 1 1 calc R . .
C16 C 0.9311(7) 0.0100(5) 0.1663(3) 0.0438(18) Uani 1 1 d . . .
H16 H 0.9423 -0.0497 0.1425 0.053 Uiso 1 1 calc R A .
C17 C 1.0147(6) 0.0577(5) 0.2120(3) 0.0367(16) Uani 1 1 d . A .
H17 H 1.0813 0.0292 0.2214 0.044 Uiso 1 1 calc R . .
C18 C 1.0025(6) 0.1475(4) 0.2444(3) 0.0286(13) Uani 1 1 d . . .
H18 H 1.0614 0.1805 0.2756 0.034 Uiso 1 1 calc R A .
C19 C 0.8885(5) 0.3216(4) 0.3500(2) 0.0205(12) Uani 1 1 d . A .
C20 C 0.8958(5) 0.4129(4) 0.3866(3) 0.0265(13) Uani 1 1 d . . .
H20 H 0.9057 0.4679 0.3674 0.032 Uiso 1 1 calc R A .
C21 C 0.8887(5) 0.4228(5) 0.4505(3) 0.0295(14) Uani 1 1 d . A .
H21 H 0.8912 0.4846 0.4750 0.035 Uiso 1 1 calc R . .
C22 C 0.8777(5) 0.3431(5) 0.4792(3) 0.0319(15) Uani 1 1 d . . .
H22 H 0.8762 0.3506 0.5234 0.038 Uiso 1 1 calc R A .
C23 C 0.8690(5) 0.2532(5) 0.4432(3) 0.0273(13) Uani 1 1 d . A .
H23 H 0.8596 0.1984 0.4627 0.033 Uiso 1 1 calc R . .
C24 C 0.8739(5) 0.2420(4) 0.3788(3) 0.0233(12) Uani 1 1 d . . .
H24 H 0.8673 0.1797 0.3543 0.028 Uiso 1 1 calc R A .
C25 C 0.8584(5) 0.3654(4) 0.0786(2) 0.0232(12) Uani 1 1 d . A .
C26 C 0.7862(5) 0.2766(4) 0.0660(3) 0.0264(13) Uani 1 1 d . . .
H26 H 0.7387 0.2541 0.0980 0.032 Uiso 1 1 calc R A .
C27 C 0.7813(6) 0.2190(5) 0.0072(3) 0.0373(16) Uani 1 1 d . A .
H27 H 0.7325 0.1572 -0.0006 0.045 Uiso 1 1 calc R . .
C28 C 0.8487(6) 0.2531(5) -0.0401(3) 0.0389(16) Uani 1 1 d . . .
H28 H 0.8443 0.2150 -0.0807 0.047 Uiso 1 1 calc R A .
C29 C 0.9216(7) 0.3416(5) -0.0285(3) 0.0434(18) Uani 1 1 d . A .
H29 H 0.9676 0.3643 -0.0609 0.052 Uiso 1 1 calc R . .
C30 C 0.9280(7) 0.3979(5) 0.0308(3) 0.0381(17) Uani 1 1 d . . .
H30 H 0.9797 0.4584 0.0390 0.046 Uiso 1 1 calc R A .
C31 C 0.8438(5) 0.5558(4) 0.1448(3) 0.0216(12) Uani 1 1 d . A .
C32 C 0.9040(5) 0.6385(4) 0.1832(2) 0.0211(12) Uani 1 1 d . . .
H32 H 0.9562 0.6336 0.2164 0.025 Uiso 1 1 calc R A .
C33 C 0.8871(5) 0.7285(4) 0.1726(3) 0.0265(13) Uani 1 1 d . A .
H33 H 0.9287 0.7849 0.1984 0.032 Uiso 1 1 calc R . .
C34 C 0.8102(5) 0.7357(4) 0.1248(3) 0.0296(14) Uani 1 1 d . . .
H34 H 0.7993 0.7970 0.1176 0.036 Uiso 1 1 calc R A .
C35 C 0.7491(6) 0.6537(4) 0.0871(3) 0.0313(14) Uani 1 1 d . A .
H35 H 0.6950 0.6588 0.0547 0.038 Uiso 1 1 calc R . .
C36 C 0.7666(5) 0.5650(4) 0.0967(3) 0.0260(13) Uani 1 1 d . . .
H36 H 0.7255 0.5091 0.0702 0.031 Uiso 1 1 calc R A .
Pt2 Pt 0.309790(18) 0.654927(15) 0.288078(9) 0.01669(6) Uani 1 1 d . C .
Cl3 Cl 0.20925(12) 0.73001(11) 0.22048(6) 0.0257(3) Uani 1 1 d . . .
Cl4 Cl 0.12657(12) 0.61939(10) 0.33937(6) 0.0231(3) Uani 1 1 d . . .
P3 P 0.48015(13) 0.70947(10) 0.24452(6) 0.0182(3) Uani 1 1 d . . .
P4 P 0.39949(12) 0.58159(10) 0.35259(6) 0.0166(3) Uani 1 1 d . . .
N2 N 0.6303(4) 0.6519(3) 0.3231(2) 0.0205(10) Uani 1 1 d . . .
C37 C 0.6129(5) 0.6565(4) 0.2577(3) 0.0206(12) Uani 1 1 d . C 1
H37A H 0.6033 0.5911 0.2327 0.025 Uiso 1 1 calc R C 1
H37B H 0.6854 0.6952 0.2436 0.025 Uiso 1 1 calc R C 1
C38 C 0.5560(5) 0.5652(4) 0.3377(2) 0.0188(11) Uani 1 1 d . C 1
H38A H 0.5915 0.5480 0.3749 0.023 Uiso 1 1 calc R C 1
H38B H 0.5565 0.5116 0.3024 0.023 Uiso 1 1 calc R C 1
C39 C 0.7599(5) 0.6558(4) 0.3399(3) 0.0221(12) Uani 1 1 d . C 1
H39A H 0.8092 0.7069 0.3215 0.026 Uiso 1 1 calc R C 1
H39B H 0.7841 0.5942 0.3212 0.026 Uiso 1 1 calc R C 1
C40 C 0.7878(6) 0.6746(5) 0.4099(3) 0.0315(14) Uani 1 1 d . . .
H40A H 0.8765 0.6843 0.4170 0.038 Uiso 1 1 calc R C 1
H40B H 0.7523 0.6171 0.4268 0.038 Uiso 1 1 calc R C 1
C41 C 0.7405(6) 0.7616(4) 0.4461(3) 0.0302(14) Uani 1 1 d . C .
H41A H 0.6515 0.7512 0.4404 0.036 Uiso 1 1 calc R . .
H41B H 0.7600 0.7674 0.4911 0.036 Uiso 1 1 calc R . .
C42 C 0.7941(7) 0.8544(5) 0.4250(3) 0.0379(16) Uani 1 1 d . . .
H42A H 0.7768 0.8471 0.3796 0.045 Uiso 1 1 calc R C .
H42B H 0.8829 0.8648 0.4315 0.045 Uiso 1 1 calc R . .
Se2 Se 0.73465(7) 0.96790(5) 0.46744(4) 0.04382(18) Uani 1 1 d . C .
C43 C 0.8308(5) 1.0012(4) 0.5431(3) 0.0289(14) Uani 1 1 d . . .
C44 C 0.8181(7) 1.0863(5) 0.5814(3) 0.0438(18) Uani 1 1 d . C .
H44 H 0.7656 1.1252 0.5686 0.053 Uiso 1 1 calc R . .
C45 C 0.8813(7) 1.1155(5) 0.6383(3) 0.0474(19) Uani 1 1 d . . .
H45 H 0.8716 1.1740 0.6642 0.057 Uiso 1 1 calc R C .
C46 C 0.9574(7) 1.0603(5) 0.6570(3) 0.0428(17) Uani 1 1 d . C .
H46 H 0.9990 1.0790 0.6964 0.051 Uiso 1 1 calc R . .
C47 C 0.9733(7) 0.9766(5) 0.6178(3) 0.0440(18) Uani 1 1 d . . .
H47 H 1.0281 0.9392 0.6302 0.053 Uiso 1 1 calc R C .
C48 C 0.9111(6) 0.9464(4) 0.5610(3) 0.0322(14) Uani 1 1 d . C .
H48 H 0.9230 0.8890 0.5345 0.039 Uiso 1 1 calc R . .
C49 C 0.4680(5) 0.6918(4) 0.1599(3) 0.0231(12) Uani 1 1 d . C .
C50 C 0.4825(6) 0.7663(5) 0.1268(3) 0.0309(14) Uani 1 1 d . . .
H50 H 0.5012 0.8308 0.1481 0.037 Uiso 1 1 calc R C .
C51 C 0.4696(6) 0.7461(5) 0.0619(3) 0.0378(16) Uani 1 1 d . C .
H51 H 0.4805 0.7972 0.0391 0.045 Uiso 1 1 calc R . .
C52 C 0.4411(6) 0.6528(5) 0.0304(3) 0.0384(16) Uani 1 1 d . . .
H52 H 0.4319 0.6400 -0.0138 0.046 Uiso 1 1 calc R C .
C53 C 0.4262(6) 0.5782(5) 0.0633(3) 0.0335(15) Uani 1 1 d . C .
H53 H 0.4075 0.5139 0.0417 0.040 Uiso 1 1 calc R . .
C54 C 0.4386(5) 0.5973(5) 0.1280(3) 0.0281(13) Uani 1 1 d . . .
H54 H 0.4272 0.5460 0.1506 0.034 Uiso 1 1 calc R C .
C55 C 0.5293(5) 0.8367(4) 0.2745(2) 0.0206(12) Uani 1 1 d . C .
C56 C 0.6444(6) 0.8834(4) 0.2626(3) 0.0291(14) Uani 1 1 d . . .
H56 H 0.6963 0.8492 0.2367 0.035 Uiso 1 1 calc R C .
C57 C 0.6829(6) 0.9783(4) 0.2882(3) 0.0322(15) Uani 1 1 d . C .
H57 H 0.7613 1.0091 0.2800 0.039 Uiso 1 1 calc R . .
C58 C 0.6080(6) 1.0293(4) 0.3258(3) 0.0337(15) Uani 1 1 d . . .
H58 H 0.6347 1.0950 0.3429 0.040 Uiso 1 1 calc R C .
C59 C 0.4953(6) 0.9850(4) 0.3382(3) 0.0314(14) Uani 1 1 d . C .
H59 H 0.4445 1.0196 0.3647 0.038 Uiso 1 1 calc R . .
C60 C 0.4552(6) 0.8890(4) 0.3120(3) 0.0278(13) Uani 1 1 d . . .
H60 H 0.3763 0.8590 0.3200 0.033 Uiso 1 1 calc R C .
C61 C 0.4125(5) 0.6481(4) 0.4322(2) 0.0208(12) Uani 1 1 d . C .
C62 C 0.4404(6) 0.6042(4) 0.4816(3) 0.0278(13) Uani 1 1 d . . .
H62 H 0.4451 0.5379 0.4740 0.033 Uiso 1 1 calc R C .
C63 C 0.4610(6) 0.6564(5) 0.5411(3) 0.0333(15) Uani 1 1 d . C .
H63 H 0.4781 0.6257 0.5745 0.040 Uiso 1 1 calc R . .
C64 C 0.4569(6) 0.7531(5) 0.5524(3) 0.0299(14) Uani 1 1 d . . .
H64 H 0.4726 0.7891 0.5934 0.036 Uiso 1 1 calc R C .
C65 C 0.4302(6) 0.7978(4) 0.5045(3) 0.0293(14) Uani 1 1 d . C .
H65 H 0.4278 0.8645 0.5125 0.035 Uiso 1 1 calc R . .
C66 C 0.4066(5) 0.7451(4) 0.4442(3) 0.0230(12) Uani 1 1 d . . .
H66 H 0.3865 0.7758 0.4114 0.028 Uiso 1 1 calc R C .
C67 C 0.3279(5) 0.4595(4) 0.3571(2) 0.0196(12) Uani 1 1 d . C .
C68 C 0.3610(5) 0.3811(4) 0.3176(3) 0.0207(12) Uani 1 1 d . . .
H68 H 0.4159 0.3912 0.2855 0.025 Uiso 1 1 calc R C .
C69 C 0.3138(5) 0.2886(4) 0.3251(3) 0.0255(13) Uani 1 1 d . C .
H69 H 0.3384 0.2356 0.2989 0.031 Uiso 1 1 calc R . .
C70 C 0.2309(5) 0.2732(4) 0.3707(3) 0.0266(13) Uani 1 1 d . . .
H70 H 0.2002 0.2097 0.3762 0.032 Uiso 1 1 calc R C .
C71 C 0.1928(5) 0.3500(4) 0.4083(3) 0.0273(13) Uani 1 1 d . C .
H71 H 0.1339 0.3390 0.4386 0.033 Uiso 1 1 calc R . .
C72 C 0.2406(5) 0.4428(4) 0.4018(3) 0.0228(12) Uani 1 1 d . . .
H72 H 0.2143 0.4954 0.4276 0.027 Uiso 1 1 calc R C .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Pt1 P2 94.79(5) . . ?
P1 Pt1 Cl1 86.03(5) . . ?
P2 Pt1 Cl1 177.88(5) . . ?
P1 Pt1 Cl2 172.75(5) . . ?
P2 Pt1 Cl2 89.19(5) . . ?
Cl1 Pt1 Cl2 89.80(5) . . ?
C19 P1 C13 108.3(3) . . ?
C19 P1 C1 103.0(3) . . ?
C13 P1 C1 102.7(3) . . ?
C19 P1 Pt1 114.54(18) . . ?
C13 P1 Pt1 111.14(19) . . ?
C1 P1 Pt1 116.2(2) . . ?
C25 P2 C31 105.3(3) . . ?
C25 P2 C2 103.7(3) . . ?
C31 P2 C2 101.5(3) . . ?
C25 P2 Pt1 111.0(2) . . ?
C31 P2 Pt1 116.70(18) . . ?
C2 P2 Pt1 117.18(18) . . ?
C1 N1 C3 115.6(5) . . ?
C1 N1 C2 111.0(4) . . ?
C3 N1 C2 112.5(4) . . ?
N1 C1 P1 109.5(4) . . ?
N1 C2 P2 110.4(4) . . ?
N1 C3 C4 111.9(5) . . ?
C3 C4 C5 111.5(6) . . ?
C6 C5 C4 116.7(7) . . ?
C5 C6 Se1X 121.6(6) . . ?
C5 C6 Se1 113.3(6) . . ?
Se1X C6 Se1 38.3(4) . . ?
C7 Se1 C6 99.3(3) . . ?
C6 Se1X C7 109.1(5) . . ?
C6 Se1X C12 119.7(5) . . ?
C7 Se1X C12 34.8(3) . . ?
C12 C7 C8 120.9(8) . . ?
C12 C7 Se1 122.6(6) . . ?
C8 C7 Se1 116.6(7) . . ?
C12 C7 Se1X 87.7(6) . . ?
C8 C7 Se1X 150.0(8) . . ?
Se1 C7 Se1X 35.8(3) . . ?
C9 C8 C7 118.5(10) . . ?
C8 C9 C10 119.9(10) . . ?
C11 C10 C9 120.9(10) . . ?
C10 C11 C12 119.9(10) . . ?
C7 C12 C11 119.9(9) . . ?
C7 C12 Se1X 57.6(5) . . ?
C11 C12 Se1X 174.1(6) . . ?
C14 C13 C18 118.7(5) . . ?
C14 C13 P1 120.5(5) . . ?
C18 C13 P1 120.5(4) . . ?
C13 C14 C15 120.3(6) . . ?
C16 C15 C14 120.3(6) . . ?
C17 C16 C15 119.9(6) . . ?
C16 C17 C18 120.3(7) . . ?
C17 C18 C13 120.3(6) . . ?
C24 C19 C20 119.3(5) . . ?
C24 C19 P1 123.0(4) . . ?
C20 C19 P1 117.7(4) . . ?
C21 C20 C19 119.9(6) . . ?
C20 C21 C22 120.6(6) . . ?
C23 C22 C21 119.5(5) . . ?
C22 C23 C24 120.5(6) . . ?
C19 C24 C23 120.1(5) . . ?
C26 C25 C30 118.8(5) . . ?
C26 C25 P2 121.5(4) . . ?
C30 C25 P2 119.7(5) . . ?
C25 C26 C27 121.3(6) . . ?
C28 C27 C26 119.2(6) . . ?
C29 C28 C27 120.4(6) . . ?
C28 C29 C30 120.1(6) . . ?
C29 C30 C25 120.2(6) . . ?
C32 C31 C36 118.9(5) . . ?
C32 C31 P2 120.0(4) . . ?
C36 C31 P2 121.1(4) . . ?
C31 C32 C33 119.8(5) . . ?
C34 C33 C32 120.2(6) . . ?
C33 C34 C35 120.2(6) . . ?
C36 C35 C34 120.0(6) . . ?
C35 C36 C31 121.0(6) . . ?
P3 Pt2 P4 94.70(5) . . ?
P3 Pt2 Cl3 86.96(5) . . ?
P4 Pt2 Cl3 178.29(5) . . ?
P3 Pt2 Cl4 172.08(5) . . ?
P4 Pt2 Cl4 88.91(5) . . ?
Cl3 Pt2 Cl4 89.50(5) . . ?
C49 P3 C55 108.4(3) . . ?
C49 P3 C37 102.5(3) . . ?
C55 P3 C37 103.5(3) . . ?
C49 P3 Pt2 113.54(19) . . ?
C55 P3 Pt2 110.65(19) . . ?
C37 P3 Pt2 117.32(18) . . ?
C61 P4 C67 106.2(3) . . ?
C61 P4 C38 102.0(2) . . ?
C67 P4 C38 101.1(2) . . ?
C61 P4 Pt2 111.96(19) . . ?
C67 P4 Pt2 116.15(18) . . ?
C38 P4 Pt2 117.71(18) . . ?
C37 N2 C38 109.9(4) . . ?
C37 N2 C39 111.6(4) . . ?
C38 N2 C39 111.0(4) . . ?
N2 C37 P3 111.6(4) . . ?
N2 C38 P4 112.0(4) . . ?
N2 C39 C40 113.9(5) . . ?
C39 C40 C41 114.3(5) . . ?
C42 C41 C40 112.6(5) . . ?
C41 C42 Se2 114.9(5) . . ?
C43 Se2 C42 102.3(3) . . ?
C44 C43 C48 119.4(6) . . ?
C44 C43 Se2 116.2(5) . . ?
C48 C43 Se2 124.3(5) . . ?
C43 C44 C45 120.7(7) . . ?
C46 C45 C44 120.1(7) . . ?
C45 C46 C47 119.3(7) . . ?
C48 C47 C46 121.3(7) . . ?
C47 C48 C43 119.1(6) . . ?
C50 C49 C54 119.6(5) . . ?
C50 C49 P3 123.4(5) . . ?
C54 C49 P3 116.9(4) . . ?
C49 C50 C51 119.5(6) . . ?
C52 C51 C50 120.9(6) . . ?
C51 C52 C53 119.8(6) . . ?
C52 C53 C54 119.9(6) . . ?
C53 C54 C49 120.2(6) . . ?
C60 C55 C56 118.3(5) . . ?
C60 C55 P3 120.5(4) . . ?
C56 C55 P3 121.1(4) . . ?
C57 C56 C55 120.6(6) . . ?
C56 C57 C58 120.4(6) . . ?
C59 C58 C57 120.0(6) . . ?
C58 C59 C60 119.9(6) . . ?
C55 C60 C59 120.8(6) . . ?
C66 C61 C62 118.8(5) . . ?
C66 C61 P4 120.6(4) . . ?
C62 C61 P4 120.3(4) . . ?
C63 C62 C61 120.5(6) . . ?
C62 C63 C64 120.1(6) . . ?
C65 C64 C63 120.3(6) . . ?
C64 C65 C66 120.0(6) . . ?
C61 C66 C65 120.1(5) . . ?
C68 C67 C72 118.9(5) . . ?
C68 C67 P4 120.8(4) . . ?
C72 C67 P4 120.3(4) . . ?
C69 C68 C67 120.2(5) . . ?
C68 C69 C70 120.3(5) . . ?
C71 C70 C69 120.3(5) . . ?
C70 C71 C72 119.9(5) . . ?
C71 C72 C67 120.3(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 P1 2.2269(14) . ?
Pt1 P2 2.2334(14) . ?
Pt1 Cl1 2.3482(14) . ?
Pt1 Cl2 2.3684(14) . ?
P1 C19 1.816(5) . ?
P1 C13 1.822(5) . ?
P1 C1 1.837(6) . ?
P2 C25 1.818(6) . ?
P2 C31 1.823(6) . ?
P2 C2 1.829(6) . ?
N1 C1 1.437(7) . ?
N1 C3 1.469(7) . ?
N1 C2 1.473(7) . ?
C3 C4 1.531(9) . ?
C4 C5 1.538(11) . ?
C5 C6 1.529(10) . ?
C6 Se1X 1.623(10) . ?
C6 Se1 1.949(8) . ?
Se1 C7 1.936(8) . ?
Se1X C7 2.000(9) . ?
Se1X C12 2.369(11) . ?
C7 C12 1.351(11) . ?
C7 C8 1.391(12) . ?
C8 C9 1.369(15) . ?
C9 C10 1.384(16) . ?
C10 C11 1.341(14) . ?
C11 C12 1.380(12) . ?
C13 C14 1.385(8) . ?
C13 C18 1.397(8) . ?
C14 C15 1.389(9) . ?
C15 C16 1.380(11) . ?
C16 C17 1.370(10) . ?
C17 C18 1.388(9) . ?
C19 C24 1.387(8) . ?
C19 C20 1.401(8) . ?
C20 C21 1.377(8) . ?
C21 C22 1.389(9) . ?
C22 C23 1.378(9) . ?
C23 C24 1.387(8) . ?
C25 C26 1.377(8) . ?
C25 C30 1.403(8) . ?
C26 C27 1.393(9) . ?
C27 C28 1.392(9) . ?
C28 C29 1.375(10) . ?
C29 C30 1.394(9) . ?
C31 C32 1.395(8) . ?
C31 C36 1.396(8) . ?
C32 C33 1.398(8) . ?
C33 C34 1.380(9) . ?
C34 C35 1.385(9) . ?
C35 C36 1.375(8) . ?
Pt2 P3 2.2269(14) . ?
Pt2 P4 2.2305(14) . ?
Pt2 Cl3 2.3604(13) . ?
Pt2 Cl4 2.3708(13) . ?
P3 C49 1.818(6) . ?
P3 C55 1.822(6) . ?
P3 C37 1.829(5) . ?
P4 C61 1.819(6) . ?
P4 C67 1.826(6) . ?
P4 C38 1.836(5) . ?
N2 C37 1.453(7) . ?
N2 C38 1.465(7) . ?
N2 C39 1.489(7) . ?
C39 C40 1.522(8) . ?
C40 C41 1.532(9) . ?
C41 C42 1.519(9) . ?
C42 Se2 1.951(7) . ?
Se2 C43 1.910(6) . ?
C43 C44 1.383(9) . ?
C43 C48 1.390(9) . ?
C44 C45 1.388(11) . ?
C45 C46 1.368(10) . ?
C46 C47 1.387(10) . ?
C47 C48 1.381(9) . ?
C49 C50 1.383(8) . ?
C49 C54 1.399(8) . ?
C50 C51 1.393(9) . ?
C51 C52 1.380(10) . ?
C52 C53 1.381(10) . ?
C53 C54 1.390(8) . ?
C55 C60 1.388(8) . ?
C55 C56 1.401(8) . ?
C56 C57 1.377(8) . ?
C57 C58 1.385(9) . ?
C58 C59 1.370(9) . ?
C59 C60 1.397(8) . ?
C61 C66 1.388(8) . ?
C61 C62 1.400(8) . ?
C62 C63 1.377(8) . ?
C63 C64 1.378(9) . ?
C64 C65 1.375(9) . ?
C65 C66 1.395(8) . ?
C67 C68 1.397(8) . ?
C67 C72 1.408(7) . ?
C68 C69 1.386(8) . ?
C69 C70 1.387(8) . ?
C70 C71 1.385(9) . ?
C71 C72 1.386(8) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P2 Pt1 P1 C19 139.9(2) . . . . ?
Cl1 Pt1 P1 C19 -42.1(2) . . . . ?
Cl2 Pt1 P1 C19 -97.1(4) . . . . ?
P2 Pt1 P1 C13 -96.98(19) . . . . ?
Cl1 Pt1 P1 C13 81.06(19) . . . . ?
Cl2 Pt1 P1 C13 26.1(5) . . . . ?
P2 Pt1 P1 C1 19.9(2) . . . . ?
Cl1 Pt1 P1 C1 -162.1(2) . . . . ?
Cl2 Pt1 P1 C1 143.0(4) . . . . ?
P1 Pt1 P2 C25 100.8(2) . . . . ?
Cl1 Pt1 P2 C25 -11.8(15) . . . . ?
Cl2 Pt1 P2 C25 -73.2(2) . . . . ?
P1 Pt1 P2 C31 -138.6(2) . . . . ?
Cl1 Pt1 P2 C31 108.8(15) . . . . ?
Cl2 Pt1 P2 C31 47.4(2) . . . . ?
P1 Pt1 P2 C2 -18.0(2) . . . . ?
Cl1 Pt1 P2 C2 -130.6(14) . . . . ?
Cl2 Pt1 P2 C2 168.0(2) . . . . ?
C3 N1 C1 P1 -143.2(4) . . . . ?
C2 N1 C1 P1 87.1(5) . . . . ?
C19 P1 C1 N1 -177.5(4) . . . . ?
C13 P1 C1 N1 70.0(4) . . . . ?
Pt1 P1 C1 N1 -51.5(4) . . . . ?
C1 N1 C2 P2 -84.1(5) . . . . ?
C3 N1 C2 P2 144.6(4) . . . . ?
C25 P2 C2 N1 -76.8(4) . . . . ?
C31 P2 C2 N1 174.2(4) . . . . ?
Pt1 P2 C2 N1 45.9(4) . . . . ?
C1 N1 C3 C4 148.1(5) . . . . ?
C2 N1 C3 C4 -82.9(6) . . . . ?
N1 C3 C4 C5 -58.4(7) . . . . ?
C3 C4 C5 C6 -176.1(6) . . . . ?
C4 C5 C6 Se1X 103.8(9) . . . . ?
C4 C5 C6 Se1 61.4(8) . . . . ?
C5 C6 Se1 C7 47.1(7) . . . . ?
Se1X C6 Se1 C7 -64.9(4) . . . . ?
C5 C6 Se1X C7 -22.2(11) . . . . ?
Se1 C6 Se1X C7 66.2(5) . . . . ?
C5 C6 Se1X C12 14.3(12) . . . . ?
Se1 C6 Se1X C12 102.7(6) . . . . ?
C6 Se1 C7 C12 65.7(7) . . . . ?
C6 Se1 C7 C8 -113.1(7) . . . . ?
C6 Se1 C7 Se1X 51.1(4) . . . . ?
C6 Se1X C7 C12 114.9(7) . . . . ?
C6 Se1X C7 C8 -48.2(16) . . . . ?
C12 Se1X C7 C8 -163.1(16) . . . . ?
C6 Se1X C7 Se1 -77.4(6) . . . . ?
C12 Se1X C7 Se1 167.7(6) . . . . ?
C12 C7 C8 C9 2.4(14) . . . . ?
Se1 C7 C8 C9 -178.8(8) . . . . ?
Se1X C7 C8 C9 162.6(11) . . . . ?
C7 C8 C9 C10 -0.1(17) . . . . ?
C8 C9 C10 C11 -1.3(18) . . . . ?
C9 C10 C11 C12 0.2(16) . . . . ?
C8 C7 C12 C11 -3.5(12) . . . . ?
Se1 C7 C12 C11 177.8(6) . . . . ?
Se1X C7 C12 C11 -173.7(7) . . . . ?
C8 C7 C12 Se1X 170.2(9) . . . . ?
Se1 C7 C12 Se1X -8.5(4) . . . . ?
C10 C11 C12 C7 2.1(14) . . . . ?
C10 C11 C12 Se1X -61(8) . . . . ?
C6 Se1X C12 C7 -80.7(8) . . . . ?
C6 Se1X C12 C11 -14(8) . . . . ?
C7 Se1X C12 C11 66(8) . . . . ?
C19 P1 C13 C14 121.3(5) . . . . ?
C1 P1 C13 C14 -130.3(5) . . . . ?
Pt1 P1 C13 C14 -5.4(5) . . . . ?
C19 P1 C13 C18 -64.9(5) . . . . ?
C1 P1 C13 C18 43.6(5) . . . . ?
Pt1 P1 C13 C18 168.5(4) . . . . ?
C18 C13 C14 C15 -2.5(9) . . . . ?
P1 C13 C14 C15 171.4(5) . . . . ?
C13 C14 C15 C16 -0.3(10) . . . . ?
C14 C15 C16 C17 3.4(11) . . . . ?
C15 C16 C17 C18 -3.7(10) . . . . ?
C16 C17 C18 C13 0.9(10) . . . . ?
C14 C13 C18 C17 2.3(9) . . . . ?
P1 C13 C18 C17 -171.7(5) . . . . ?
C13 P1 C19 C24 -7.0(6) . . . . ?
C1 P1 C19 C24 -115.3(5) . . . . ?
Pt1 P1 C19 C24 117.6(4) . . . . ?
C13 P1 C19 C20 173.3(4) . . . . ?
C1 P1 C19 C20 65.1(5) . . . . ?
Pt1 P1 C19 C20 -62.0(5) . . . . ?
C24 C19 C20 C21 0.1(9) . . . . ?
P1 C19 C20 C21 179.7(5) . . . . ?
C19 C20 C21 C22 1.9(9) . . . . ?
C20 C21 C22 C23 -2.6(9) . . . . ?
C21 C22 C23 C24 1.5(9) . . . . ?
C20 C19 C24 C23 -1.2(8) . . . . ?
P1 C19 C24 C23 179.1(4) . . . . ?
C22 C23 C24 C19 0.5(9) . . . . ?
C31 P2 C25 C26 -129.5(5) . . . . ?
C2 P2 C25 C26 124.3(5) . . . . ?
Pt1 P2 C25 C26 -2.3(6) . . . . ?
C31 P2 C25 C30 53.4(6) . . . . ?
C2 P2 C25 C30 -52.8(6) . . . . ?
Pt1 P2 C25 C30 -179.4(5) . . . . ?
C30 C25 C26 C27 0.1(9) . . . . ?
P2 C25 C26 C27 -177.1(5) . . . . ?
C25 C26 C27 C28 -1.5(10) . . . . ?
C26 C27 C28 C29 1.6(11) . . . . ?
C27 C28 C29 C30 -0.3(12) . . . . ?
C28 C29 C30 C25 -1.3(12) . . . . ?
C26 C25 C30 C29 1.3(10) . . . . ?
P2 C25 C30 C29 178.5(6) . . . . ?
C25 P2 C31 C32 -146.2(4) . . . . ?
C2 P2 C31 C32 -38.4(5) . . . . ?
Pt1 P2 C31 C32 90.2(4) . . . . ?
C25 P2 C31 C36 31.7(5) . . . . ?
C2 P2 C31 C36 139.5(5) . . . . ?
Pt1 P2 C31 C36 -91.9(5) . . . . ?
C36 C31 C32 C33 -0.7(8) . . . . ?
P2 C31 C32 C33 177.3(4) . . . . ?
C31 C32 C33 C34 0.7(8) . . . . ?
C32 C33 C34 C35 0.2(9) . . . . ?
C33 C34 C35 C36 -1.2(9) . . . . ?
C34 C35 C36 C31 1.2(9) . . . . ?
C32 C31 C36 C35 -0.3(9) . . . . ?
P2 C31 C36 C35 -178.2(5) . . . . ?
P4 Pt2 P3 C49 134.2(2) . . . . ?
Cl3 Pt2 P3 C49 -45.4(2) . . . . ?
Cl4 Pt2 P3 C49 -108.9(4) . . . . ?
P4 Pt2 P3 C55 -103.62(19) . . . . ?
Cl3 Pt2 P3 C55 76.79(19) . . . . ?
Cl4 Pt2 P3 C55 13.2(4) . . . . ?
P4 Pt2 P3 C37 14.8(2) . . . . ?
Cl3 Pt2 P3 C37 -164.8(2) . . . . ?
Cl4 Pt2 P3 C37 131.7(4) . . . . ?
P3 Pt2 P4 C61 104.1(2) . . . . ?
Cl3 Pt2 P4 C61 -89.7(18) . . . . ?
Cl4 Pt2 P4 C61 -68.9(2) . . . . ?
P3 Pt2 P4 C67 -133.6(2) . . . . ?
Cl3 Pt2 P4 C67 32.6(18) . . . . ?
Cl4 Pt2 P4 C67 53.4(2) . . . . ?
P3 Pt2 P4 C38 -13.6(2) . . . . ?
Cl3 Pt2 P4 C38 152.6(17) . . . . ?
Cl4 Pt2 P4 C38 173.5(2) . . . . ?
C38 N2 C37 P3 84.3(4) . . . . ?
C39 N2 C37 P3 -152.1(4) . . . . ?
C49 P3 C37 N2 -172.6(4) . . . . ?
C55 P3 C37 N2 74.6(4) . . . . ?
Pt2 P3 C37 N2 -47.6(4) . . . . ?
C37 N2 C38 P4 -82.3(5) . . . . ?
C39 N2 C38 P4 153.7(4) . . . . ?
C61 P4 C38 N2 -78.7(4) . . . . ?
C67 P4 C38 N2 171.8(4) . . . . ?
Pt2 P4 C38 N2 44.2(4) . . . . ?
C37 N2 C39 C40 166.5(5) . . . . ?
C38 N2 C39 C40 -70.5(6) . . . . ?
N2 C39 C40 C41 -51.3(7) . . . . ?
C39 C40 C41 C42 -60.7(7) . . . . ?
C40 C41 C42 Se2 178.4(4) . . . . ?
C41 C42 Se2 C43 81.7(5) . . . . ?
C42 Se2 C43 C44 173.7(5) . . . . ?
C42 Se2 C43 C48 -5.8(6) . . . . ?
C48 C43 C44 C45 -2.4(10) . . . . ?
Se2 C43 C44 C45 178.1(6) . . . . ?
C43 C44 C45 C46 0.3(11) . . . . ?
C44 C45 C46 C47 1.9(11) . . . . ?
C45 C46 C47 C48 -1.9(11) . . . . ?
C46 C47 C48 C43 -0.2(11) . . . . ?
C44 C43 C48 C47 2.3(10) . . . . ?
Se2 C43 C48 C47 -178.2(5) . . . . ?
C55 P3 C49 C50 -6.0(6) . . . . ?
C37 P3 C49 C50 -115.1(5) . . . . ?
Pt2 P3 C49 C50 117.4(5) . . . . ?
C55 P3 C49 C54 176.0(4) . . . . ?
C37 P3 C49 C54 66.9(5) . . . . ?
Pt2 P3 C49 C54 -60.6(5) . . . . ?
C54 C49 C50 C51 -1.0(9) . . . . ?
P3 C49 C50 C51 -178.9(5) . . . . ?
C49 C50 C51 C52 0.7(10) . . . . ?
C50 C51 C52 C53 -0.6(10) . . . . ?
C51 C52 C53 C54 0.7(10) . . . . ?
C52 C53 C54 C49 -0.9(9) . . . . ?
C50 C49 C54 C53 1.1(9) . . . . ?
P3 C49 C54 C53 179.2(5) . . . . ?
C49 P3 C55 C60 116.6(5) . . . . ?
C37 P3 C55 C60 -135.1(5) . . . . ?
Pt2 P3 C55 C60 -8.5(5) . . . . ?
C49 P3 C55 C56 -66.2(5) . . . . ?
C37 P3 C55 C56 42.1(5) . . . . ?
Pt2 P3 C55 C56 168.6(4) . . . . ?
C60 C55 C56 C57 0.6(9) . . . . ?
P3 C55 C56 C57 -176.6(5) . . . . ?
C55 C56 C57 C58 -0.4(10) . . . . ?
C56 C57 C58 C59 0.7(10) . . . . ?
C57 C58 C59 C60 -1.3(10) . . . . ?
C56 C55 C60 C59 -1.2(9) . . . . ?
P3 C55 C60 C59 176.0(5) . . . . ?
C58 C59 C60 C55 1.5(9) . . . . ?
C67 P4 C61 C66 -148.6(5) . . . . ?
C38 P4 C61 C66 105.9(5) . . . . ?
Pt2 P4 C61 C66 -20.9(5) . . . . ?
C67 P4 C61 C62 37.6(5) . . . . ?
C38 P4 C61 C62 -67.9(5) . . . . ?
Pt2 P4 C61 C62 165.4(4) . . . . ?
C66 C61 C62 C63 0.3(9) . . . . ?
P4 C61 C62 C63 174.1(5) . . . . ?
C61 C62 C63 C64 -1.4(10) . . . . ?
C62 C63 C64 C65 1.1(10) . . . . ?
C63 C64 C65 C66 0.3(10) . . . . ?
C62 C61 C66 C65 1.1(9) . . . . ?
P4 C61 C66 C65 -172.8(4) . . . . ?
C64 C65 C66 C61 -1.4(9) . . . . ?
C61 P4 C67 C68 -144.0(4) . . . . ?
C38 P4 C67 C68 -37.9(5) . . . . ?
Pt2 P4 C67 C68 90.7(4) . . . . ?
C61 P4 C67 C72 34.1(5) . . . . ?
C38 P4 C67 C72 140.3(4) . . . . ?
Pt2 P4 C67 C72 -91.1(4) . . . . ?
C72 C67 C68 C69 -3.9(8) . . . . ?
P4 C67 C68 C69 174.3(4) . . . . ?
C67 C68 C69 C70 1.8(8) . . . . ?
C68 C69 C70 C71 1.3(8) . . . . ?
C69 C70 C71 C72 -2.2(9) . . . . ?
C70 C71 C72 C67 0.0(9) . . . . ?
C68 C67 C72 C71 3.1(8) . . . . ?
P4 C67 C72 C71 -175.2(4) . . . . ?
