#------------------------------------------------------------------------------
#$Date: 2016-02-16 02:10:39 +0100 (mar 16 de feb de 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/24/7102428.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7102428
loop_
_publ_author_name
'Langley, Stuart'
'Helliwell, Madeleine'
'Raftery, James'
'Tolis, Evangelos I'
'Winpenny, Richard E P'
_publ_section_title
;
 Phosphonate ligands encourage a platonic relationship between
 cobalt(II) and alkali metal ions.
;
_journal_issue                   2
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              142
_journal_page_last               143
_journal_paper_doi               10.1039/b312769a
_journal_year                    2004
_chemical_formula_sum            'C109.5 H100 Cl22 Co6 Li9 N18 O23 P'
_chemical_formula_weight         3262.99
_chemical_name_systematic
;
?
;
_space_group_IT_number           147
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-P 3'
_symmetry_space_group_name_H-M   'P -3'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            2
_cell_length_a                   23.5886(12)
_cell_length_b                   23.5886(12)
_cell_length_c                   15.9501(14)
_cell_measurement_reflns_used    8393
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      26.05
_cell_measurement_theta_min      2.36
_cell_volume                     7686.0(9)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0465
_diffrn_reflns_av_sigmaI/netI    0.0432
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            45119
_diffrn_reflns_theta_full        26.46
_diffrn_reflns_theta_max         26.46
_diffrn_reflns_theta_min         1.62
_exptl_absorpt_coefficient_mu    1.088
_exptl_absorpt_correction_T_max  0.8990
_exptl_absorpt_correction_T_min  0.7360
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            pink/purple
_exptl_crystal_density_diffrn    1.410
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3290
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.626
_refine_diff_density_min         -1.033
_refine_diff_density_rms         0.130
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.965
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     598
_refine_ls_number_reflns         10519
_refine_ls_number_restraints     553
_refine_ls_restrained_S_all      0.942
_refine_ls_R_factor_all          0.0753
_refine_ls_R_factor_gt           0.0537
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1060P)²+20.8805P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1567
_refine_ls_wR_factor_ref         0.1736
_reflns_number_gt                7965
_reflns_number_total             10519
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b312769a.txt
_cod_data_source_block           s1533abs
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal' according
to '/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-3
_cod_original_formula_sum        'C109.50 H100 Cl22 Co6 Li9 N18 O23 P'
_cod_database_code               7102428
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.39095(3) 0.63449(3) 0.54639(3) 0.01714(14) Uani 1 1 d U . .
Co2 Co 0.13934(3) 0.43188(3) 0.25916(3) 0.01875(14) Uani 1 1 d U . .
Li1 Li 0.4841(3) 0.7424(3) 0.4013(4) 0.0193(13) Uani 1 1 d U . .
Li2 Li 0.2885(3) 0.5763(3) 0.2281(4) 0.0196(12) Uani 1 1 d U . .
Li3 Li 0.1901(3) 0.5893(3) 0.3378(4) 0.0199(12) Uani 1 1 d U . .
Cl1 Cl 0.43659(6) 0.75204(6) 0.91499(7) 0.0373(3) Uani 1 1 d U . .
Cl2 Cl 0.45426(6) 0.56336(6) 0.73871(7) 0.0351(3) Uani 1 1 d U . .
Cl3 Cl 0.24284(6) 0.38907(6) 0.02501(7) 0.0315(3) Uani 1 1 d U . .
Cl4 Cl -0.00611(6) 0.27013(6) 0.34918(9) 0.0427(3) Uani 1 1 d U . .
Cl5 Cl -0.01906(5) 0.38459(7) 0.13550(8) 0.0418(3) Uani 1 1 d U . .
Cl6 Cl 0.09546(7) 0.27493(7) 0.13091(8) 0.0429(3) Uani 1 1 d U . .
Cl7 Cl 0.36070(5) 0.53813(4) 0.45928(6) 0.0189(2) Uani 1 1 d U . .
Cl8 Cl 0.3333 0.6667 0.13747(10) 0.0196(3) Uani 1 3 d SU . .
P1 P 0.3333 0.6667 0.37451(10) 0.0138(3) Uani 1 3 d SU . .
O1 O 0.41051(14) 0.71823(13) 0.61483(18) 0.0215(6) Uani 1 1 d U . .
O2 O 0.47960(13) 0.68700(14) 0.48736(17) 0.0210(6) Uani 1 1 d U . .
O3 O 0.35522(13) 0.55104(13) 0.24206(17) 0.0195(6) Uani 1 1 d U . .
O4 O 0.12379(13) 0.50348(13) 0.31927(17) 0.0199(6) Uani 1 1 d U . .
O5 O 0.21446(13) 0.50405(13) 0.17365(17) 0.0191(6) Uani 1 1 d U . .
O6 O 0.21456(14) 0.43885(14) 0.33834(18) 0.0225(6) Uani 1 1 d U . .
O7 O 0.3333 0.6667 0.4727(3) 0.0148(9) Uani 1 3 d SU . .
O8 O 0.27878(12) 0.60014(12) 0.34263(16) 0.0152(5) Uani 1 1 d U . .
N1 N 0.42956(17) 0.73722(17) 0.7526(2) 0.0219(7) Uani 1 1 d U . .
N2 N 0.47537(17) 0.63257(17) 0.6027(2) 0.0215(7) Uani 1 1 d U . .
N3 N 0.30960(17) 0.47394(17) 0.1409(2) 0.0216(7) Uani 1 1 d U . .
N4 N 0.05832(16) 0.39717(16) 0.3389(2) 0.0210(7) Uani 1 1 d U . .
N5 N 0.10787(16) 0.45274(17) 0.1456(2) 0.0206(7) Uani 1 1 d U . .
N6 N 0.16600(17) 0.36075(17) 0.2440(2) 0.0223(7) Uani 1 1 d U . .
C1 C 0.4543(2) 0.75065(19) 0.6743(3) 0.0204(8) Uani 1 1 d U . .
C2 C 0.5197(2) 0.7951(2) 0.6574(3) 0.0260(9) Uani 1 1 d U . .
H2 H 0.5361 0.8023 0.6017 0.031 Uiso 1 1 calc R . .
C3 C 0.5597(2) 0.8280(2) 0.7239(3) 0.0297(10) Uani 1 1 d U . .
H3 H 0.6044 0.8592 0.7141 0.036 Uiso 1 1 calc R . .
C4 C 0.5355(2) 0.8162(2) 0.8052(3) 0.0295(10) Uani 1 1 d U . .
H4 H 0.5625 0.8387 0.8518 0.035 Uiso 1 1 calc R . .
C5 C 0.4707(2) 0.7703(2) 0.8147(3) 0.0262(9) Uani 1 1 d U . .
C6 C 0.5123(2) 0.6730(2) 0.5401(3) 0.0214(8) Uani 1 1 d U . .
C7 C 0.5802(2) 0.6976(2) 0.5357(3) 0.0284(9) Uani 1 1 d U . .
H7 H 0.6059 0.7272 0.4927 0.034 Uiso 1 1 calc R . .
C8 C 0.6080(2) 0.6773(3) 0.5953(3) 0.0388(12) Uani 1 1 d U . .
H8 H 0.6536 0.6926 0.5934 0.047 Uiso 1 1 calc R . .
C9 C 0.5697(2) 0.6343(3) 0.6593(3) 0.0387(12) Uani 1 1 d U . .
H9 H 0.5883 0.6194 0.7005 0.046 Uiso 1 1 calc R . .
C10 C 0.5046(2) 0.6149(2) 0.6598(3) 0.0282(9) Uani 1 1 d U . .
C11 C 0.3590(2) 0.5093(2) 0.1986(2) 0.0206(8) Uani 1 1 d U . .
C12 C 0.4097(2) 0.4937(2) 0.2021(3) 0.0226(8) Uani 1 1 d U . .
H12 H 0.4451 0.5164 0.2400 0.027 Uiso 1 1 calc R . .
C13 C 0.4080(2) 0.4465(2) 0.1513(3) 0.0289(10) Uani 1 1 d U . .
H13 H 0.4426 0.4370 0.1543 0.035 Uiso 1 1 calc R . .
C14 C 0.3563(2) 0.4113(2) 0.0944(3) 0.0311(10) Uani 1 1 d U . .
H14 H 0.3550 0.3779 0.0598 0.037 Uiso 1 1 calc R . .
C15 C 0.3090(2) 0.4273(2) 0.0913(3) 0.0241(9) Uani 1 1 d U . .
C16 C 0.07088(19) 0.4590(2) 0.3541(3) 0.0214(8) Uani 1 1 d U . .
C17 C 0.0270(2) 0.4702(2) 0.4012(3) 0.0303(10) Uani 1 1 d U . .
H17 H 0.0350 0.5132 0.4109 0.036 Uiso 1 1 calc R . .
C18 C -0.0276(2) 0.4165(3) 0.4325(3) 0.0371(11) Uani 1 1 d U . .
H18 H -0.0580 0.4229 0.4644 0.044 Uiso 1 1 calc R . .
C19 C -0.0399(2) 0.3537(2) 0.4192(3) 0.0358(11) Uani 1 1 d U . .
H19 H -0.0775 0.3169 0.4418 0.043 Uiso 1 1 calc R . .
C20 C 0.0050(2) 0.3469(2) 0.3715(3) 0.0278(9) Uani 1 1 d U . .
C21 C 0.16884(19) 0.49965(19) 0.1227(2) 0.0194(8) Uani 1 1 d U . .
C22 C 0.1788(2) 0.5392(2) 0.0527(3) 0.0269(9) Uani 1 1 d U . .
H22 H 0.2215 0.5729 0.0378 0.032 Uiso 1 1 calc R . .
C23 C 0.1255(2) 0.5282(2) 0.0065(3) 0.0324(10) Uani 1 1 d U . .
H23 H 0.1313 0.5543 -0.0416 0.039 Uiso 1 1 calc R . .
C24 C 0.0629(2) 0.4792(2) 0.0291(3) 0.0330(10) Uani 1 1 d U . .
H24 H 0.0256 0.4706 -0.0032 0.040 Uiso 1 1 calc R . .
C25 C 0.0572(2) 0.4439(2) 0.0998(3) 0.0259(9) Uani 1 1 d U . .
C26 C 0.2137(2) 0.3896(2) 0.3032(3) 0.0217(8) Uani 1 1 d U . .
C27 C 0.2566(2) 0.3654(2) 0.3189(3) 0.0307(10) Uani 1 1 d U . .
H27 H 0.2902 0.3853 0.3599 0.037 Uiso 1 1 calc R . .
C28 C 0.2486(3) 0.3127(3) 0.2737(4) 0.0463(14) Uani 1 1 d U . .
H28 H 0.2776 0.2962 0.2831 0.056 Uiso 1 1 calc R . .
C29 C 0.1989(3) 0.2823(3) 0.2137(4) 0.0482(14) Uani 1 1 d U . .
H29 H 0.1932 0.2456 0.1823 0.058 Uiso 1 1 calc R . .
C30 C 0.1590(2) 0.3085(2) 0.2030(3) 0.0318(10) Uani 1 1 d U . .
C1S C 0.0626(8) 0.1128(7) 0.2531(12) 0.081(4) Uani 0.50 1 d PU . .
H1S1 H 0.0277 0.0728 0.2273 0.122 Uiso 0.50 1 calc PR . .
H1S2 H 0.1027 0.1101 0.2562 0.122 Uiso 0.50 1 calc PR . .
H1S3 H 0.0707 0.1508 0.2192 0.122 Uiso 0.50 1 calc PR . .
C2S C 0.0439(8) 0.1194(7) 0.3332(13) 0.084(4) Uani 0.50 1 d PU . .
H2S1 H 0.0361 0.0807 0.3662 0.101 Uiso 0.50 1 calc PR . .
H2S2 H 0.0015 0.1184 0.3289 0.101 Uiso 0.50 1 calc PR . .
C3S C 0.0933(6) 0.1834(6) 0.3847(10) 0.061(3) Uani 0.50 1 d PU B .
H3S1 H 0.1360 0.1851 0.3861 0.073 Uiso 0.50 1 calc PR . .
H3S2 H 0.0996 0.2218 0.3520 0.073 Uiso 0.50 1 calc PR . .
C4S C 0.0774(6) 0.1922(6) 0.4712(10) 0.061(3) Uani 0.50 1 d PU . .
H4S1 H 0.0332 0.1872 0.4711 0.073 Uiso 0.50 1 calc PR A 1
H4S2 H 0.0752 0.1563 0.5057 0.073 Uiso 0.50 1 calc PR A 1
C5S C 0.1191(6) 0.2500(6) 0.5097(7) 0.065(4) Uiso 0.614(15) 1 d PU B 1
H5S1 H 0.1207 0.2863 0.4765 0.078 Uiso 0.614(15) 1 calc PR B 1
H5S2 H 0.1636 0.2557 0.5098 0.078 Uiso 0.614(15) 1 calc PR B 1
C5T C 0.0992(13) 0.1908(13) 0.5857(16) 0.094(8) Uiso 0.386(15) 1 d PU B 2
H5T1 H 0.0654 0.1523 0.6166 0.113 Uiso 0.386(15) 1 calc PR B 2
H5T2 H 0.1428 0.1948 0.5933 0.113 Uiso 0.386(15) 1 calc PR B 2
C6S C 0.0987(9) 0.2556(7) 0.6067(12) 0.089(5) Uani 0.50 1 d PU . .
H6S1 H 0.1305 0.2984 0.6298 0.133 Uiso 0.50 1 calc PR B 1
H6S2 H 0.0986 0.2209 0.6407 0.133 Uiso 0.50 1 calc PR B 1
H6S3 H 0.0550 0.2508 0.6073 0.133 Uiso 0.50 1 calc PR B 1
O1S O 0.3333 0.6667 0.7296(7) 0.088(3) Uani 1 3 d S . .
C7S C 0.0994 0.3476 0.8872 0.068 Uiso 0.25 1 d PU . .
C8S C 0.1541 0.3196 0.8722 0.041 Uiso 0.50 1 d PU . .
C9S C 0.1352 0.3068 0.8914 0.065 Uiso 0.50 1 d PU . .
C10S C 0.1453 0.2161 0.9332 0.039 Uiso 0.25 1 d PU . .
C11S C 0.1705 0.2489 0.8602 0.045 Uiso 0.25 1 d PU . .
C12S C 0.1078 0.2463 0.9050 0.045 Uiso 0.25 1 d PU . .
C14S C 0.0481 0.2179 0.9133 0.065 Uiso 0.25 1 d PU . .
C15S C 0.1091 0.3336 0.8458 0.036 Uiso 0.25 1 d PU . .
C16S C 0.1206 0.3969 0.8875 0.035 Uiso 0.50 1 d PU . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Co1 O2 173.91(12) 3_565 .
O1 Co1 O1 84.95(16) 3_565 .
O2 Co1 O1 89.56(12) . .
O1 Co1 O7 82.19(11) 3_565 .
O2 Co1 O7 99.55(10) . .
O1 Co1 O7 80.55(10) . .
O1 Co1 N2 114.78(12) 3_565 .
O2 Co1 N2 62.65(12) . .
O1 Co1 N2 91.82(12) . .
O7 Co1 N2 160.88(10) . .
O1 Co1 Cl7 93.63(9) 3_565 .
O2 Co1 Cl7 92.07(8) . .
O1 Co1 Cl7 174.72(8) . .
O7 Co1 Cl7 94.23(7) . .
N2 Co1 Cl7 93.39(9) . .
N6 Co2 N4 109.92(14) . .
N6 Co2 N5 111.86(13) . .
N4 Co2 N5 104.73(13) . .
N6 Co2 O6 63.40(12) . .
N4 Co2 O6 103.54(12) . .
N5 Co2 O6 150.99(12) . .
N6 Co2 O4 159.20(12) . .
N4 Co2 O4 63.28(12) . .
N5 Co2 O4 88.93(12) . .
O6 Co2 O4 98.05(11) . .
N6 Co2 O5 95.75(12) . .
N4 Co2 O5 154.25(12) . .
N5 Co2 O5 61.96(11) . .
O6 Co2 O5 89.44(11) . .
O4 Co2 O5 93.25(10) . .
N6 Co2 C26 32.82(13) . .
N4 Co2 C26 110.91(13) . .
N5 Co2 C26 136.94(13) . .
O6 Co2 C26 30.63(12) . .
O4 Co2 C26 128.37(12) . .
O5 Co2 C26 91.65(12) . .
N6 Co2 C16 139.99(14) . .
N4 Co2 C16 32.60(13) . .
N5 Co2 C16 96.43(13) . .
O6 Co2 C16 103.92(12) . .
O4 Co2 C16 30.73(12) . .
O5 Co2 C16 122.99(12) . .
C26 Co2 C16 126.58(13) . .
O2 Li1 O6 113.1(3) . 2_665
O2 Li1 O8 97.4(3) . 2_665
O6 Li1 O8 116.8(4) 2_665 2_665
O2 Li1 Cl7 108.2(3) . 2_665
O6 Li1 Cl7 115.3(3) 2_665 2_665
O8 Li1 Cl7 104.2(3) 2_665 2_665
O2 Li1 Li2 130.8(3) . 2_665
O6 Li1 Li2 81.6(3) 2_665 2_665
O8 Li1 Li2 39.76(19) 2_665 2_665
Cl7 Li1 Li2 106.0(3) 2_665 2_665
O2 Li1 Li3 71.1(3) . 2_665
O6 Li1 Li3 100.4(3) 2_665 2_665
O8 Li1 Li3 39.44(19) 2_665 2_665
Cl7 Li1 Li3 139.8(3) 2_665 2_665
Li2 Li1 Li3 59.9(2) 2_665 2_665
O2 Li1 P1 92.9(3) . .
O6 Li1 P1 139.4(3) 2_665 .
O8 Li1 P1 25.01(12) 2_665 .
Cl7 Li1 P1 82.39(18) 2_665 .
Li2 Li1 P1 58.03(18) 2_665 .
Li3 Li1 P1 57.85(17) 2_665 .
O2 Li1 Li3 137.3(3) . 3_565
O6 Li1 Li3 109.4(3) 2_665 3_565
O8 Li1 Li3 66.9(2) 2_665 3_565
Cl7 Li1 Li3 46.06(16) 2_665 3_565
Li2 Li1 Li3 60.2(2) 2_665 3_565
Li3 Li1 Li3 106.1(3) 2_665 3_565
P1 Li1 Li3 55.68(16) . 3_565
O5 Li2 O3 107.0(3) . .
O5 Li2 O8 119.2(3) . .
O3 Li2 O8 102.1(3) . .
O5 Li2 Cl8 108.8(3) . .
O3 Li2 Cl8 106.4(3) . .
O8 Li2 Cl8 112.2(3) . .
O5 Li2 P1 145.6(3) . .
O3 Li2 P1 94.4(3) . .
O8 Li2 P1 27.54(12) . .
Cl8 Li2 P1 89.7(2) . .
O5 Li2 Li1 95.7(3) . 3_565
O3 Li2 Li1 77.8(3) . 3_565
O8 Li2 Li1 41.40(19) . 3_565
Cl8 Li2 Li1 152.1(3) . 3_565
P1 Li2 Li1 62.40(18) . 3_565
O5 Li2 Li3 87.0(3) . .
O3 Li2 Li3 137.5(3) . .
O8 Li2 Li3 39.63(19) . .
Cl8 Li2 Li3 106.4(3) . .
P1 Li2 Li3 59.51(18) . .
Li1 Li2 Li3 60.7(2) 3_565 .
O5 Li2 Li3 138.4(3) . 2_665
O3 Li2 Li3 36.38(19) . 2_665
O8 Li2 Li3 70.1(2) . 2_665
Cl8 Li2 Li3 102.7(2) . 2_665
P1 Li2 Li3 58.09(17) . 2_665
Li1 Li2 Li3 63.9(2) 3_565 2_665
Li3 Li2 Li3 109.6(3) . 2_665
O5 Li2 Li2 153.2(2) . 2_665
O3 Li2 Li2 75.8(3) . 2_665
O8 Li2 Li2 85.03(18) . 2_665
Cl8 Li2 Li2 47.02(12) . 2_665
P1 Li2 Li2 57.51(10) . 2_665
Li1 Li2 Li2 110.74(19) 3_565 2_665
Li3 Li2 Li2 109.1(2) . 2_665
Li3 Li2 Li2 57.1(2) 2_665 2_665
O5 Li2 Li2 115.2(4) . 3_565
O3 Li2 Li2 135.3(3) . 3_565
O8 Li2 Li2 69.7(2) . 3_565
Cl8 Li2 Li2 47.02(12) . 3_565
P1 Li2 Li2 57.51(10) . 3_565
Li1 Li2 Li2 110.6(2) 3_565 3_565
Li3 Li2 Li2 61.0(3) . 3_565
Li3 Li2 Li2 106.0(2) 2_665 3_565
Li2 Li2 Li2 60.0 2_665 3_565
O4 Li3 O3 109.9(3) . 3_565
O4 Li3 O8 114.0(3) . .
O3 Li3 O8 103.2(3) 3_565 .
O4 Li3 Cl7 115.2(3) . 3_565
O3 Li3 Cl7 106.7(3) 3_565 3_565
O8 Li3 Cl7 107.0(3) . 3_565
O4 Li3 P1 140.7(3) . .
O3 Li3 P1 93.7(2) 3_565 .
O8 Li3 P1 27.54(12) . .
Cl7 Li3 P1 85.5(2) 3_565 .
O4 Li3 Li2 93.9(3) . .
O3 Li3 Li2 79.6(3) 3_565 .
O8 Li3 Li2 39.14(19) . .
Cl7 Li3 Li2 144.6(3) 3_565 .
P1 Li3 Li2 59.15(18) . .
O4 Li3 Li1 80.3(3) . 3_565
O3 Li3 Li1 138.6(3) 3_565 3_565
O8 Li3 Li1 40.55(19) . 3_565
Cl7 Li3 Li1 104.1(3) 3_565 3_565
P1 Li3 Li1 61.79(17) . 3_565
Li2 Li3 Li1 59.4(2) . 3_565
O4 Li3 Li2 137.3(3) . 3_565
O3 Li3 Li2 36.00(19) 3_565 3_565
O8 Li3 Li2 70.3(2) . 3_565
Cl7 Li3 Li2 102.4(3) 3_565 3_565
P1 Li3 Li2 57.75(17) . 3_565
Li2 Li3 Li2 61.9(3) . 3_565
Li1 Li3 Li2 110.3(3) 3_565 3_565
O4 Li3 Li1 157.5(3) . 2_665
O3 Li3 Li1 71.2(2) 3_565 2_665
O8 Li3 Li1 86.8(3) . 2_665
Cl7 Li3 Li1 46.61(17) 3_565 2_665
P1 Li3 Li1 59.27(16) . 2_665
Li2 Li3 Li1 108.1(3) . 2_665
Li1 Li3 Li1 114.4(3) 3_565 2_665
Li2 Li3 Li1 55.9(2) 3_565 2_665
Li3 Cl7 Li1 87.3(2) 2_665 3_565
Li3 Cl7 Co1 93.56(16) 2_665 .
Li1 Cl7 Co1 102.55(16) 3_565 .
Li2 Cl8 Li2 86.0(2) 3_565 2_665
Li2 Cl8 Li2 86.0(2) 3_565 .
Li2 Cl8 Li2 86.0(2) 2_665 .
O8 P1 O8 109.61(11) 3_565 .
O8 P1 O8 109.61(11) 3_565 2_665
O8 P1 O8 109.61(11) . 2_665
O8 P1 O7 109.34(11) 3_565 .
O8 P1 O7 109.34(11) . .
O8 P1 O7 109.34(11) 2_665 .
O8 P1 Li2 36.12(16) 3_565 3_565
O8 P1 Li2 80.58(17) . 3_565
O8 P1 Li2 101.09(17) 2_665 3_565
O7 P1 Li2 141.66(13) . 3_565
O8 P1 Li2 101.09(17) 3_565 .
O8 P1 Li2 36.12(16) . .
O8 P1 Li2 80.58(17) 2_665 .
O7 P1 Li2 141.66(13) . .
Li2 P1 Li2 65.0(2) 3_565 .
O8 P1 Li2 80.58(17) 3_565 2_665
O8 P1 Li2 101.09(17) . 2_665
O8 P1 Li2 36.12(16) 2_665 2_665
O7 P1 Li2 141.66(13) . 2_665
Li2 P1 Li2 65.0(2) 3_565 2_665
Li2 P1 Li2 65.0(2) . 2_665
O8 P1 Li3 79.70(16) 3_565 .
O8 P1 Li3 36.56(16) . .
O8 P1 Li3 141.92(17) 2_665 .
O7 P1 Li3 101.31(13) . .
Li2 P1 Li3 64.16(19) 3_565 .
Li2 P1 Li3 61.34(18) . .
Li2 P1 Li3 116.99(19) 2_665 .
O8 P1 Li3 36.56(16) 3_565 3_565
O8 P1 Li3 141.92(17) . 3_565
O8 P1 Li3 79.70(16) 2_665 3_565
O7 P1 Li3 101.31(13) . 3_565
Li2 P1 Li3 61.34(18) 3_565 3_565
Li2 P1 Li3 116.99(19) . 3_565
Li2 P1 Li3 64.16(18) 2_665 3_565
Li3 P1 Li3 116.25(9) . 3_565
O8 P1 Li3 141.92(18) 3_565 2_665
O8 P1 Li3 79.70(16) . 2_665
O8 P1 Li3 36.56(16) 2_665 2_665
O7 P1 Li3 101.31(13) . 2_665
Li2 P1 Li3 116.99(19) 3_565 2_665
Li2 P1 Li3 64.16(18) . 2_665
Li2 P1 Li3 61.34(18) 2_665 2_665
Li3 P1 Li3 116.25(9) . 2_665
Li3 P1 Li3 116.25(9) 3_565 2_665
O8 P1 Li1 33.88(16) 3_565 2_665
O8 P1 Li1 101.57(15) . 2_665
O8 P1 Li1 140.01(16) 2_665 2_665
O7 P1 Li1 82.10(13) . 2_665
Li2 P1 Li1 59.56(18) 3_565 2_665
Li2 P1 Li1 114.58(18) . 2_665
Li2 P1 Li1 114.46(18) 2_665 2_665
Li3 P1 Li1 65.05(17) . 2_665
Li3 P1 Li1 60.35(17) 3_565 2_665
Li3 P1 Li1 175.80(18) 2_665 2_665
O8 P1 Li1 140.01(16) 3_565 3_565
O8 P1 Li1 33.88(16) . 3_565
O8 P1 Li1 101.57(15) 2_665 3_565
O7 P1 Li1 82.10(13) . 3_565
Li2 P1 Li1 114.46(18) 3_565 3_565
Li2 P1 Li1 59.56(18) . 3_565
Li2 P1 Li1 114.58(18) 2_665 3_565
Li3 P1 Li1 60.35(17) . 3_565
Li3 P1 Li1 175.80(18) 3_565 3_565
Li3 P1 Li1 65.05(17) 2_665 3_565
Li1 P1 Li1 118.14(6) 2_665 3_565
C1 O1 Co1 124.0(2) . 2_665
C1 O1 Co1 131.0(2) . .
Co1 O1 Co1 102.82(12) 2_665 .
C6 O2 Li1 146.0(3) . .
C6 O2 Co1 96.0(2) . .
Li1 O2 Co1 116.5(2) . .
C11 O3 Li2 124.5(3) . .
C11 O3 Li3 127.9(3) . 2_665
Li2 O3 Li3 107.6(3) . 2_665
C16 O4 Li3 139.7(3) . .
C16 O4 Co2 91.7(2) . .
Li3 O4 Co2 123.4(2) . .
C21 O5 Li2 133.9(3) . .
C21 O5 Co2 90.6(2) . .
Li2 O5 Co2 115.1(2) . .
C26 O6 Li1 150.1(3) . 3_565
C26 O6 Co2 92.1(2) . .
Li1 O6 Co2 115.5(2) 3_565 .
P1 O7 Co1 122.29(10) . 2_665
P1 O7 Co1 122.29(10) . 3_565
Co1 O7 Co1 94.12(13) 2_665 3_565
P1 O7 Co1 122.29(10) . .
Co1 O7 Co1 94.12(13) 2_665 .
Co1 O7 Co1 94.12(13) 3_565 .
P1 O8 Li2 116.3(2) . .
P1 O8 Li3 115.9(2) . .
Li2 O8 Li3 101.2(3) . .
P1 O8 Li1 121.1(2) . 3_565
Li2 O8 Li1 98.8(3) . 3_565
Li3 O8 Li1 100.0(3) . 3_565
C5 N1 C1 116.7(4) . .
C10 N2 C6 118.3(4) . .
C10 N2 Co1 154.3(3) . .
C6 N2 Co1 87.4(2) . .
C15 N3 C11 122.8(4) . .
C20 N4 C16 119.3(4) . .
C20 N4 Co2 149.2(3) . .
C16 N4 Co2 91.3(2) . .
C25 N5 C21 119.0(4) . .
C25 N5 Co2 146.4(3) . .
C21 N5 Co2 93.9(2) . .
C30 N6 C26 119.5(4) . .
C30 N6 Co2 149.0(3) . .
C26 N6 Co2 91.4(2) . .
O1 C1 N1 114.0(4) . .
O1 C1 C2 123.1(4) . .
N1 C1 C2 122.9(4) . .
C3 C2 C1 117.8(4) . .
C3 C2 H2 121.1 . .
C1 C2 H2 121.1 . .
C2 C3 C4 120.7(4) . .
C2 C3 H3 119.6 . .
C4 C3 H3 119.6 . .
C5 C4 C3 116.5(4) . .
C5 C4 H4 121.8 . .
C3 C4 H4 121.8 . .
N1 C5 C4 125.4(4) . .
N1 C5 Cl1 115.2(3) . .
C4 C5 Cl1 119.4(3) . .
O2 C6 N2 113.9(4) . .
O2 C6 C7 124.4(4) . .
N2 C6 C7 121.7(4) . .
C8 C7 C6 117.8(4) . .
C8 C7 H7 121.1 . .
C6 C7 H7 121.1 . .
C7 C8 C9 120.6(4) . .
C7 C8 H8 119.7 . .
C9 C8 H8 119.7 . .
C10 C9 C8 117.2(4) . .
C10 C9 H9 121.4 . .
C8 C9 H9 121.4 . .
N2 C10 C9 124.3(4) . .
N2 C10 Cl2 115.7(3) . .
C9 C10 Cl2 120.0(4) . .
O3 C11 N3 118.3(4) . .
O3 C11 C12 126.0(4) . .
N3 C11 C12 115.7(4) . .
C13 C12 C11 120.4(4) . .
C13 C12 H12 119.8 . .
C11 C12 H12 119.8 . .
C12 C13 C14 121.8(4) . .
C12 C13 H13 119.1 . .
C14 C13 H13 119.1 . .
C15 C14 C13 117.0(4) . .
C15 C14 H14 121.5 . .
C13 C14 H14 121.5 . .
C14 C15 N3 122.3(4) . .
C14 C15 Cl3 122.5(3) . .
N3 C15 Cl3 115.1(3) . .
O4 C16 N4 113.6(4) . .
O4 C16 C17 125.6(4) . .
N4 C16 C17 120.8(4) . .
O4 C16 Co2 57.6(2) . .
N4 C16 Co2 56.1(2) . .
C17 C16 Co2 173.8(3) . .
C18 C17 C16 117.5(4) . .
C18 C17 H17 121.2 . .
C16 C17 H17 121.2 . .
C17 C18 C19 122.1(4) . .
C17 C18 H18 118.9 . .
C19 C18 H18 118.9 . .
C18 C19 C20 116.8(4) . .
C18 C19 H19 121.6 . .
C20 C19 H19 121.6 . .
N4 C20 C19 123.5(4) . .
N4 C20 Cl4 115.7(3) . .
C19 C20 Cl4 120.8(4) . .
O5 C21 N5 113.1(3) . .
O5 C21 C22 125.8(4) . .
N5 C21 C22 121.1(4) . .
C23 C22 C21 118.3(4) . .
C23 C22 H22 120.9 . .
C21 C22 H22 120.9 . .
C22 C23 C24 120.8(4) . .
C22 C23 H23 119.6 . .
C24 C23 H23 119.6 . .
C25 C24 C23 117.2(4) . .
C25 C24 H24 121.4 . .
C23 C24 H24 121.4 . .
N5 C25 C24 123.6(4) . .
N5 C25 Cl5 115.9(3) . .
C24 C25 Cl5 120.5(3) . .
O6 C26 N6 113.0(4) . .
O6 C26 C27 126.8(4) . .
N6 C26 C27 120.1(4) . .
O6 C26 Co2 57.3(2) . .
N6 C26 Co2 55.8(2) . .
C27 C26 Co2 174.0(3) . .
C28 C27 C26 118.3(4) . .
C28 C27 H27 120.9 . .
C26 C27 H27 120.9 . .
C27 C28 C29 121.6(5) . .
C27 C28 H28 119.2 . .
C29 C28 H28 119.2 . .
C30 C29 C28 116.3(5) . .
C30 C29 H29 121.8 . .
C28 C29 H29 121.8 . .
N6 C30 C29 124.1(4) . .
N6 C30 Cl6 115.3(3) . .
C29 C30 Cl6 120.6(4) . .
C2S C1S H1S1 109.5 . .
C2S C1S H1S2 109.5 . .
H1S1 C1S H1S2 109.5 . .
C2S C1S H1S3 109.5 . .
H1S1 C1S H1S3 109.5 . .
H1S2 C1S H1S3 109.5 . .
C1S C2S C3S 117.2(13) . .
C1S C2S H2S1 108.0 . .
C3S C2S H2S1 108.0 . .
C1S C2S H2S2 108.0 . .
C3S C2S H2S2 108.0 . .
H2S1 C2S H2S2 107.2 . .
C4S C3S C2S 120.0(12) . .
C4S C3S H3S1 107.3 . .
C2S C3S H3S1 107.3 . .
C4S C3S H3S2 107.3 . .
C2S C3S H3S2 107.3 . .
H3S1 C3S H3S2 106.9 . .
C5S C4S C3S 117.2(11) . .
C5S C4S C5T 61.3(11) . .
C3S C4S C5T 143.9(12) . .
C5S C4S H4S1 108.0 . .
C3S C4S H4S1 108.0 . .
C5T C4S H4S1 106.1 . .
C5S C4S H4S2 108.0 . .
C3S C4S H4S2 108.0 . .
C5T C4S H4S2 49.5 . .
H4S1 C4S H4S2 107.3 . .
C4S C5S C6S 114.2(12) . .
C4S C5S H5S1 108.7 . .
C6S C5S H5S1 108.7 . .
C4S C5S H5S2 108.7 . .
C6S C5S H5S2 108.7 . .
H5S1 C5S H5S2 107.6 . .
C6S C5T C4S 93.1(15) . .
C6S C5T H5T1 113.1 . .
C4S C5T H5T1 113.1 . .
C6S C5T H5T2 113.1 . .
C4S C5T H5T2 113.1 . .
H5T1 C5T H5T2 110.5 . .
C5T C6S C5S 65.0(12) . .
C5T C6S H6S1 135.2 . .
C5S C6S H6S1 109.5 . .
C5T C6S H6S2 45.9 . .
C5S C6S H6S2 109.5 . .
H6S1 C6S H6S2 109.5 . .
C5T C6S H6S3 114.2 . .
C5S C6S H6S3 109.5 . .
H6S1 C6S H6S3 109.5 . .
H6S2 C6S H6S3 109.5 . .
C15S C7S C16S 112.9 . .
C15S C7S C9S 56.0 . .
C16S C7S C9S 126.7 . .
C15S C7S C8S 47.5 . .
C16S C7S C8S 113.8 . .
C9S C7S C8S 16.4 . .
C15S C8S C12S 100.0 . .
C15S C8S C7S 27.1 . .
C12S C8S C7S 97.5 . .
C15S C8S C11S 136.5 . .
C12S C8S C11S 54.1 . .
C7S C8S C11S 149.8 . .
C12S C9S C15S 123.2 . .
C12S C9S C7S 125.0 . .
C15S C9S C7S 31.5 . .
C12S C9S C11S 54.4 . .
C15S C9S C11S 131.1 . .
C7S C9S C11S 162.1 . .
C11S C10S C12S 69.9 . .
C10S C11S C12S 57.9 . .
C10S C11S C8S 101.0 . .
C12S C11S C8S 53.5 . .
C10S C11S C9S 87.9 . .
C12S C11S C9S 39.2 . .
C8S C11S C9S 14.5 . .
C14S C12S C9S 115.9 . .
C14S C12S C10S 120.8 . .
C9S C12S C10S 120.9 . .
C14S C12S C8S 126.9 . .
C9S C12S C8S 14.5 . .
C10S C12S C8S 112.0 . .
C14S C12S C11S 147.9 . .
C9S C12S C11S 86.5 . .
C10S C12S C11S 52.1 . .
C8S C12S C11S 72.4 . .
C7S C15S C9S 92.5 . .
C7S C15S C8S 105.4 . .
C9S C15S C8S 21.8 . .
C7S C15S C16S 37.5 . .
C9S C15S C16S 109.6 . .
C8S C15S C16S 109.4 . .
C7S C16S C15S 29.6 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 O1 2.022(3) 3_565
Co1 O2 2.050(3) .
Co1 O1 2.096(3) .
Co1 O7 2.199(2) .
Co1 N2 2.205(3) .
Co1 Cl7 2.4462(11) .
Co2 N6 2.080(3) .
Co2 N4 2.091(3) .
Co2 N5 2.107(3) .
Co2 O6 2.116(3) .
Co2 O4 2.127(3) .
Co2 O5 2.209(3) .
Co2 C26 2.513(4) .
Co2 C16 2.519(4) .
Li1 O2 1.862(7) .
Li1 O6 1.871(7) 2_665
Li1 O8 2.024(7) 2_665
Li1 Cl7 2.386(6) 2_665
Li1 Li2 3.025(9) 2_665
Li1 Li3 3.066(9) 2_665
Li1 P1 3.109(6) .
Li1 Li3 3.280(9) 3_565
Li2 O5 1.933(7) .
Li2 O3 1.954(7) .
Li2 O8 1.958(7) .
Li2 Cl8 2.345(7) .
Li2 P1 2.976(7) .
Li2 Li1 3.025(9) 3_565
Li2 Li3 3.042(9) .
Li2 Li3 3.167(9) 2_665
Li2 Li2 3.198(12) 2_665
Li2 Li2 3.198(12) 3_565
Li3 O4 1.861(7) .
Li3 O3 1.971(7) 3_565
Li3 O8 1.978(7) .
Li3 Cl7 2.364(7) 3_565
Li3 P1 2.987(6) .
Li3 Li1 3.066(9) 3_565
Li3 Li2 3.167(9) 3_565
Li3 Li1 3.280(9) 2_665
Cl1 C5 1.746(4) .
Cl2 C10 1.741(5) .
Cl3 C15 1.721(4) .
Cl4 C20 1.731(5) .
Cl5 C25 1.733(4) .
Cl6 C30 1.734(5) .
Cl7 Li3 2.364(7) 2_665
Cl7 Li1 2.386(7) 3_565
Cl8 Li2 2.345(7) 3_565
Cl8 Li2 2.345(7) 2_665
P1 O8 1.535(3) 3_565
P1 O8 1.535(3) .
P1 O8 1.535(3) 2_665
P1 O7 1.567(5) .
P1 Li2 2.976(7) 3_565
P1 Li2 2.976(7) 2_665
P1 Li3 2.987(6) 3_565
P1 Li3 2.987(6) 2_665
P1 Li1 3.109(6) 2_665
P1 Li1 3.109(6) 3_565
O1 C1 1.327(5) .
O1 Co1 2.022(3) 2_665
O2 C6 1.290(5) .
O3 C11 1.244(5) .
O3 Li3 1.971(7) 2_665
O4 C16 1.288(5) .
O5 C21 1.310(5) .
O6 C26 1.281(5) .
O6 Li1 1.871(7) 3_565
O7 Co1 2.199(2) 2_665
O7 Co1 2.199(2) 3_565
O8 Li1 2.024(7) 3_565
N1 C5 1.332(6) .
N1 C1 1.347(5) .
N2 C10 1.330(5) .
N2 C6 1.354(5) .
N3 C15 1.349(5) .
N3 C11 1.389(5) .
N4 C20 1.329(5) .
N4 C16 1.357(5) .
N5 C25 1.324(5) .
N5 C21 1.355(5) .
N6 C30 1.330(6) .
N6 C26 1.362(5) .
C1 C2 1.391(6) .
C2 C3 1.372(6) .
C2 H2 0.9500 .
C3 C4 1.389(7) .
C3 H3 0.9500 .
C4 C5 1.369(7) .
C4 H4 0.9500 .
C6 C7 1.407(6) .
C7 C8 1.369(7) .
C7 H7 0.9500 .
C8 C9 1.403(7) .
C8 H8 0.9500 .
C9 C10 1.364(6) .
C9 H9 0.9500 .
C11 C12 1.416(6) .
C12 C13 1.362(6) .
C12 H12 0.9500 .
C13 C14 1.409(6) .
C13 H13 0.9500 .
C14 C15 1.346(6) .
C14 H14 0.9500 .
C16 C17 1.405(6) .
C17 C18 1.372(7) .
C17 H17 0.9500 .
C18 C19 1.375(7) .
C18 H18 0.9500 .
C19 C20 1.377(7) .
C19 H19 0.9500 .
C21 C22 1.398(6) .
C22 C23 1.364(6) .
C22 H22 0.9500 .
C23 C24 1.394(7) .
C23 H23 0.9500 .
C24 C25 1.369(7) .
C24 H24 0.9500 .
C26 C27 1.411(6) .
C27 C28 1.368(7) .
C27 H27 0.9500 .
C28 C29 1.401(7) .
C28 H28 0.9500 .
C29 C30 1.371(7) .
C29 H29 0.9500 .
C1S C2S 1.38(2) .
C1S H1S1 0.9800 .
C1S H1S2 0.9800 .
C1S H1S3 0.9800 .
C2S C3S 1.60(2) .
C2S H2S1 0.9900 .
C2S H2S2 0.9900 .
C3S C4S 1.47(2) .
C3S H3S1 0.9900 .
C3S H3S2 0.9900 .
C4S C5S 1.365(18) .
C4S C5T 1.90(3) .
C4S H4S1 0.9900 .
C4S H4S2 0.9900 .
C5S C6S 1.64(2) .
C5S H5S1 0.9900 .
C5S H5S2 0.9900 .
C5T C6S 1.57(3) .
C5T H5T1 0.9900 .
C5T H5T2 0.9900 .
C6S H6S1 0.9800 .
C6S H6S2 0.9800 .
C6S H6S3 0.9800 .
C7S C15S 0.8208 .
C7S C16S 1.0103 .
C7S C9S 1.5691 .
C7S C8S 1.7349 .
C8S C15S 1.3264 .
C8S C12S 1.6024 .
C8S C11S 1.9017 .
C9S C12S 1.2558 .
C9S C15S 1.3026 .
C9S C11S 1.9845 .
C10S C11S 1.3580 .
C10S C12S 1.4575 .
C11S C12S 1.6159 .
C12S C14S 1.2272 .
C15S C16S 1.5298 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O5 Li2 Li3 O4 21.9(3) . .
O3 Li2 Li3 O4 -90.3(5) . .
O8 Li2 Li3 O4 -124.1(4) . .
Cl8 Li2 Li3 O4 130.6(3) . .
P1 Li2 Li3 O4 -149.7(3) . .
Li1 Li2 Li3 O4 -76.3(3) 3_565 .
Li3 Li2 Li3 O4 -119.0(3) 2_665 .
Li2 Li2 Li3 O4 -179.9(2) 2_665 .
Li2 Li2 Li3 O4 143.0(3) 3_565 .
O5 Li2 Li3 O3 -87.6(3) . 3_565
O3 Li2 Li3 O3 160.2(5) . 3_565
O8 Li2 Li3 O3 126.3(4) . 3_565
Cl8 Li2 Li3 O3 21.1(3) . 3_565
P1 Li2 Li3 O3 100.8(2) . 3_565
Li1 Li2 Li3 O3 174.1(3) 3_565 3_565
Li3 Li2 Li3 O3 131.4(3) 2_665 3_565
Li2 Li2 Li3 O3 70.5(3) 2_665 3_565
Li2 Li2 Li3 O3 33.5(2) 3_565 3_565
O5 Li2 Li3 O8 146.1(4) . .
O3 Li2 Li3 O8 33.9(4) . .
Cl8 Li2 Li3 O8 -105.2(3) . .
P1 Li2 Li3 O8 -25.54(17) . .
Li1 Li2 Li3 O8 47.8(2) 3_565 .
Li3 Li2 Li3 O8 5.1(2) 2_665 .
Li2 Li2 Li3 O8 -55.8(3) 2_665 .
Li2 Li2 Li3 O8 -92.8(3) 3_565 .
O5 Li2 Li3 Cl7 168.1(5) . 3_565
O3 Li2 Li3 Cl7 55.9(8) . 3_565
O8 Li2 Li3 Cl7 22.1(5) . 3_565
Cl8 Li2 Li3 Cl7 -83.1(5) . 3_565
P1 Li2 Li3 Cl7 -3.5(5) . 3_565
Li1 Li2 Li3 Cl7 69.9(5) 3_565 3_565
Li3 Li2 Li3 Cl7 27.2(6) 2_665 3_565
Li2 Li2 Li3 Cl7 -33.7(6) 2_665 3_565
Li2 Li2 Li3 Cl7 -70.8(5) 3_565 3_565
O5 Li2 Li3 P1 171.6(3) . .
O3 Li2 Li3 P1 59.4(4) . .
O8 Li2 Li3 P1 25.54(17) . .
Cl8 Li2 Li3 P1 -79.7(2) . .
Li1 Li2 Li3 P1 73.37(19) 3_565 .
Li3 Li2 Li3 P1 30.64(17) 2_665 .
Li2 Li2 Li3 P1 -30.23(18) 2_665 .
Li2 Li2 Li3 P1 -67.29(16) 3_565 .
O5 Li2 Li3 Li1 98.2(3) . 3_565
O3 Li2 Li3 Li1 -14.0(4) . 3_565
O8 Li2 Li3 Li1 -47.8(2) . 3_565
Cl8 Li2 Li3 Li1 -153.1(3) . 3_565
P1 Li2 Li3 Li1 -73.37(19) . 3_565
Li3 Li2 Li3 Li1 -42.7(2) 2_665 3_565
Li2 Li2 Li3 Li1 -103.6(3) 2_665 3_565
Li2 Li2 Li3 Li1 -140.7(2) 3_565 3_565
O5 Li2 Li3 Li2 -121.1(3) . 3_565
O3 Li2 Li3 Li2 126.7(5) . 3_565
O8 Li2 Li3 Li2 92.8(3) . 3_565
Cl8 Li2 Li3 Li2 -12.4(3) . 3_565
P1 Li2 Li3 Li2 67.29(16) . 3_565
Li1 Li2 Li3 Li2 140.7(2) 3_565 3_565
Li3 Li2 Li3 Li2 97.9(2) 2_665 3_565
Li2 Li2 Li3 Li2 37.06(14) 2_665 3_565
O5 Li2 Li3 Li1 -153.7(3) . 2_665
O3 Li2 Li3 Li1 94.1(5) . 2_665
O8 Li2 Li3 Li1 60.2(3) . 2_665
Cl8 Li2 Li3 Li1 -45.0(3) . 2_665
P1 Li2 Li3 Li1 34.7(2) . 2_665
Li1 Li2 Li3 Li1 108.1(3) 3_565 2_665
Li3 Li2 Li3 Li1 65.3(3) 2_665 2_665
Li2 Li2 Li3 Li1 4.5(3) 2_665 2_665
Li2 Li2 Li3 Li1 -32.6(2) 3_565 2_665
O1 Co1 Cl7 Li3 145.09(18) 3_565 2_665
O2 Co1 Cl7 Li3 -37.07(18) . 2_665
O1 Co1 Cl7 Li3 70.9(10) . 2_665
O7 Co1 Cl7 Li3 62.66(18) . 2_665
N2 Co1 Cl7 Li3 -99.79(19) . 2_665
O1 Co1 Cl7 Li1 57.04(19) 3_565 3_565
O2 Co1 Cl7 Li1 -125.12(18) . 3_565
O1 Co1 Cl7 Li1 -17.2(10) . 3_565
O7 Co1 Cl7 Li1 -25.39(18) . 3_565
N2 Co1 Cl7 Li1 172.16(19) . 3_565
O5 Li2 Cl8 Li2 107.3(4) . 3_565
O3 Li2 Cl8 Li2 -137.7(2) . 3_565
O8 Li2 Cl8 Li2 -26.8(2) . 3_565
P1 Li2 Cl8 Li2 -43.11(11) . 3_565
Li1 Li2 Cl8 Li2 -42.9(5) 3_565 3_565
Li3 Li2 Cl8 Li2 14.9(3) . 3_565
Li3 Li2 Cl8 Li2 -100.24(13) 2_665 3_565
Li2 Li2 Cl8 Li2 -86.2(2) 2_665 3_565
O5 Li2 Cl8 Li2 -166.4(4) . 2_665
O3 Li2 Cl8 Li2 -51.4(4) . 2_665
O8 Li2 Cl8 Li2 59.41(16) . 2_665
P1 Li2 Cl8 Li2 43.11(11) . 2_665
Li1 Li2 Cl8 Li2 43.3(5) 3_565 2_665
Li3 Li2 Cl8 Li2 101.08(14) . 2_665
Li3 Li2 Cl8 Li2 -14.0(3) 2_665 2_665
Li2 Li2 Cl8 Li2 86.2(2) 3_565 2_665
O5 Li2 P1 O8 -86.6(6) . 3_565
O3 Li2 P1 O8 144.0(2) . 3_565
O8 Li2 P1 O8 -108.15(18) . 3_565
Cl8 Li2 P1 O8 37.7(2) . 3_565
Li1 Li2 P1 O8 -142.23(18) 3_565 3_565
Li3 Li2 P1 O8 -71.66(19) . 3_565
Li3 Li2 P1 O8 142.79(18) 2_665 3_565
Li2 Li2 P1 O8 74.0(2) 2_665 3_565
Li2 Li2 P1 O8 1.3(2) 3_565 3_565
O5 Li2 P1 O8 21.5(4) . .
O3 Li2 P1 O8 -107.8(4) . .
Cl8 Li2 P1 O8 145.8(4) . .
Li1 Li2 P1 O8 -34.1(2) 3_565 .
Li3 Li2 P1 O8 36.5(2) . .
Li3 Li2 P1 O8 -109.1(3) 2_665 .
Li2 Li2 P1 O8 -177.8(4) 2_665 .
Li2 Li2 P1 O8 109.5(4) 3_565 .
O5 Li2 P1 O8 165.1(6) . 2_665
O3 Li2 P1 O8 35.7(2) . 2_665
O8 Li2 P1 O8 143.5(2) . 2_665
Cl8 Li2 P1 O8 -70.65(19) . 2_665
Li1 Li2 P1 O8 109.47(19) 3_565 2_665
Li3 Li2 P1 O8 -180.0(2) . 2_665
Li3 Li2 P1 O8 34.48(18) 2_665 2_665
Li2 Li2 P1 O8 -34.30(19) 2_665 2_665
Li2 Li2 P1 O8 -107.01(19) 3_565 2_665
O5 Li2 P1 O7 55.7(7) . .
O3 Li2 P1 O7 -73.6(3) . .
O8 Li2 P1 O7 34.2(4) . .
Cl8 Li2 P1 O7 180.000(2) . .
Li1 Li2 P1 O7 0.1(3) 3_565 .
Li3 Li2 P1 O7 70.7(2) . .
Li3 Li2 P1 O7 -74.9(2) 2_665 .
Li2 Li2 P1 O7 -143.64(5) 2_665 .
Li2 Li2 P1 O7 143.64(5) 3_565 .
O5 Li2 P1 Li2 -87.9(7) . 3_565
O3 Li2 P1 Li2 142.7(3) . 3_565
O8 Li2 P1 Li2 -109.5(4) . 3_565
Cl8 Li2 P1 Li2 36.36(5) . 3_565
Li1 Li2 P1 Li2 -143.5(3) 3_565 3_565
Li3 Li2 P1 Li2 -73.0(3) . 3_565
Li3 Li2 P1 Li2 141.5(2) 2_665 3_565
Li2 Li2 P1 Li2 72.71(10) 2_665 3_565
O5 Li2 P1 Li2 -160.6(6) . 2_665
O3 Li2 P1 Li2 70.0(3) . 2_665
O8 Li2 P1 Li2 177.8(4) . 2_665
Cl8 Li2 P1 Li2 -36.36(5) . 2_665
Li1 Li2 P1 Li2 143.8(3) 3_565 2_665
Li3 Li2 P1 Li2 -145.7(2) . 2_665
Li3 Li2 P1 Li2 68.8(2) 2_665 2_665
Li2 Li2 P1 Li2 -72.71(9) 3_565 2_665
O5 Li2 P1 Li3 -15.0(5) . .
O3 Li2 P1 Li3 -144.3(3) . .
O8 Li2 P1 Li3 -36.5(2) . .
Cl8 Li2 P1 Li3 109.3(2) . .
Li1 Li2 P1 Li3 -70.6(2) 3_565 .
Li3 Li2 P1 Li3 -145.6(2) 2_665 .
Li2 Li2 P1 Li3 145.7(2) 2_665 .
Li2 Li2 P1 Li3 73.0(3) 3_565 .
O5 Li2 P1 Li3 -121.7(5) . 3_565
O3 Li2 P1 Li3 109.0(3) . 3_565
O8 Li2 P1 Li3 -143.2(3) . 3_565
Cl8 Li2 P1 Li3 2.6(3) . 3_565
Li1 Li2 P1 Li3 -177.3(2) 3_565 3_565
Li3 Li2 P1 Li3 -106.70(12) . 3_565
Li3 Li2 P1 Li3 107.75(12) 2_665 3_565
Li2 Li2 P1 Li3 39.0(3) 2_665 3_565
Li2 Li2 P1 Li3 -33.7(3) 3_565 3_565
O5 Li2 P1 Li3 130.6(6) . 2_665
O3 Li2 P1 Li3 1.3(2) . 2_665
O8 Li2 P1 Li3 109.1(3) . 2_665
Cl8 Li2 P1 Li3 -105.1(2) . 2_665
Li1 Li2 P1 Li3 75.0(2) 3_565 2_665
Li3 Li2 P1 Li3 145.6(2) . 2_665
Li2 Li2 P1 Li3 -68.8(2) 2_665 2_665
Li2 Li2 P1 Li3 -141.5(2) 3_565 2_665
O5 Li2 P1 Li1 -53.8(6) . 2_665
O3 Li2 P1 Li1 176.8(2) . 2_665
O8 Li2 P1 Li1 -75.4(3) . 2_665
Cl8 Li2 P1 Li1 70.4(2) . 2_665
Li1 Li2 P1 Li1 -109.44(12) 3_565 2_665
Li3 Li2 P1 Li1 -38.9(2) . 2_665
Li3 Li2 P1 Li1 175.6(2) 2_665 2_665
Li2 Li2 P1 Li1 106.8(2) 2_665 2_665
Li2 Li2 P1 Li1 34.1(2) 3_565 2_665
O5 Li2 P1 Li1 55.6(5) . 3_565
O3 Li2 P1 Li1 -73.7(3) . 3_565
O8 Li2 P1 Li1 34.1(2) . 3_565
Cl8 Li2 P1 Li1 179.9(3) . 3_565
Li3 Li2 P1 Li1 70.6(2) . 3_565
Li3 Li2 P1 Li1 -75.0(2) 2_665 3_565
Li2 Li2 P1 Li1 -143.8(3) 2_665 3_565
Li2 Li2 P1 Li1 143.5(3) 3_565 3_565
O4 Li3 P1 O8 161.5(5) . 3_565
O3 Li3 P1 O8 33.3(2) 3_565 3_565
O8 Li3 P1 O8 144.8(3) . 3_565
Cl7 Li3 P1 O8 -73.23(18) 3_565 3_565
Li2 Li3 P1 O8 108.8(2) . 3_565
Li1 Li3 P1 O8 178.1(2) 3_565 3_565
Li2 Li3 P1 O8 34.50(18) 3_565 3_565
Li1 Li3 P1 O8 -32.21(18) 2_665 3_565
O4 Li3 P1 O8 16.7(4) . .
O3 Li3 P1 O8 -111.6(4) 3_565 .
Cl7 Li3 P1 O8 141.9(4) 3_565 .
Li2 Li3 P1 O8 -36.1(3) . .
Li1 Li3 P1 O8 33.3(2) 3_565 .
Li2 Li3 P1 O8 -110.3(3) 3_565 .
Li1 Li3 P1 O8 -177.1(3) 2_665 .
O4 Li3 P1 O8 52.8(6) . 2_665
O3 Li3 P1 O8 -75.5(3) 3_565 2_665
O8 Li3 P1 O8 36.1(4) . 2_665
Cl7 Li3 P1 O8 178.04(18) 3_565 2_665
Li2 Li3 P1 O8 0.1(3) . 2_665
Li1 Li3 P1 O8 69.4(3) 3_565 2_665
Li2 Li3 P1 O8 -74.2(3) 3_565 2_665
Li1 Li3 P1 O8 -140.9(3) 2_665 2_665
O4 Li3 P1 O7 -90.6(5) . .
O3 Li3 P1 O7 141.1(2) 3_565 .
O8 Li3 P1 O7 -107.3(2) . .
Cl7 Li3 P1 O7 34.64(18) 3_565 .
Li2 Li3 P1 O7 -143.35(15) . .
Li1 Li3 P1 O7 -74.03(17) 3_565 .
Li2 Li3 P1 O7 142.36(14) 3_565 .
Li1 Li3 P1 O7 75.66(16) 2_665 .
O4 Li3 P1 Li2 127.0(6) . 3_565
O3 Li3 P1 Li2 -1.2(2) 3_565 3_565
O8 Li3 P1 Li2 110.3(3) . 3_565
Cl7 Li3 P1 Li2 -107.7(2) 3_565 3_565
Li2 Li3 P1 Li2 74.3(3) . 3_565
Li1 Li3 P1 Li2 143.6(2) 3_565 3_565
Li1 Li3 P1 Li2 -66.7(2) 2_665 3_565
O4 Li3 P1 Li2 52.7(5) . .
O3 Li3 P1 Li2 -75.5(3) 3_565 .
O8 Li3 P1 Li2 36.1(3) . .
Cl7 Li3 P1 Li2 178.0(3) 3_565 .
Li1 Li3 P1 Li2 69.3(2) 3_565 .
Li2 Li3 P1 Li2 -74.3(3) 3_565 .
Li1 Li3 P1 Li2 -141.0(2) 2_665 .
O4 Li3 P1 Li2 87.7(5) . 2_665
O3 Li3 P1 Li2 -40.5(3) 3_565 2_665
O8 Li3 P1 Li2 71.1(3) . 2_665
Cl7 Li3 P1 Li2 -147.02(18) 3_565 2_665
Li2 Li3 P1 Li2 35.0(3) . 2_665
Li1 Li3 P1 Li2 104.3(2) 3_565 2_665
Li2 Li3 P1 Li2 -39.3(3) 3_565 2_665
Li1 Li3 P1 Li2 -106.0(2) 2_665 2_665
O4 Li3 P1 Li3 160.6(3) . 3_565
O3 Li3 P1 Li3 32.4(4) 3_565 3_565
O8 Li3 P1 Li3 143.95(19) . 3_565
Cl7 Li3 P1 Li3 -74.1(3) 3_565 3_565
Li2 Li3 P1 Li3 107.9(2) . 3_565
Li1 Li3 P1 Li3 177.2(2) 3_565 3_565
Li2 Li3 P1 Li3 33.6(3) 3_565 3_565
Li1 Li3 P1 Li3 -33.1(3) 2_665 3_565
O4 Li3 P1 Li3 18.1(7) . 2_665
O3 Li3 P1 Li3 -110.11(17) 3_565 2_665
O8 Li3 P1 Li3 1.5(4) . 2_665
Cl7 Li3 P1 Li3 143.40(19) 3_565 2_665
Li2 Li3 P1 Li3 -34.6(3) . 2_665
Li1 Li3 P1 Li3 34.7(3) 3_565 2_665
Li2 Li3 P1 Li3 -108.9(2) 3_565 2_665
Li1 Li3 P1 Li3 -175.6(2) 2_665 2_665
O4 Li3 P1 Li1 -166.3(6) . 2_665
O3 Li3 P1 Li1 65.5(2) 3_565 2_665
O8 Li3 P1 Li1 177.1(3) . 2_665
Cl7 Li3 P1 Li1 -41.02(18) 3_565 2_665
Li2 Li3 P1 Li1 141.0(2) . 2_665
Li1 Li3 P1 Li1 -149.7(3) 3_565 2_665
Li2 Li3 P1 Li1 66.7(2) 3_565 2_665
O4 Li3 P1 Li1 -16.6(5) . 3_565
O3 Li3 P1 Li1 -144.8(3) 3_565 3_565
O8 Li3 P1 Li1 -33.3(2) . 3_565
Cl7 Li3 P1 Li1 108.7(2) 3_565 3_565
Li2 Li3 P1 Li1 -69.3(2) . 3_565
Li2 Li3 P1 Li1 -143.6(2) 3_565 3_565
Li1 Li3 P1 Li1 149.7(3) 2_665 3_565
O1 Co1 O1 C1 109.1(3) 3_565 .
O2 Co1 O1 C1 -68.3(3) . .
O7 Co1 O1 C1 -168.0(4) . .
N2 Co1 O1 C1 -5.6(3) . .
Cl7 Co1 O1 C1 -176.3(8) . .
O1 Co1 O1 Co1 -87.44(14) 3_565 2_665
O2 Co1 O1 Co1 95.21(13) . 2_665
O7 Co1 O1 Co1 -4.54(11) . 2_665
N2 Co1 O1 Co1 157.84(14) . 2_665
Cl7 Co1 O1 Co1 -12.9(10) . 2_665
O6 Li1 O2 C6 29.7(8) 2_665 .
O8 Li1 O2 C6 153.0(5) 2_665 .
Cl7 Li1 O2 C6 -99.3(6) 2_665 .
Li2 Li1 O2 C6 128.8(6) 2_665 .
Li3 Li1 O2 C6 123.2(6) 2_665 .
P1 Li1 O2 C6 177.7(5) . .
Li3 Li1 O2 C6 -143.3(5) 3_565 .
O6 Li1 O2 Co1 -169.0(3) 2_665 .
O8 Li1 O2 Co1 -45.7(3) 2_665 .
Cl7 Li1 O2 Co1 61.9(3) 2_665 .
Li2 Li1 O2 Co1 -70.0(4) 2_665 .
Li3 Li1 O2 Co1 -75.5(2) 2_665 .
P1 Li1 O2 Co1 -21.0(3) . .
Li3 Li1 O2 Co1 18.0(6) 3_565 .
O1 Co1 O2 C6 65.6(11) 3_565 .
O1 Co1 O2 C6 91.4(2) . .
O7 Co1 O2 C6 171.7(2) . .
N2 Co1 O2 C6 -0.9(2) . .
Cl7 Co1 O2 C6 -93.7(2) . .
O1 Co1 O2 Li1 -104.0(11) 3_565 .
O1 Co1 O2 Li1 -78.2(3) . .
O7 Co1 O2 Li1 2.1(3) . .
N2 Co1 O2 Li1 -170.5(3) . .
Cl7 Co1 O2 Li1 96.8(3) . .
O5 Li2 O3 C11 23.3(5) . .
O8 Li2 O3 C11 149.4(3) . .
Cl8 Li2 O3 C11 -92.9(4) . .
P1 Li2 O3 C11 176.1(3) . .
Li1 Li2 O3 C11 115.6(4) 3_565 .
Li3 Li2 O3 C11 128.0(5) . .
Li3 Li2 O3 C11 177.9(5) 2_665 .
Li2 Li2 O3 C11 -129.0(4) 2_665 .
Li2 Li2 O3 C11 -137.3(3) 3_565 .
O5 Li2 O3 Li3 -154.6(3) . 2_665
O8 Li2 O3 Li3 -28.6(4) . 2_665
Cl8 Li2 O3 Li3 89.2(3) . 2_665
P1 Li2 O3 Li3 -1.8(3) . 2_665
Li1 Li2 O3 Li3 -62.3(3) 3_565 2_665
Li3 Li2 O3 Li3 -49.9(6) . 2_665
Li2 Li2 O3 Li3 53.1(2) 2_665 2_665
Li2 Li2 O3 Li3 44.8(4) 3_565 2_665
O3 Li3 O4 C16 -123.1(5) 3_565 .
O8 Li3 O4 C16 121.7(5) . .
Cl7 Li3 O4 C16 -2.6(7) 3_565 .
P1 Li3 O4 C16 113.3(6) . .
Li2 Li3 O4 C16 156.5(4) . .
Li1 Li3 O4 C16 98.5(5) 3_565 .
Li2 Li3 O4 C16 -151.9(5) 3_565 .
Li1 Li3 O4 C16 -34.4(12) 2_665 .
O3 Li3 O4 Co2 90.6(3) 3_565 .
O8 Li3 O4 Co2 -24.6(5) . .
Cl7 Li3 O4 Co2 -148.8(2) 3_565 .
P1 Li3 O4 Co2 -32.9(6) . .
Li2 Li3 O4 Co2 10.3(3) . .
Li1 Li3 O4 Co2 -47.7(3) 3_565 .
Li2 Li3 O4 Co2 61.9(5) 3_565 .
Li1 Li3 O4 Co2 179.4(7) 2_665 .
N6 Co2 O4 C16 -78.1(4) . .
N4 Co2 O4 C16 -2.6(2) . .
N5 Co2 O4 C16 104.5(2) . .
O6 Co2 O4 C16 -103.7(2) . .
O5 Co2 O4 C16 166.4(2) . .
C26 Co2 O4 C16 -99.0(3) . .
N6 Co2 O4 Li3 80.9(5) . .
N4 Co2 O4 Li3 156.3(3) . .
N5 Co2 O4 Li3 -96.5(3) . .
O6 Co2 O4 Li3 55.2(3) . .
O5 Co2 O4 Li3 -34.7(3) . .
C26 Co2 O4 Li3 60.0(3) . .
C16 Co2 O4 Li3 158.9(4) . .
O3 Li2 O5 C21 -150.2(4) . .
O8 Li2 O5 C21 94.8(5) . .
Cl8 Li2 O5 C21 -35.6(5) . .
P1 Li2 O5 C21 83.6(7) . .
Li1 Li2 O5 C21 130.9(4) 3_565 .
Li3 Li2 O5 C21 70.7(4) . .
Li3 Li2 O5 C21 -172.7(4) 2_665 .
Li2 Li2 O5 C21 -58.0(10) 2_665 .
Li2 Li2 O5 C21 14.9(5) 3_565 .
O3 Li2 O5 Co2 91.9(3) . .
O8 Li2 O5 Co2 -23.2(5) . .
Cl8 Li2 O5 Co2 -153.59(19) . .
P1 Li2 O5 Co2 -34.4(6) . .
Li1 Li2 O5 Co2 12.9(3) 3_565 .
Li3 Li2 O5 Co2 -47.2(3) . .
Li3 Li2 O5 Co2 69.3(5) 2_665 .
Li2 Li2 O5 Co2 -176.0(7) 2_665 .
Li2 Li2 O5 Co2 -103.06(17) 3_565 .
N6 Co2 O5 C21 115.6(2) . .
N4 Co2 O5 C21 -59.9(4) . .
N5 Co2 O5 C21 3.9(2) . .
O6 Co2 O5 C21 178.8(2) . .
O4 Co2 O5 C21 -83.2(2) . .
C26 Co2 O5 C21 148.3(2) . .
C16 Co2 O5 C21 -74.9(2) . .
N6 Co2 O5 Li2 -103.9(3) . .
N4 Co2 O5 Li2 80.5(4) . .
N5 Co2 O5 Li2 144.4(3) . .
O6 Co2 O5 Li2 -40.7(3) . .
O4 Co2 O5 Li2 57.3(3) . .
C26 Co2 O5 Li2 -71.3(3) . .
C16 Co2 O5 Li2 65.6(3) . .
N6 Co2 O6 C26 2.5(2) . .
N4 Co2 O6 C26 108.3(2) . .
N5 Co2 O6 C26 -84.9(3) . .
O4 Co2 O6 C26 172.6(2) . .
O5 Co2 O6 C26 -94.2(2) . .
C16 Co2 O6 C26 141.9(2) . .
N6 Co2 O6 Li1 170.4(3) . 3_565
N4 Co2 O6 Li1 -83.9(3) . 3_565
N5 Co2 O6 Li1 83.0(4) . 3_565
O4 Co2 O6 Li1 -19.5(3) . 3_565
O5 Co2 O6 Li1 73.7(3) . 3_565
C26 Co2 O6 Li1 167.9(4) . 3_565
C16 Co2 O6 Li1 -50.3(3) . 3_565
O8 P1 O7 Co1 -30.43(10) 3_565 2_665
O8 P1 O7 Co1 -150.43(10) . 2_665
O8 P1 O7 Co1 89.57(10) 2_665 2_665
Li2 P1 O7 Co1 -51.0(2) 3_565 2_665
Li2 P1 O7 Co1 -171.0(2) . 2_665
Li2 P1 O7 Co1 69.0(2) 2_665 2_665
Li3 P1 O7 Co1 -113.37(13) . 2_665
Li3 P1 O7 Co1 6.63(13) 3_565 2_665
Li3 P1 O7 Co1 126.63(13) 2_665 2_665
Li1 P1 O7 Co1 -50.89(12) 2_665 2_665
Li1 P1 O7 Co1 -170.89(12) 3_565 2_665
O8 P1 O7 Co1 89.57(10) 3_565 3_565
O8 P1 O7 Co1 -30.43(10) . 3_565
O8 P1 O7 Co1 -150.43(10) 2_665 3_565
Li2 P1 O7 Co1 69.0(2) 3_565 3_565
Li2 P1 O7 Co1 -51.0(2) . 3_565
Li2 P1 O7 Co1 -171.0(2) 2_665 3_565
Li3 P1 O7 Co1 6.63(13) . 3_565
Li3 P1 O7 Co1 126.63(13) 3_565 3_565
Li3 P1 O7 Co1 -113.37(13) 2_665 3_565
Li1 P1 O7 Co1 69.11(12) 2_665 3_565
Li1 P1 O7 Co1 -50.89(12) 3_565 3_565
O8 P1 O7 Co1 -150.43(10) 3_565 .
O8 P1 O7 Co1 89.57(10) . .
O8 P1 O7 Co1 -30.43(10) 2_665 .
Li2 P1 O7 Co1 -171.0(2) 3_565 .
Li2 P1 O7 Co1 69.0(2) . .
Li2 P1 O7 Co1 -51.0(2) 2_665 .
Li3 P1 O7 Co1 126.63(13) . .
Li3 P1 O7 Co1 -113.37(13) 3_565 .
Li3 P1 O7 Co1 6.63(13) 2_665 .
Li1 P1 O7 Co1 -170.89(12) 2_665 .
Li1 P1 O7 Co1 69.11(12) 3_565 .
O1 Co1 O7 P1 -136.99(8) 3_565 .
O2 Co1 O7 P1 48.91(8) . .
O1 Co1 O7 P1 136.86(8) . .
N2 Co1 O7 P1 69.3(4) . .
Cl7 Co1 O7 P1 -43.90(3) . .
O1 Co1 O7 Co1 90.23(12) 3_565 2_665
O2 Co1 O7 Co1 -83.87(12) . 2_665
O1 Co1 O7 Co1 4.08(10) . 2_665
N2 Co1 O7 Co1 -63.5(4) . 2_665
Cl7 Co1 O7 Co1 -176.69(8) . 2_665
O1 Co1 O7 Co1 -4.21(11) 3_565 3_565
O2 Co1 O7 Co1 -178.31(10) . 3_565
O1 Co1 O7 Co1 -90.36(12) . 3_565
N2 Co1 O7 Co1 -157.9(3) . 3_565
Cl7 Co1 O7 Co1 88.88(9) . 3_565
O8 P1 O8 Li2 81.8(3) 3_565 .
O8 P1 O8 Li2 -38.5(3) 2_665 .
O7 P1 O8 Li2 -158.3(2) . .
Li2 P1 O8 Li2 60.0(4) 3_565 .
Li2 P1 O8 Li2 -2.0(3) 2_665 .
Li3 P1 O8 Li2 118.8(4) . .
Li3 P1 O8 Li2 60.0(4) 3_565 .
Li3 P1 O8 Li2 -59.8(3) 2_665 .
Li1 P1 O8 Li2 116.1(3) 2_665 .
Li1 P1 O8 Li2 -119.9(4) 3_565 .
O8 P1 O8 Li3 -37.0(3) 3_565 .
O8 P1 O8 Li3 -157.3(2) 2_665 .
O7 P1 O8 Li3 82.9(3) . .
Li2 P1 O8 Li3 -58.8(3) 3_565 .
Li2 P1 O8 Li3 -118.8(4) . .
Li2 P1 O8 Li3 -120.8(3) 2_665 .
Li3 P1 O8 Li3 -58.9(3) 3_565 .
Li3 P1 O8 Li3 -178.7(4) 2_665 .
Li1 P1 O8 Li3 -2.7(3) 2_665 .
Li1 P1 O8 Li3 121.2(4) 3_565 .
O8 P1 O8 Li1 -158.2(3) 3_565 3_565
O8 P1 O8 Li1 81.5(3) 2_665 3_565
O7 P1 O8 Li1 -38.4(3) . 3_565
Li2 P1 O8 Li1 180.0(3) 3_565 3_565
Li2 P1 O8 Li1 119.9(4) . 3_565
Li2 P1 O8 Li1 117.9(3) 2_665 3_565
Li3 P1 O8 Li1 -121.2(4) . 3_565
Li3 P1 O8 Li1 179.9(3) 3_565 3_565
Li3 P1 O8 Li1 60.1(3) 2_665 3_565
Li1 P1 O8 Li1 -124.0(3) 2_665 3_565
O5 Li2 O8 P1 -166.3(3) . .
O3 Li2 O8 P1 76.1(3) . .
Cl8 Li2 O8 P1 -37.4(4) . .
Li1 Li2 O8 P1 131.3(3) 3_565 .
Li3 Li2 O8 P1 -126.5(3) . .
Li3 Li2 O8 P1 58.6(2) 2_665 .
Li2 Li2 O8 P1 1.8(3) 2_665 .
Li2 Li2 O8 P1 -58.0(3) 3_565 .
O5 Li2 O8 Li3 -39.7(4) . .
O3 Li2 O8 Li3 -157.3(3) . .
Cl8 Li2 O8 Li3 89.2(3) . .
P1 Li2 O8 Li3 126.5(3) . .
Li1 Li2 O8 Li3 -102.1(3) 3_565 .
Li3 Li2 O8 Li3 -174.9(2) 2_665 .
Li2 Li2 O8 Li3 128.4(3) 2_665 .
Li2 Li2 O8 Li3 68.6(3) 3_565 .
O5 Li2 O8 Li1 62.4(4) . 3_565
O3 Li2 O8 Li1 -55.2(3) . 3_565
Cl8 Li2 O8 Li1 -168.7(3) . 3_565
P1 Li2 O8 Li1 -131.3(3) . 3_565
Li3 Li2 O8 Li1 102.1(3) . 3_565
Li3 Li2 O8 Li1 -72.8(2) 2_665 3_565
Li2 Li2 O8 Li1 -129.5(3) 2_665 3_565
Li2 Li2 O8 Li1 170.7(3) 3_565 3_565
O4 Li3 O8 P1 -168.5(3) . .
O3 Li3 O8 P1 72.3(3) 3_565 .
Cl7 Li3 O8 P1 -40.0(4) 3_565 .
Li2 Li3 O8 P1 126.8(3) . .
Li1 Li3 O8 P1 -132.0(3) 3_565 .
Li2 Li3 O8 P1 57.4(2) 3_565 .
Li1 Li3 O8 P1 2.5(3) 2_665 .
O4 Li3 O8 Li2 64.6(4) . .
O3 Li3 O8 Li2 -54.5(4) 3_565 .
Cl7 Li3 O8 Li2 -166.8(3) 3_565 .
P1 Li3 O8 Li2 -126.8(3) . .
Li1 Li3 O8 Li2 101.2(3) 3_565 .
Li2 Li3 O8 Li2 -69.4(3) 3_565 .
Li1 Li3 O8 Li2 -124.3(3) 2_665 .
O4 Li3 O8 Li1 -36.6(4) . 3_565
O3 Li3 O8 Li1 -155.7(3) 3_565 3_565
Cl7 Li3 O8 Li1 92.0(3) 3_565 3_565
P1 Li3 O8 Li1 132.0(3) . 3_565
Li2 Li3 O8 Li1 -101.2(3) . 3_565
Li2 Li3 O8 Li1 -170.6(3) 3_565 3_565
Li1 Li3 O8 Li1 134.5(3) 2_665 3_565
O1 Co1 N2 C10 5.6(7) 3_565 .
O2 Co1 N2 C10 179.4(7) . .
O1 Co1 N2 C10 90.9(7) . .
O7 Co1 N2 C10 156.7(6) . .
Cl7 Co1 N2 C10 -90.0(7) . .
O1 Co1 N2 C6 -173.0(2) 3_565 .
O2 Co1 N2 C6 0.9(2) . .
O1 Co1 N2 C6 -87.7(2) . .
O7 Co1 N2 C6 -21.9(5) . .
Cl7 Co1 N2 C6 91.4(2) . .
N6 Co2 N4 C20 -25.7(6) . .
N5 Co2 N4 C20 94.6(6) . .
O6 Co2 N4 C20 -92.0(6) . .
O4 Co2 N4 C20 175.7(6) . .
O5 Co2 N4 C20 149.6(5) . .
C26 Co2 N4 C20 -60.8(6) . .
C16 Co2 N4 C20 173.3(7) . .
N6 Co2 N4 C16 161.0(2) . .
N5 Co2 N4 C16 -78.7(2) . .
O6 Co2 N4 C16 94.7(2) . .
O4 Co2 N4 C16 2.5(2) . .
O5 Co2 N4 C16 -23.7(4) . .
C26 Co2 N4 C16 125.9(2) . .
N6 Co2 N5 C25 102.5(5) . .
N4 Co2 N5 C25 -16.5(6) . .
O6 Co2 N5 C25 176.7(5) . .
O4 Co2 N5 C25 -78.5(5) . .
O5 Co2 N5 C25 -172.8(6) . .
C26 Co2 N5 C25 128.7(5) . .
C16 Co2 N5 C25 -48.7(6) . .
N6 Co2 N5 C21 -88.5(3) . .
N4 Co2 N5 C21 152.5(2) . .
O6 Co2 N5 C21 -14.3(4) . .
O4 Co2 N5 C21 90.5(2) . .
O5 Co2 N5 C21 -3.8(2) . .
C26 Co2 N5 C21 -62.3(3) . .
C16 Co2 N5 C21 120.3(2) . .
N4 Co2 N6 C30 87.3(6) . .
N5 Co2 N6 C30 -28.6(7) . .
O6 Co2 N6 C30 -177.1(7) . .
O4 Co2 N6 C30 154.2(5) . .
O5 Co2 N6 C30 -90.6(6) . .
C26 Co2 N6 C30 -174.7(8) . .
C16 Co2 N6 C30 103.2(6) . .
N4 Co2 N6 C26 -97.9(2) . .
N5 Co2 N6 C26 146.1(2) . .
O6 Co2 N6 C26 -2.4(2) . .
O4 Co2 N6 C26 -31.1(5) . .
O5 Co2 N6 C26 84.1(2) . .
C16 Co2 N6 C26 -82.1(3) . .
Co1 O1 C1 N1 98.8(4) 2_665 .
Co1 O1 C1 N1 -100.7(4) . .
Co1 O1 C1 C2 -80.6(5) 2_665 .
Co1 O1 C1 C2 79.9(5) . .
C5 N1 C1 O1 -177.5(3) . .
C5 N1 C1 C2 2.0(6) . .
O1 C1 C2 C3 176.9(4) . .
N1 C1 C2 C3 -2.4(6) . .
C1 C2 C3 C4 1.1(7) . .
C2 C3 C4 C5 0.4(7) . .
C1 N1 C5 C4 -0.2(6) . .
C1 N1 C5 Cl1 179.4(3) . .
C3 C4 C5 N1 -0.9(7) . .
C3 C4 C5 Cl1 179.5(3) . .
Li1 O2 C6 N2 164.6(5) . .
Co1 O2 C6 N2 1.4(4) . .
Li1 O2 C6 C7 -14.4(8) . .
Co1 O2 C6 C7 -177.6(4) . .
C10 N2 C6 O2 179.4(4) . .
Co1 N2 C6 O2 -1.3(3) . .
C10 N2 C6 C7 -1.6(6) . .
Co1 N2 C6 C7 177.7(4) . .
O2 C6 C7 C8 -178.7(4) . .
N2 C6 C7 C8 2.3(7) . .
C6 C7 C8 C9 -1.0(8) . .
C7 C8 C9 C10 -1.0(8) . .
C6 N2 C10 C9 -0.6(7) . .
Co1 N2 C10 C9 -179.0(5) . .
C6 N2 C10 Cl2 179.5(3) . .
Co1 N2 C10 Cl2 1.1(9) . .
C8 C9 C10 N2 1.9(8) . .
C8 C9 C10 Cl2 -178.2(4) . .
Li2 O3 C11 N3 -5.7(6) . .
Li3 O3 C11 N3 171.8(4) 2_665 .
Li2 O3 C11 C12 174.2(4) . .
Li3 O3 C11 C12 -8.3(6) 2_665 .
C15 N3 C11 O3 -179.6(4) . .
C15 N3 C11 C12 0.5(6) . .
O3 C11 C12 C13 179.6(4) . .
N3 C11 C12 C13 -0.4(6) . .
C11 C12 C13 C14 -0.4(7) . .
C12 C13 C14 C15 1.1(7) . .
C13 C14 C15 N3 -1.1(7) . .
C13 C14 C15 Cl3 179.8(4) . .
C11 N3 C15 C14 0.3(7) . .
C11 N3 C15 Cl3 179.4(3) . .
Li3 O4 C16 N4 -148.4(4) . .
Co2 O4 C16 N4 3.9(3) . .
Li3 O4 C16 C17 34.0(7) . .
Co2 O4 C16 C17 -173.6(4) . .
Li3 O4 C16 Co2 -152.3(5) . .
C20 N4 C16 O4 -180.0(4) . .
Co2 N4 C16 O4 -4.0(3) . .
C20 N4 C16 C17 -2.3(6) . .
Co2 N4 C16 C17 173.7(4) . .
C20 N4 C16 Co2 -176.0(4) . .
N6 Co2 C16 O4 147.3(2) . .
N4 Co2 C16 O4 175.7(4) . .
N5 Co2 C16 O4 -76.9(2) . .
O6 Co2 C16 O4 82.3(2) . .
O5 Co2 C16 O4 -16.3(3) . .
C26 Co2 C16 O4 105.3(2) . .
N6 Co2 C16 N4 -28.4(3) . .
N5 Co2 C16 N4 107.4(2) . .
O6 Co2 C16 N4 -93.4(2) . .
O4 Co2 C16 N4 -175.7(4) . .
O5 Co2 C16 N4 168.0(2) . .
C26 Co2 C16 N4 -70.4(3) . .
N6 Co2 C16 C17 -90(3) . .
N4 Co2 C16 C17 -61(3) . .
N5 Co2 C16 C17 46(3) . .
O6 Co2 C16 C17 -155(3) . .
O4 Co2 C16 C17 123(3) . .
O5 Co2 C16 C17 107(3) . .
C26 Co2 C16 C17 -132(3) . .
O4 C16 C17 C18 178.9(4) . .
N4 C16 C17 C18 1.6(7) . .
Co2 C16 C17 C18 60(3) . .
C16 C17 C18 C19 0.1(7) . .
C17 C18 C19 C20 -1.0(8) . .
C16 N4 C20 C19 1.5(6) . .
Co2 N4 C20 C19 -170.8(4) . .
C16 N4 C20 Cl4 -179.4(3) . .
Co2 N4 C20 Cl4 8.4(8) . .
C18 C19 C20 N4 0.2(7) . .
C18 C19 C20 Cl4 -178.9(4) . .
Li2 O5 C21 N5 -132.7(4) . .
Co2 O5 C21 N5 -5.8(3) . .
Li2 O5 C21 C22 45.2(6) . .
Co2 O5 C21 C22 172.1(4) . .
C25 N5 C21 O5 179.2(4) . .
Co2 N5 C21 O5 6.1(3) . .
C25 N5 C21 C22 1.1(6) . .
Co2 N5 C21 C22 -171.9(3) . .
O5 C21 C22 C23 -179.6(4) . .
N5 C21 C22 C23 -1.8(6) . .
C21 C22 C23 C24 0.7(7) . .
C22 C23 C24 C25 1.1(7) . .
C21 N5 C25 C24 0.8(7) . .
Co2 N5 C25 C24 168.2(4) . .
C21 N5 C25 Cl5 -178.1(3) . .
Co2 N5 C25 Cl5 -10.7(7) . .
C23 C24 C25 N5 -1.9(7) . .
C23 C24 C25 Cl5 176.9(4) . .
Li1 O6 C26 N6 -161.4(6) 3_565 .
Co2 O6 C26 N6 -3.8(3) . .
Li1 O6 C26 C27 17.0(9) 3_565 .
Co2 O6 C26 C27 174.7(4) . .
Li1 O6 C26 Co2 -157.6(7) 3_565 .
C30 N6 C26 O6 -179.3(4) . .
Co2 N6 C26 O6 3.8(3) . .
C30 N6 C26 C27 2.1(6) . .
Co2 N6 C26 C27 -174.7(4) . .
C30 N6 C26 Co2 176.9(4) . .
N6 Co2 C26 O6 -175.8(4) . .
N4 Co2 C26 O6 -81.2(2) . .
N5 Co2 C26 O6 135.0(2) . .
O4 Co2 C26 O6 -9.3(3) . .
O5 Co2 C26 O6 86.1(2) . .
C16 Co2 C26 O6 -48.3(3) . .
N4 Co2 C26 N6 94.6(2) . .
N5 Co2 C26 N6 -49.2(3) . .
O6 Co2 C26 N6 175.8(4) . .
O4 Co2 C26 N6 166.5(2) . .
O5 Co2 C26 N6 -98.1(2) . .
C16 Co2 C26 N6 127.5(2) . .
N6 Co2 C26 C27 49(3) . .
N4 Co2 C26 C27 144(3) . .
N5 Co2 C26 C27 0(3) . .
O6 Co2 C26 C27 -135(3) . .
O4 Co2 C26 C27 -144(3) . .
O5 Co2 C26 C27 -49(3) . .
C16 Co2 C26 C27 177(3) . .
O6 C26 C27 C28 -178.7(5) . .
N6 C26 C27 C28 -0.4(7) . .
Co2 C26 C27 C28 -47(3) . .
C26 C27 C28 C29 -0.8(9) . .
C27 C28 C29 C30 0.2(9) . .
C26 N6 C30 C29 -2.9(8) . .
Co2 N6 C30 C29 171.0(5) . .
C26 N6 C30 Cl6 178.5(3) . .
Co2 N6 C30 Cl6 -7.6(8) . .
C28 C29 C30 N6 1.7(9) . .
C28 C29 C30 Cl6 -179.8(5) . .
C1S C2S C3S C4S -177.8(14) . .
C2S C3S C4S C5S -175.2(12) . .
C2S C3S C4S C5T 107(2) . .
C3S C4S C5S C6S -179.0(10) . .
C5T C4S C5S C6S -40.0(12) . .
C5S C4S C5T C6S 38.0(12) . .
C3S C4S C5T C6S 135.6(19) . .
C4S C5T C6S C5S -29.6(9) . .
C4S C5S C6S C5T 48.9(14) . .
C16S C7S C8S C15S -99.9 . .
C9S C7S C8S C15S 115.6 . .
C15S C7S C8S C12S -97.4 . .
C16S C7S C8S C12S 162.7 . .
C9S C7S C8S C12S 18.2 . .
C15S C7S C8S C11S -79.0 . .
C16S C7S C8S C11S -178.9 . .
C9S C7S C8S C11S 36.6 . .
C15S C7S C9S C12S -97.8 . .
C16S C7S C9S C12S 167.4 . .
C8S C7S C9S C12S -151.2 . .
C16S C7S C9S C15S -94.8 . .
C8S C7S C9S C15S -53.3 . .
C15S C7S C9S C11S -16.1 . .
C16S C7S C9S C11S -110.9 . .
C8S C7S C9S C11S -69.4 . .
C12S C10S C11S C8S 33.1 . .
C12S C10S C11S C9S 26.8 . .
C15S C8S C11S C10S -98.4 . .
C12S C8S C11S C10S -35.2 . .
C7S C8S C11S C10S -57.9 . .
C15S C8S C11S C12S -63.3 . .
C7S C8S C11S C12S -22.7 . .
C15S C8S C11S C9S -72.5 . .
C12S C8S C11S C9S -9.3 . .
C7S C8S C11S C9S -31.9 . .
C12S C9S C11S C10S -37.3 . .
C15S C9S C11S C10S -142.9 . .
C7S C9S C11S C10S -131.8 . .
C15S C9S C11S C12S -105.6 . .
C7S C9S C11S C12S -94.5 . .
C12S C9S C11S C8S 168.2 . .
C15S C9S C11S C8S 62.6 . .
C7S C9S C11S C8S 73.7 . .
C15S C9S C12S C14S -36.3 . .
C7S C9S C12S C14S 2.0 . .
C11S C9S C12S C14S -156.1 . .
C15S C9S C12S C10S 160.9 . .
C7S C9S C12S C10S -160.9 . .
C11S C9S C12S C10S 41.1 . .
C15S C9S C12S C8S 105.7 . .
C7S C9S C12S C8S 144.0 . .
C11S C9S C12S C8S -14.1 . .
C15S C9S C12S C11S 119.8 . .
C7S C9S C12S C11S 158.1 . .
C11S C10S C12S C14S 141.8 . .
C11S C10S C12S C9S -56.2 . .
C11S C10S C12S C8S -43.4 . .
C15S C8S C12S C14S -9.6 . .
C7S C8S C12S C14S 17.8 . .
C11S C8S C12S C14S -150.9 . .
C15S C8S C12S C9S -53.4 . .
C7S C8S C12S C9S -26.1 . .
C11S C8S C12S C9S 165.2 . .
C15S C8S C12S C10S 176.0 . .
C7S C8S C12S C10S -156.6 . .
C11S C8S C12S C10S 34.7 . .
C15S C8S C12S C11S 141.3 . .
C7S C8S C12S C11S 168.7 . .
C10S C11S C12S C14S -88.9 . .
C8S C11S C12S C14S 133.0 . .
C9S C11S C12S C14S 136.6 . .
C10S C11S C12S C9S 134.4 . .
C8S C11S C12S C9S -3.7 . .
C8S C11S C12S C10S -138.1 . .
C9S C11S C12S C10S -134.4 . .
C10S C11S C12S C8S 138.1 . .
C9S C11S C12S C8S 3.7 . .
C16S C7S C15S C9S 119.8 . .
C8S C7S C15S C9S 17.8 . .
C16S C7S C15S C8S 102.0 . .
C9S C7S C15S C8S -17.8 . .
C9S C7S C15S C16S -119.8 . .
C8S C7S C15S C16S -102.0 . .
C12S C9S C15S C7S 104.2 . .
C11S C9S C15S C7S 173.5 . .
C12S C9S C15S C8S -128.5 . .
C7S C9S C15S C8S 127.3 . .
C11S C9S C15S C8S -59.2 . .
C12S C9S C15S C16S 138.3 . .
C7S C9S C15S C16S 34.1 . .
C11S C9S C15S C16S -152.4 . .
C12S C8S C15S C7S 86.9 . .
C11S C8S C15S C7S 134.2 . .
C12S C8S C15S C9S 31.4 . .
C7S C8S C15S C9S -55.5 . .
C11S C8S C15S C9S 78.7 . .
C12S C8S C15S C16S 126.0 . .
C7S C8S C15S C16S 39.1 . .
C11S C8S C15S C16S 173.3 . .
C9S C7S C16S C15S 63.8 . .
C8S C7S C16S C15S 52.0 . .
C9S C15S C16S C7S -67.0 . .
C8S C15S C16S C7S -90.1 . .
