#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:11:53 +0100 (vie 25 de mar de 2016) $
#$Revision: 180064 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/10/7051058.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7051058
loop_
_publ_author_name
'Rice, Craig R.'
'Guerrero, Ana'
'Bell, Zöe R.'
'Paul, Rowena L.'
'Motson, Graham R.'
'Jeffery, John C.'
'Ward, Michael D.'
_publ_section_title
;
 New hybrid ditopic ligands containing fused phenanthroline and crown
 ether units
;
_journal_issue                   2
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              185
_journal_paper_doi               10.1039/b008378j
_journal_volume                  25
_journal_year                    2001
_chemical_formula_sum            'C36 H29 Cl2 N7 O10 Ru'
_chemical_formula_weight         891.63
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                81.7780(10)
_cell_angle_beta                 80.3950(10)
_cell_angle_gamma                78.8510(10)
_cell_formula_units_Z            2
_cell_length_a                   8.7139(4)
_cell_length_b                   12.6362(5)
_cell_length_c                   16.8896(7)
_cell_measurement_temperature    173(2)
_cell_volume                     1787.22(13)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device       'Siemens SMART Area Detector'
_diffrn_measurement_method
'ω rotation with narrow frames (0.3 degrees)'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0285
_diffrn_reflns_av_sigmaI/netI    0.0353
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            18754
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.65
_exptl_absorpt_coefficient_mu    0.659
_exptl_absorpt_correction_T_max  0.9370
_exptl_absorpt_correction_T_min  0.8268
_exptl_absorpt_correction_type   'Empirical, pseudo-azimuthal scan (SADABS)'
_exptl_crystal_colour            Orange
_exptl_crystal_density_diffrn    1.657
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Plate
_exptl_crystal_F_000             904
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.956
_refine_diff_density_min         -0.564
_refine_diff_density_rms         0.074
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.028
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     535
_refine_ls_number_reflns         8108
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.028
_refine_ls_R_factor_all          0.0451
_refine_ls_R_factor_gt           0.0356
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0487P)²+1.3353P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0888
_refine_ls_wR_factor_ref         0.0932
_reflns_number_gt                6910
_reflns_number_total             8108
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b008378j.txt
_cod_data_source_block           sad1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7051058
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru -0.61572(2) -0.323806(15) -0.259281(11) 0.02242(7) Uani 1 1 d . . .
N11 N -0.5684(2) -0.28394(17) -0.15320(12) 0.0269(4) Uani 1 1 d . . .
C12 C -0.5952(3) -0.1763(2) -0.14498(15) 0.0291(5) Uani 1 1 d . . .
C13 C -0.5682(3) -0.1390(2) -0.07604(17) 0.0378(6) Uani 1 1 d . . .
H13 H -0.5864 -0.0633 -0.0717 0.045 Uiso 1 1 calc R . .
C14 C -0.5149(3) -0.2123(3) -0.01409(17) 0.0403(7) Uani 1 1 d . . .
H14 H -0.4945 -0.1879 0.0331 0.048 Uiso 1 1 calc R . .
C15 C -0.4914(4) -0.3222(3) -0.02136(17) 0.0393(6) Uani 1 1 d . . .
H15 H -0.4576 -0.3743 0.0214 0.047 Uiso 1 1 calc R . .
C16 C -0.5176(3) -0.3547(2) -0.09138(16) 0.0332(6) Uani 1 1 d . . .
H16 H -0.4994 -0.4302 -0.0965 0.040 Uiso 1 1 calc R . .
N21 N -0.6902(3) -0.15799(17) -0.27224(13) 0.0273(4) Uani 1 1 d . . .
C22 C -0.6576(3) -0.1055(2) -0.21367(16) 0.0302(5) Uani 1 1 d . . .
C23 C -0.6865(4) 0.0067(2) -0.2193(2) 0.0457(7) Uani 1 1 d . . .
H23 H -0.6579 0.0423 -0.1795 0.055 Uiso 1 1 calc R . .
C24 C -0.7565(5) 0.0669(3) -0.2825(2) 0.0544(9) Uani 1 1 d . . .
H24 H -0.7782 0.1439 -0.2862 0.065 Uiso 1 1 calc R . .
C25 C -0.7944(4) 0.0140(2) -0.3399(2) 0.0479(8) Uani 1 1 d . . .
H25 H -0.8453 0.0538 -0.3833 0.057 Uiso 1 1 calc R . .
C26 C -0.7576(4) -0.0982(2) -0.33383(17) 0.0369(6) Uani 1 1 d . . .
H26 H -0.7810 -0.1344 -0.3748 0.044 Uiso 1 1 calc R . .
N31 N -0.4076(2) -0.29251(17) -0.32894(12) 0.0268(4) Uani 1 1 d . . .
C32 C -0.3962(3) -0.2991(2) -0.40926(15) 0.0285(5) Uani 1 1 d . . .
C33 C -0.2686(3) -0.2709(2) -0.46352(17) 0.0366(6) Uani 1 1 d . . .
H33 H -0.2621 -0.2774 -0.5194 0.044 Uiso 1 1 calc R . .
C34 C -0.1512(3) -0.2333(3) -0.43573(18) 0.0403(7) Uani 1 1 d . . .
H34 H -0.0632 -0.2133 -0.4721 0.048 Uiso 1 1 calc R . .
C35 C -0.1637(3) -0.2252(2) -0.35450(18) 0.0382(6) Uani 1 1 d . . .
H35 H -0.0847 -0.1988 -0.3342 0.046 Uiso 1 1 calc R . .
C36 C -0.2917(3) -0.2557(2) -0.30264(17) 0.0338(6) Uani 1 1 d . . .
H36 H -0.2985 -0.2507 -0.2465 0.041 Uiso 1 1 calc R . .
N41 N -0.6497(2) -0.35125(16) -0.37246(12) 0.0249(4) Uani 1 1 d . . .
C42 C -0.5303(3) -0.3353(2) -0.43358(15) 0.0283(5) Uani 1 1 d . . .
C43 C -0.5388(4) -0.3508(2) -0.51250(16) 0.0360(6) Uani 1 1 d . . .
H43 H -0.4548 -0.3386 -0.5546 0.043 Uiso 1 1 calc R . .
C44 C -0.6710(4) -0.3842(2) -0.52887(17) 0.0386(6) Uani 1 1 d . . .
H44 H -0.6796 -0.3941 -0.5826 0.046 Uiso 1 1 calc R . .
C45 C -0.7905(3) -0.4030(2) -0.46663(17) 0.0359(6) Uani 1 1 d . . .
H45 H -0.8814 -0.4272 -0.4767 0.043 Uiso 1 1 calc R . .
C46 C -0.7757(3) -0.3861(2) -0.38961(16) 0.0307(5) Uani 1 1 d . . .
H46 H -0.8579 -0.3996 -0.3469 0.037 Uiso 1 1 calc R . .
N51 N -0.5514(2) -0.49062(16) -0.23469(12) 0.0238(4) Uani 1 1 d . . .
C52 C -0.6719(3) -0.5401(2) -0.19263(14) 0.0239(5) Uani 1 1 d . . .
C53 C -0.6565(3) -0.6527(2) -0.17144(14) 0.0266(5) Uani 1 1 d . . .
C54 C -0.5099(3) -0.7167(2) -0.19635(16) 0.0310(5) Uani 1 1 d . . .
H54 H -0.4948 -0.7935 -0.1849 0.037 Uiso 1 1 calc R . .
C55 C -0.3891(3) -0.6663(2) -0.23744(16) 0.0332(6) Uani 1 1 d . . .
H55 H -0.2889 -0.7084 -0.2537 0.040 Uiso 1 1 calc R . .
C56 C -0.4129(3) -0.5533(2) -0.25546(15) 0.0295(5) Uani 1 1 d . . .
H56 H -0.3273 -0.5201 -0.2835 0.035 Uiso 1 1 calc R . .
N61 N -0.8243(2) -0.36245(16) -0.19454(12) 0.0245(4) Uani 1 1 d . . .
C62 C -0.8177(3) -0.47079(19) -0.16909(14) 0.0240(5) Uani 1 1 d . . .
C63 C -0.9453(3) -0.5141(2) -0.12266(14) 0.0270(5) Uani 1 1 d . . .
C64 C -1.0848(3) -0.4411(2) -0.10087(16) 0.0324(6) Uani 1 1 d . . .
H64 H -1.1743 -0.4666 -0.0696 0.039 Uiso 1 1 calc R . .
C65 C -1.0895(3) -0.3325(2) -0.12549(16) 0.0342(6) Uani 1 1 d . . .
H65 H -1.1826 -0.2823 -0.1107 0.041 Uiso 1 1 calc R . .
C66 C -0.9582(3) -0.2951(2) -0.17226(16) 0.0305(5) Uani 1 1 d . . .
H66 H -0.9644 -0.2195 -0.1887 0.037 Uiso 1 1 calc R . .
C71 C -0.9277(3) -0.6292(2) -0.10119(16) 0.0309(5) Uani 1 1 d . . .
C72 C -0.7888(3) -0.6958(2) -0.12499(15) 0.0279(5) Uani 1 1 d . . .
O73 O -0.7671(2) -0.80613(15) -0.10728(12) 0.0371(4) Uani 1 1 d . . .
C74 C -0.8932(5) -0.8440(3) -0.0515(3) 0.0637(11) Uani 1 1 d . . .
H74A H -0.8746 -0.8408 0.0043 0.076 Uiso 1 1 calc R . .
H74B H -0.8921 -0.9210 -0.0577 0.076 Uiso 1 1 calc R . .
C75 C -1.0479(4) -0.7818(3) -0.0629(3) 0.0606(10) Uani 1 1 d . . .
H75A H -1.0723 -0.7923 -0.1161 0.073 Uiso 1 1 calc R . .
H75B H -1.1284 -0.8096 -0.0208 0.073 Uiso 1 1 calc R . .
O76 O -1.0582(2) -0.66719(17) -0.05912(13) 0.0404(5) Uani 1 1 d . . .
Cl1 Cl 0.02628(8) -0.63490(6) -0.33637(4) 0.03906(16) Uani 1 1 d . . .
O11 O -0.0551(3) -0.5329(2) -0.3689(2) 0.0798(9) Uani 1 1 d . . .
O12 O -0.0271(3) -0.6562(3) -0.25328(15) 0.0837(10) Uani 1 1 d . . .
O13 O -0.0104(3) -0.7174(2) -0.37687(17) 0.0691(8) Uani 1 1 d . . .
O14 O 0.1947(3) -0.6379(2) -0.34884(14) 0.0500(6) Uani 1 1 d . . .
Cl2 Cl -1.19722(9) -1.00156(6) -0.15801(5) 0.04241(17) Uani 1 1 d . . .
O21 O -1.1894(4) -0.9063(2) -0.2149(2) 0.0858(10) Uani 1 1 d . . .
O22 O -1.3141(4) -0.9752(3) -0.0924(2) 0.0906(11) Uani 1 1 d . . .
O23 O -1.2372(3) -1.08446(19) -0.19558(16) 0.0569(6) Uani 1 1 d . . .
O24 O -1.0440(3) -1.0382(2) -0.13317(16) 0.0567(6) Uani 1 1 d . . .
N200 N -0.0979(12) 0.0485(8) -0.4825(5) 0.094(3) Uani 0.50 1 d P A 1
C201 C -0.2128(16) 0.0562(9) -0.4381(6) 0.073(3) Uani 0.50 1 d P A 1
C202 C -0.3574(15) 0.0624(10) -0.3834(9) 0.077(3) Uani 0.50 1 d P A 1
H20A H -0.4137 0.0053 -0.3909 0.115 Uiso 0.50 1 calc PR A 1
H20B H -0.4234 0.1336 -0.3941 0.115 Uiso 0.50 1 calc PR A 1
H20C H -0.3344 0.0526 -0.3277 0.115 Uiso 0.50 1 calc PR A 1
N210 N -0.4479(12) 0.0390(9) -0.4785(6) 0.106(3) Uani 0.50 1 d P . 2
C211 C -0.3698(15) 0.0570(8) -0.4385(7) 0.078(3) Uani 0.50 1 d P B 2
C212 C -0.265(2) 0.0806(12) -0.3861(11) 0.108(5) Uani 0.50 1 d P B 2
H21A H -0.3018 0.1542 -0.3706 0.162 Uiso 0.50 1 calc PR B 2
H21B H -0.1570 0.0754 -0.4152 0.162 Uiso 0.50 1 calc PR B 2
H21C H -0.2657 0.0281 -0.3374 0.162 Uiso 0.50 1 calc PR B 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N11 Ru1 N21 78.95(8) . . ?
N11 Ru1 N31 96.42(8) . . ?
N21 Ru1 N31 86.09(8) . . ?
N11 Ru1 N61 86.86(8) . . ?
N21 Ru1 N61 96.30(8) . . ?
N31 Ru1 N61 176.28(8) . . ?
N11 Ru1 N41 173.83(8) . . ?
N21 Ru1 N41 97.23(8) . . ?
N31 Ru1 N41 78.39(8) . . ?
N61 Ru1 N41 98.44(8) . . ?
N11 Ru1 N51 96.93(8) . . ?
N21 Ru1 N51 174.43(8) . . ?
N31 Ru1 N51 98.17(8) . . ?
N61 Ru1 N51 79.63(8) . . ?
N41 Ru1 N51 87.19(8) . . ?
C16 N11 C12 118.1(2) . . ?
C16 N11 Ru1 125.89(18) . . ?
C12 N11 Ru1 115.97(17) . . ?
N11 C12 C13 121.5(3) . . ?
N11 C12 C22 114.4(2) . . ?
C13 C12 C22 124.1(2) . . ?
C14 C13 C12 119.5(3) . . ?
C13 C14 C15 119.2(3) . . ?
C16 C15 C14 118.9(3) . . ?
N11 C16 C15 122.7(3) . . ?
C26 N21 C22 118.3(2) . . ?
C26 N21 Ru1 126.73(19) . . ?
C22 N21 Ru1 114.86(17) . . ?
N21 C22 C23 120.9(3) . . ?
N21 C22 C12 115.3(2) . . ?
C23 C22 C12 123.8(3) . . ?
C24 C23 C22 120.1(3) . . ?
C25 C24 C23 119.0(3) . . ?
C24 C25 C26 119.1(3) . . ?
N21 C26 C25 122.5(3) . . ?
C36 N31 C32 118.2(2) . . ?
C36 N31 Ru1 125.43(18) . . ?
C32 N31 Ru1 116.02(17) . . ?
N31 C32 C33 121.7(2) . . ?
N31 C32 C42 114.9(2) . . ?
C33 C32 C42 123.4(2) . . ?
C34 C33 C32 119.4(3) . . ?
C35 C34 C33 118.9(3) . . ?
C34 C35 C36 119.6(3) . . ?
N31 C36 C35 122.2(3) . . ?
C46 N41 C42 118.3(2) . . ?
C46 N41 Ru1 125.82(17) . . ?
C42 N41 Ru1 115.86(17) . . ?
N41 C42 C43 121.5(2) . . ?
N41 C42 C32 114.7(2) . . ?
C43 C42 C32 123.8(2) . . ?
C44 C43 C42 119.1(3) . . ?
C45 C44 C43 119.5(3) . . ?
C46 C45 C44 118.8(3) . . ?
N41 C46 C45 122.8(3) . . ?
C56 N51 C52 117.8(2) . . ?
C56 N51 Ru1 128.80(18) . . ?
C52 N51 Ru1 113.39(16) . . ?
N51 C52 C53 123.2(2) . . ?
N51 C52 C62 116.6(2) . . ?
C53 C52 C62 120.1(2) . . ?
C52 C53 C54 117.4(2) . . ?
C52 C53 C72 118.7(2) . . ?
C54 C53 C72 123.9(2) . . ?
C55 C54 C53 119.0(2) . . ?
C54 C55 C56 120.3(2) . . ?
N51 C56 C55 122.3(2) . . ?
C66 N61 C62 117.8(2) . . ?
C66 N61 Ru1 128.18(18) . . ?
C62 N61 Ru1 113.92(16) . . ?
N61 C62 C63 123.2(2) . . ?
N61 C62 C52 116.3(2) . . ?
C63 C62 C52 120.5(2) . . ?
C62 C63 C64 117.5(2) . . ?
C62 C63 C71 118.8(2) . . ?
C64 C63 C71 123.7(2) . . ?
C65 C64 C63 118.9(2) . . ?
C64 C65 C66 120.5(2) . . ?
N61 C66 C65 122.0(2) . . ?
O76 C71 C72 123.1(2) . . ?
O76 C71 C63 116.1(2) . . ?
C72 C71 C63 120.7(2) . . ?
O73 C72 C71 122.9(2) . . ?
O73 C72 C53 115.8(2) . . ?
C71 C72 C53 121.2(2) . . ?
C72 O73 C74 113.7(2) . . ?
O73 C74 C75 113.3(3) . . ?
O76 C75 C74 112.8(3) . . ?
C71 O76 C75 111.9(2) . . ?
O12 Cl1 O11 110.7(2) . . ?
O12 Cl1 O13 107.98(19) . . ?
O11 Cl1 O13 107.36(19) . . ?
O12 Cl1 O14 109.60(16) . . ?
O11 Cl1 O14 111.32(16) . . ?
O13 Cl1 O14 109.78(16) . . ?
O22 Cl2 O23 109.44(18) . . ?
O22 Cl2 O21 108.7(2) . . ?
O23 Cl2 O21 109.66(19) . . ?
O22 Cl2 O24 111.8(2) . . ?
O23 Cl2 O24 109.19(15) . . ?
O21 Cl2 O24 108.04(18) . . ?
N200 C201 C202 178.0(13) . . ?
C211 N210 N210 157.8(14) . 2_454 ?
N210 C211 C212 179.4(16) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 N11 2.054(2) . ?
Ru1 N21 2.061(2) . ?
Ru1 N31 2.065(2) . ?
Ru1 N61 2.065(2) . ?
Ru1 N41 2.069(2) . ?
Ru1 N51 2.074(2) . ?
N11 C16 1.349(3) . ?
N11 C12 1.358(3) . ?
C12 C13 1.387(4) . ?
C12 C22 1.473(4) . ?
C13 C14 1.374(4) . ?
C14 C15 1.384(4) . ?
C15 C16 1.373(4) . ?
N21 C26 1.344(3) . ?
N21 C22 1.362(3) . ?
C22 C23 1.383(4) . ?
C23 C24 1.377(5) . ?
C24 C25 1.368(5) . ?
C25 C26 1.386(4) . ?
N31 C36 1.350(3) . ?
N31 C32 1.357(3) . ?
C32 C33 1.386(4) . ?
C32 C42 1.471(4) . ?
C33 C34 1.380(4) . ?
C34 C35 1.375(4) . ?
C35 C36 1.379(4) . ?
N41 C46 1.346(3) . ?
N41 C42 1.361(3) . ?
C42 C43 1.391(4) . ?
C43 C44 1.382(4) . ?
C44 C45 1.380(4) . ?
C45 C46 1.379(4) . ?
N51 C56 1.332(3) . ?
N51 C52 1.370(3) . ?
C52 C53 1.403(3) . ?
C52 C62 1.428(3) . ?
C53 C54 1.408(4) . ?
C53 C72 1.435(4) . ?
C54 C55 1.372(4) . ?
C55 C56 1.400(4) . ?
N61 C66 1.338(3) . ?
N61 C62 1.368(3) . ?
C62 C63 1.405(3) . ?
C63 C64 1.407(4) . ?
C63 C71 1.432(4) . ?
C64 C65 1.370(4) . ?
C65 C66 1.399(4) . ?
C71 O76 1.369(3) . ?
C71 C72 1.370(4) . ?
C72 O73 1.366(3) . ?
O73 C74 1.433(4) . ?
C74 C75 1.451(6) . ?
C75 O76 1.443(4) . ?
Cl1 O12 1.407(3) . ?
Cl1 O11 1.428(3) . ?
Cl1 O13 1.437(3) . ?
Cl1 O14 1.442(2) . ?
Cl2 O22 1.405(3) . ?
Cl2 O23 1.423(2) . ?
Cl2 O21 1.434(3) . ?
Cl2 O24 1.437(2) . ?
N200 C201 1.144(14) . ?
C201 C202 1.429(18) . ?
N210 C211 1.108(14) . ?
N210 N210 1.76(2) 2_454 ?
C211 C212 1.471(19) . ?
