#------------------------------------------------------------------------------
#$Date: 2018-09-09 19:32:12 +0200 (dom 09 de sep de 2018) $
#$Revision: 210660 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/39/7103937.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7103937
loop_
_publ_author_name
'Leung, Wing-Por'
'So, Cheuk-Wai'
'Wang, Jin-Zhi'
'Mak, Thomas C. W.'
_publ_section_title
;
 A novel synthesis of metallogermacyclopropane and molybdenum
 bis(iminophosphorano)carbene complexes from bisgermavinylidene
;
_journal_coden_ASTM              CHCOFS
_journal_issue                   2
_journal_name_full
;
 Chemical Communications (Cambridge, United Kingdom)
;
_journal_page_first              248
_journal_page_last               249
_journal_paper_doi               10.1039/b210598e
_journal_year                    2003
_chemical_formula_sum            'C42 H59 Mo N2 O5 P2 Si2'
_chemical_formula_weight         885.97
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.922(2)
_cell_angle_beta                 95.369(2)
_cell_angle_gamma                110.193(2)
_cell_formula_units_Z            2
_cell_length_a                   11.1278(11)
_cell_length_b                   14.2454(13)
_cell_length_c                   16.2005(15)
_cell_measurement_temperature    293(2)
_cell_volume                     2350.9(4)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.974
_diffrn_measured_fraction_theta_max 0.974
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0158
_diffrn_reflns_av_sigmaI/netI    0.0292
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            15832
_diffrn_reflns_theta_full        28.03
_diffrn_reflns_theta_max         28.03
_diffrn_reflns_theta_min         1.55
_exptl_absorpt_coefficient_mu    0.439
_exptl_absorpt_correction_T_max  0.7634
_exptl_absorpt_correction_T_min  0.5588
_exptl_absorpt_correction_type   SADABS
_exptl_crystal_density_diffrn    1.252
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             930
_exptl_crystal_size_max          1.50
_exptl_crystal_size_mid          0.72
_exptl_crystal_size_min          0.65
_refine_diff_density_max         3.783
_refine_diff_density_min         -0.340
_refine_diff_density_rms         0.073
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.037
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     487
_refine_ls_number_reflns         11098
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.037
_refine_ls_R_factor_all          0.0499
_refine_ls_R_factor_gt           0.0429
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0772P)²+1.3708P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1219
_refine_ls_wR_factor_ref         0.1282
_reflns_number_gt                9410
_reflns_number_total             11098
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b210598e.txt
_cod_data_source_block           scw178
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      p-1
_cod_database_code               7103937
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Mo1 Mo 0.241860(18) 0.312975(14) 0.282715(12) 0.03131(7) Uani 1 1 d . . .
Si1 Si 0.12002(8) 0.03739(6) 0.22077(6) 0.04780(19) Uani 1 1 d . . .
Si2 Si 0.24154(8) 0.37143(6) 0.07373(5) 0.04578(17) Uani 1 1 d . . .
P1 P -0.02871(6) 0.17684(4) 0.26861(4) 0.03172(13) Uani 1 1 d . . .
P2 P 0.04410(6) 0.36743(4) 0.19379(4) 0.03373(13) Uani 1 1 d . . .
N1 N 0.0843(2) 0.14538(15) 0.23636(13) 0.0350(4) Uani 1 1 d . . .
N2 N 0.1538(2) 0.33851(16) 0.15334(13) 0.0367(4) Uani 1 1 d . . .
O1 O 0.3465(2) 0.30689(18) 0.46473(13) 0.0571(5) Uani 1 1 d . . .
O2 O 0.4987(2) 0.2930(2) 0.23970(18) 0.0763(8) Uani 1 1 d . . .
O3 O 0.4254(2) 0.53083(16) 0.36836(15) 0.0614(6) Uani 1 1 d . . .
O4 O 0.3712(3) 0.6733(2) 0.51137(17) 0.0696(6) Uani 1 1 d . . .
O5 O 0.5793(2) 0.74328(19) 0.35927(17) 0.0679(6) Uani 1 1 d . . .
C1 C 0.3010(2) 0.30242(19) 0.39392(17) 0.0389(5) Uani 1 1 d . . .
C2 C 0.4009(3) 0.2975(2) 0.25348(18) 0.0451(6) Uani 1 1 d . . .
C3 C 0.3513(3) 0.4501(2) 0.33097(17) 0.0405(5) Uani 1 1 d . . .
C4 C 0.0230(2) 0.30970(17) 0.28185(15) 0.0328(4) Uani 1 1 d . . .
H4A H 0.0047 0.3469 0.3322 0.039 Uiso 1 1 calc R . .
C5 C 0.1647(7) 0.0164(4) 0.1151(4) 0.124(3) Uani 1 1 d . . .
H5A H 0.2338 0.0764 0.1087 0.186 Uiso 1 1 calc R . .
H5B H 0.0908 0.0024 0.0729 0.186 Uiso 1 1 calc R . .
H5C H 0.1927 -0.0406 0.1085 0.186 Uiso 1 1 calc R . .
C6 C 0.2609(4) 0.0501(3) 0.2995(4) 0.0911(15) Uani 1 1 d . . .
H6A H 0.3332 0.1101 0.2972 0.137 Uiso 1 1 calc R . .
H6B H 0.2840 -0.0089 0.2867 0.137 Uiso 1 1 calc R . .
H6C H 0.2379 0.0556 0.3553 0.137 Uiso 1 1 calc R . .
C7 C -0.0151(4) -0.0821(2) 0.2305(3) 0.0750(11) Uani 1 1 d . . .
H7A H -0.0904 -0.0927 0.1908 0.113 Uiso 1 1 calc R . .
H7B H -0.0353 -0.0750 0.2869 0.113 Uiso 1 1 calc R . .
H7C H 0.0117 -0.1394 0.2187 0.113 Uiso 1 1 calc R . .
C8 C 0.1502(5) 0.3987(4) -0.0172(3) 0.0889(14) Uani 1 1 d . . .
H8A H 0.1236 0.4544 0.0028 0.133 Uiso 1 1 calc R . .
H8B H 0.0751 0.3391 -0.0419 0.133 Uiso 1 1 calc R . .
H8C H 0.2053 0.4166 -0.0590 0.133 Uiso 1 1 calc R . .
C9 C 0.2887(5) 0.2633(3) 0.0290(3) 0.0810(12) Uani 1 1 d . . .
H9A H 0.3360 0.2464 0.0733 0.121 Uiso 1 1 calc R . .
H9B H 0.3422 0.2825 -0.0133 0.121 Uiso 1 1 calc R . .
H9C H 0.2121 0.2051 0.0039 0.121 Uiso 1 1 calc R . .
C10 C 0.3914(4) 0.4856(3) 0.1139(3) 0.0859(13) Uani 1 1 d . . .
H10A H 0.4402 0.4739 0.1607 0.129 Uiso 1 1 calc R . .
H10B H 0.3687 0.5438 0.1321 0.129 Uiso 1 1 calc R . .
H10C H 0.4429 0.4980 0.0695 0.129 Uiso 1 1 calc R . .
C11 C 0.3252(5) 0.5819(5) 0.5501(4) 0.1017(16) Uani 1 1 d . . .
H11A H 0.3338 0.5247 0.5133 0.122 Uiso 1 1 calc R . .
H11B H 0.3811 0.5947 0.6035 0.122 Uiso 1 1 calc R . .
C12 C 0.1941(7) 0.5537(7) 0.5649(5) 0.162(3) Uani 1 1 d . . .
H12A H 0.1718 0.4944 0.5900 0.243 Uiso 1 1 calc R . .
H12B H 0.1375 0.5388 0.5122 0.243 Uiso 1 1 calc R . .
H12C H 0.1849 0.6090 0.6025 0.243 Uiso 1 1 calc R . .
C13 C 0.3823(6) 0.7667(4) 0.5630(3) 0.0991(16) Uani 1 1 d . . .
H13A H 0.4337 0.7761 0.6175 0.119 Uiso 1 1 calc R . .
H13B H 0.2969 0.7652 0.5724 0.119 Uiso 1 1 calc R . .
C14 C 0.4441(7) 0.8516(4) 0.5219(4) 0.1122(18) Uani 1 1 d . . .
H14A H 0.4510 0.9146 0.5570 0.168 Uiso 1 1 calc R . .
H14B H 0.3926 0.8424 0.4682 0.168 Uiso 1 1 calc R . .
H14C H 0.5291 0.8535 0.5134 0.168 Uiso 1 1 calc R . .
C15 C 0.7033(5) 0.7501(4) 0.3381(4) 0.0981(15) Uani 1 1 d . . .
H15A H 0.7289 0.8011 0.3033 0.118 Uiso 1 1 calc R . .
H15B H 0.7655 0.7748 0.3900 0.118 Uiso 1 1 calc R . .
C16 C 0.7126(7) 0.6590(6) 0.2951(6) 0.172(4) Uani 1 1 d . . .
H16A H 0.8000 0.6722 0.2850 0.258 Uiso 1 1 calc R . .
H16B H 0.6549 0.6353 0.2420 0.258 Uiso 1 1 calc R . .
H16C H 0.6892 0.6079 0.3290 0.258 Uiso 1 1 calc R . .
C17 C 0.4850(5) 0.7389(4) 0.2907(3) 0.0953(15) Uani 1 1 d . . .
H17A H 0.3994 0.7124 0.3064 0.114 Uiso 1 1 calc R . .
H17B H 0.4878 0.6913 0.2418 0.114 Uiso 1 1 calc R . .
C18 C 0.5034(8) 0.8365(6) 0.2668(6) 0.177(4) Uani 1 1 d . . .
H18A H 0.4369 0.8276 0.2208 0.265 Uiso 1 1 calc R . .
H18B H 0.5868 0.8626 0.2495 0.265 Uiso 1 1 calc R . .
H18C H 0.4986 0.8839 0.3143 0.265 Uiso 1 1 calc R . .
C21 C -0.0655(3) 0.1476(2) 0.37125(17) 0.0426(5) Uani 1 1 d . . .
C22 C 0.0029(3) 0.2156(3) 0.44591(19) 0.0553(7) Uani 1 1 d . . .
H22A H 0.0638 0.2790 0.4441 0.066 Uiso 1 1 calc R . .
C23 C -0.0202(4) 0.1882(4) 0.5233(2) 0.0797(12) Uani 1 1 d . . .
H23A H 0.0246 0.2342 0.5731 0.096 Uiso 1 1 calc R . .
C24 C -0.1076(5) 0.0949(4) 0.5274(3) 0.0883(14) Uani 1 1 d . . .
H24A H -0.1201 0.0768 0.5796 0.106 Uiso 1 1 calc R . .
C25 C -0.1772(5) 0.0278(3) 0.4537(3) 0.0880(14) Uani 1 1 d . . .
H25A H -0.2380 -0.0354 0.4561 0.106 Uiso 1 1 calc R . .
C26 C -0.1568(4) 0.0543(3) 0.3762(2) 0.0671(9) Uani 1 1 d . . .
H26A H -0.2049 0.0090 0.3268 0.081 Uiso 1 1 calc R . .
C31 C -0.1856(2) 0.11030(18) 0.20152(16) 0.0373(5) Uani 1 1 d . . .
C32 C -0.2057(3) 0.0355(2) 0.13138(17) 0.0453(6) Uani 1 1 d . . .
H32A H -0.1364 0.0185 0.1154 0.054 Uiso 1 1 calc R . .
C33 C -0.3289(3) -0.0151(2) 0.0841(2) 0.0560(7) Uani 1 1 d . . .
H33A H -0.3421 -0.0665 0.0374 0.067 Uiso 1 1 calc R . .
C34 C -0.4309(3) 0.0107(3) 0.1062(2) 0.0582(8) Uani 1 1 d . . .
H34A H -0.5136 -0.0244 0.0754 0.070 Uiso 1 1 calc R . .
C35 C -0.4109(3) 0.0885(3) 0.1739(2) 0.0643(9) Uani 1 1 d . . .
H35A H -0.4794 0.1078 0.1877 0.077 Uiso 1 1 calc R . .
C36 C -0.2895(3) 0.1378(3) 0.2212(2) 0.0553(7) Uani 1 1 d . . .
H36A H -0.2766 0.1903 0.2670 0.066 Uiso 1 1 calc R . .
C41 C -0.1052(3) 0.3318(2) 0.11940(17) 0.0408(5) Uani 1 1 d . . .
C42 C -0.1316(3) 0.2578(2) 0.04781(19) 0.0505(6) Uani 1 1 d . . .
H42A H -0.0710 0.2283 0.0356 0.061 Uiso 1 1 calc R . .
C43 C -0.2490(3) 0.2266(3) -0.0067(2) 0.0638(9) Uani 1 1 d . . .
H43A H -0.2655 0.1775 -0.0557 0.077 Uiso 1 1 calc R . .
C44 C -0.3398(3) 0.2679(3) 0.0117(2) 0.0680(9) Uani 1 1 d . . .
H44A H -0.4181 0.2467 -0.0246 0.082 Uiso 1 1 calc R . .
C45 C -0.3151(3) 0.3406(3) 0.0838(3) 0.0708(10) Uani 1 1 d . . .
H45A H -0.3774 0.3680 0.0965 0.085 Uiso 1 1 calc R . .
C46 C -0.1980(3) 0.3734(3) 0.1379(2) 0.0595(8) Uani 1 1 d . . .
H46A H -0.1815 0.4232 0.1865 0.071 Uiso 1 1 calc R . .
C51 C 0.0817(3) 0.50320(19) 0.23285(17) 0.0419(5) Uani 1 1 d . . .
C52 C 0.0849(4) 0.5662(2) 0.1750(2) 0.0647(9) Uani 1 1 d . . .
H52A H 0.0672 0.5384 0.1173 0.078 Uiso 1 1 calc R . .
C53 C 0.1141(5) 0.6699(3) 0.2020(3) 0.0770(11) Uani 1 1 d . . .
H53A H 0.1170 0.7113 0.1626 0.092 Uiso 1 1 calc R . .
C54 C 0.1387(4) 0.7113(2) 0.2865(3) 0.0704(10) Uani 1 1 d . . .
H54A H 0.1552 0.7804 0.3045 0.084 Uiso 1 1 calc R . .
C55 C 0.1392(4) 0.6509(3) 0.3448(2) 0.0694(10) Uani 1 1 d . . .
H55A H 0.1576 0.6792 0.4024 0.083 Uiso 1 1 calc R . .
C56 C 0.1123(4) 0.5478(2) 0.3176(2) 0.0566(8) Uani 1 1 d . . .
H56A H 0.1148 0.5077 0.3574 0.068 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 Mo1 C1 77.98(11) . . ?
C3 Mo1 C2 84.62(12) . . ?
C1 Mo1 C2 85.86(11) . . ?
C3 Mo1 N2 99.12(9) . . ?
C1 Mo1 N2 172.54(9) . . ?
C2 Mo1 N2 100.78(10) . . ?
C3 Mo1 N1 171.56(9) . . ?
C1 Mo1 N1 98.96(9) . . ?
C2 Mo1 N1 103.11(10) . . ?
N2 Mo1 N1 82.94(7) . . ?
C3 Mo1 C4 105.34(10) . . ?
C1 Mo1 C4 106.54(9) . . ?
C2 Mo1 C4 165.32(10) . . ?
N2 Mo1 C4 67.40(8) . . ?
N1 Mo1 C4 67.78(7) . . ?
C3 Mo1 P2 94.83(8) . . ?
C1 Mo1 P2 139.95(8) . . ?
C2 Mo1 P2 133.17(8) . . ?
N2 Mo1 P2 32.91(5) . . ?
N1 Mo1 P2 82.42(5) . . ?
C4 Mo1 P2 36.93(6) . . ?
C3 Mo1 P1 139.53(8) . . ?
C1 Mo1 P1 97.81(8) . . ?
C2 Mo1 P1 135.64(9) . . ?
N2 Mo1 P1 79.87(5) . . ?
N1 Mo1 P1 32.55(5) . . ?
C4 Mo1 P1 36.63(5) . . ?
P2 Mo1 P1 62.557(18) . . ?
N1 Si1 C5 109.60(18) . . ?
N1 Si1 C6 110.85(17) . . ?
C5 Si1 C6 107.5(3) . . ?
N1 Si1 C7 114.77(15) . . ?
C5 Si1 C7 107.9(3) . . ?
C6 Si1 C7 105.88(18) . . ?
N2 Si2 C10 111.26(16) . . ?
N2 Si2 C9 108.89(16) . . ?
C10 Si2 C9 108.4(2) . . ?
N2 Si2 C8 114.19(16) . . ?
C10 Si2 C8 107.5(2) . . ?
C9 Si2 C8 106.3(2) . . ?
N1 P1 C4 106.80(11) . . ?
N1 P1 C31 114.05(11) . . ?
C4 P1 C31 113.30(11) . . ?
N1 P1 C21 114.92(12) . . ?
C4 P1 C21 105.84(12) . . ?
C31 P1 C21 101.79(12) . . ?
N1 P1 Mo1 54.07(7) . . ?
C4 P1 Mo1 55.59(8) . . ?
C31 P1 Mo1 147.30(8) . . ?
C21 P1 Mo1 110.80(9) . . ?
N2 P2 C4 105.51(11) . . ?
N2 P2 C41 113.38(12) . . ?
C4 P2 C41 113.48(12) . . ?
N2 P2 C51 116.01(12) . . ?
C4 P2 C51 106.37(12) . . ?
C41 P2 C51 102.15(12) . . ?
N2 P2 Mo1 54.28(8) . . ?
C4 P2 Mo1 56.17(8) . . ?
C41 P2 Mo1 150.61(9) . . ?
C51 P2 Mo1 107.19(9) . . ?
P1 N1 Si1 136.62(13) . . ?
P1 N1 Mo1 93.38(9) . . ?
Si1 N1 Mo1 124.14(11) . . ?
P2 N2 Si2 136.17(14) . . ?
P2 N2 Mo1 92.81(9) . . ?
Si2 N2 Mo1 123.71(11) . . ?
C13 O4 C11 115.6(4) . . ?
C15 O5 C17 115.6(4) . . ?
O1 C1 Mo1 172.8(2) . . ?
O2 C2 Mo1 176.2(3) . . ?
O3 C3 Mo1 172.1(2) . . ?
P1 C4 P2 120.05(13) . . ?
P1 C4 Mo1 87.78(9) . . ?
P2 C4 Mo1 86.90(9) . . ?
C12 C11 O4 114.5(6) . . ?
O4 C13 C14 109.9(4) . . ?
C16 C15 O5 116.6(5) . . ?
O5 C17 C18 114.3(5) . . ?
C26 C21 C22 118.7(3) . . ?
C26 C21 P1 120.4(2) . . ?
C22 C21 P1 120.8(2) . . ?
C23 C22 C21 119.6(3) . . ?
C24 C23 C22 121.2(4) . . ?
C23 C24 C25 119.5(4) . . ?
C24 C25 C26 120.1(4) . . ?
C25 C26 C21 120.8(4) . . ?
C32 C31 C36 118.5(2) . . ?
C32 C31 P1 123.1(2) . . ?
C36 C31 P1 118.5(2) . . ?
C31 C32 C33 120.4(3) . . ?
C34 C33 C32 120.2(3) . . ?
C33 C34 C35 119.9(3) . . ?
C34 C35 C36 119.9(3) . . ?
C35 C36 C31 121.0(3) . . ?
C42 C41 C46 119.3(3) . . ?
C42 C41 P2 120.3(2) . . ?
C46 C41 P2 120.2(2) . . ?
C41 C42 C43 120.3(3) . . ?
C44 C43 C42 120.2(3) . . ?
C43 C44 C45 119.9(3) . . ?
C44 C45 C46 120.5(3) . . ?
C45 C46 C41 119.8(3) . . ?
C56 C51 C52 117.7(3) . . ?
C56 C51 P2 123.1(2) . . ?
C52 C51 P2 119.1(2) . . ?
C53 C52 C51 120.9(3) . . ?
C54 C53 C52 120.0(3) . . ?
C53 C54 C55 120.1(3) . . ?
C54 C55 C56 119.7(3) . . ?
C51 C56 C55 121.5(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Mo1 C3 1.901(3) . ?
Mo1 C1 1.906(3) . ?
Mo1 C2 1.950(3) . ?
Mo1 N2 2.363(2) . ?
Mo1 N1 2.376(2) . ?
Mo1 C4 2.419(2) . ?
Mo1 P2 2.9072(6) . ?
Mo1 P1 2.9294(7) . ?
Si1 N1 1.706(2) . ?
Si1 C5 1.836(4) . ?
Si1 C6 1.864(4) . ?
Si1 C7 1.882(4) . ?
Si2 N2 1.716(2) . ?
Si2 C10 1.856(4) . ?
Si2 C9 1.859(4) . ?
Si2 C8 1.877(4) . ?
P1 N1 1.579(2) . ?
P1 C4 1.749(2) . ?
P1 C31 1.819(3) . ?
P1 C21 1.825(3) . ?
P2 N2 1.581(2) . ?
P2 C4 1.749(2) . ?
P2 C41 1.823(3) . ?
P2 C51 1.824(3) . ?
O1 C1 1.193(3) . ?
O2 C2 1.151(4) . ?
O3 C3 1.186(3) . ?
O4 C13 1.418(5) . ?
O4 C11 1.484(6) . ?
O5 C15 1.428(6) . ?
O5 C17 1.434(5) . ?
C11 C12 1.428(8) . ?
C13 C14 1.463(8) . ?
C15 C16 1.417(8) . ?
C17 C18 1.453(8) . ?
C21 C26 1.386(4) . ?
C21 C22 1.391(4) . ?
C22 C23 1.390(5) . ?
C23 C24 1.365(7) . ?
C24 C25 1.379(7) . ?
C25 C26 1.383(5) . ?
C31 C32 1.375(4) . ?
C31 C36 1.391(4) . ?
C32 C33 1.392(4) . ?
C33 C34 1.369(5) . ?
C34 C35 1.374(5) . ?
C35 C36 1.374(4) . ?
C41 C42 1.374(4) . ?
C41 C46 1.390(4) . ?
C42 C43 1.394(4) . ?
C43 C44 1.367(5) . ?
C44 C45 1.371(6) . ?
C45 C46 1.388(5) . ?
C51 C56 1.378(4) . ?
C51 C52 1.390(4) . ?
C52 C53 1.386(5) . ?
C53 C54 1.365(6) . ?
C54 C55 1.374(5) . ?
C55 C56 1.382(4) . ?
