#------------------------------------------------------------------------------
#$Date: 2015-06-18 10:22:19 +0200 (jue 18 de jun de 2015) $
#$Revision: 139322 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/73/7117319.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7117319
loop_
_publ_author_name
'Jessica L. Durham'
'Wade B. Wilson'
'Daniel N. Huh'
'Robert McDonald'
'Lisa F. Szczepura'
_publ_section_title
;
 Organometallic rhenium(III) chalcogenide clusters: coordination of
 N-heterocyclic carbenes
;
_journal_name_full               Chem.Commun.
_journal_page_first              10536
_journal_paper_doi               10.1039/C5cc03215F
_journal_volume                  51
_journal_year                    2015
_chemical_formula_moiety         'C54 H78 Cl2 N4 P2 Re6 S8, C H2 Cl2'
_chemical_formula_sum            'C55 H80 Cl4 N4 P2 Re6 S8'
_chemical_formula_weight         2374.65
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-04-09 deposited with the CCDC.
2015-05-28 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 92.1776(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.6282(11)
_cell_length_b                   16.7446(11)
_cell_length_c                   25.1262(17)
_cell_measurement_reflns_used    9532
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      28.27
_cell_measurement_theta_min      2.34
_cell_volume                     6990.9(8)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'DIRDIF-2008 (Beurskens et al., 2008)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0487
_diffrn_reflns_av_unetI/netI     0.0366
_diffrn_reflns_laue_measured_fraction_full 0.997
_diffrn_reflns_laue_measured_fraction_max 0.987
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            248189
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.312
_diffrn_reflns_theta_min         1.462
_exptl_absorpt_coefficient_mu    10.823
_exptl_absorpt_correction_T_max  0.1085
_exptl_absorpt_correction_T_min  0.0433
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'TWINABS (Sheldrick, 2008)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.256
_exptl_crystal_description       prism
_exptl_crystal_F_000             4456
_exptl_crystal_preparation       Luminescent
_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: dichloromethane/diethylether'
_exptl_crystal_size_max          0.344
_exptl_crystal_size_mid          0.322
_exptl_crystal_size_min          0.186
_refine_diff_density_max         2.571
_refine_diff_density_min         -2.745
_refine_diff_density_rms         0.241
_refine_ls_extinction_coef       0.000110(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     708
_refine_ls_number_reflns         33649
_refine_ls_number_restraints     25
_refine_ls_restrained_S_all      1.067
_refine_ls_R_factor_all          0.0631
_refine_ls_R_factor_gt           0.0492
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0583P)²+240.3996P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1472
_refine_ls_wR_factor_ref         0.1555
_reflns_Friedel_coverage         0.000
_reflns_friedel_fraction_full    .
_reflns_friedel_fraction_max     .
_reflns_number_gt                28321
_reflns_number_total             33649
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5cc03215f2.cif
_cod_data_source_block           isu1403
_cod_database_code               7117319
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.118
_shelx_estimated_absorpt_t_max   0.238
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.13291(3) 0.54042(3) 0.26266(2) 0.01981(11) Uani 1 1 d . . . . .
Re2 Re 0.26497(3) 0.62198(3) 0.25656(2) 0.02261(11) Uani 1 1 d . . . . .
Re3 Re 0.34513(3) 0.48928(3) 0.24807(2) 0.02778(13) Uani 1 1 d . . . . .
Re4 Re 0.21234(3) 0.40886(3) 0.25397(2) 0.02537(12) Uani 1 1 d D . . . .
Re5 Re 0.22434(3) 0.52079(3) 0.18143(2) 0.02161(11) Uani 1 1 d . . . . .
Re6 Re 0.25353(3) 0.51195(3) 0.32927(2) 0.02335(11) Uani 1 1 d . . . . .
Cl1 Cl -0.0091(2) 0.5645(2) 0.27332(16) 0.0386(8) Uani 1 1 d . . . . .
Cl2 Cl 0.2954(3) 0.7633(2) 0.25887(17) 0.0441(9) Uani 1 1 d . . . . .
S1 S 0.15116(19) 0.64266(18) 0.19619(12) 0.0238(6) Uani 1 1 d . . . . .
S2 S 0.1044(2) 0.44458(19) 0.19351(12) 0.0260(6) Uani 1 1 d . . . . .
S3 S 0.1306(2) 0.43594(18) 0.32801(12) 0.0229(6) Uani 1 1 d . . . . .
S4 S 0.1777(2) 0.63431(19) 0.33015(13) 0.0271(6) Uani 1 1 d . . . . .
S5 S 0.3497(2) 0.5944(2) 0.18363(12) 0.0270(6) Uani 1 1 d . . . . .
S6 S 0.2990(3) 0.3961(2) 0.17935(14) 0.0355(8) Uani 1 1 d . . . . .
S7 S 0.3256(2) 0.3886(2) 0.31562(15) 0.0373(8) Uani 1 1 d . . . . .
S8 S 0.3755(2) 0.5862(3) 0.31573(13) 0.0352(8) Uani 1 1 d . . . . .
P1A P 0.4907(11) 0.4649(9) 0.2380(8) 0.038(4) Uani 0.5 1 d D . P A 1
P1B P 0.4823(13) 0.4380(8) 0.2330(8) 0.036(3) Uani 0.5 1 d D . P A 2
P2A P 0.1483(7) 0.2735(4) 0.2523(7) 0.039(3) Uani 0.6 1 d D . P B 1
P2B P 0.1691(13) 0.2664(7) 0.2471(11) 0.039(3) Uani 0.4 1 d D . P B 2
N1 N 0.2437(8) 0.5817(10) 0.0595(5) 0.044(3) Uani 1 1 d . . . . .
N2 N 0.1292(8) 0.5240(8) 0.0662(4) 0.035(3) Uani 1 1 d . . . . .
N3 N 0.2093(8) 0.4970(8) 0.4537(5) 0.037(3) Uani 1 1 d . . . . .
N4 N 0.3235(7) 0.5554(8) 0.4490(4) 0.033(3) Uani 1 1 d . . . . .
C1 C 0.2002(9) 0.5386(9) 0.0950(6) 0.033(3) Uani 1 1 d . . . . .
C2 C 0.2024(12) 0.5900(15) 0.0103(7) 0.061(6) Uani 1 1 d . . . . .
H2 H 0.2216 0.6151 -0.0206 0.073 Uiso 1 1 calc R U . . .
C3 C 0.1309(12) 0.5557(14) 0.0152(6) 0.057(5) Uani 1 1 d . . . . .
H3 H 0.0887 0.5533 -0.0114 0.068 Uiso 1 1 calc R U . . .
C4 C 0.2654(9) 0.5183(9) 0.4168(6) 0.031(3) Uani 1 1 d . . . . .
C5 C 0.2331(11) 0.5209(11) 0.5040(6) 0.046(4) Uani 1 1 d . . . . .
H5 H 0.2037 0.5131 0.5352 0.056 Uiso 1 1 calc R U . . .
C6 C 0.3041(10) 0.5567(11) 0.5018(6) 0.041(4) Uani 1 1 d . . . . .
H6 H 0.3352 0.5786 0.5308 0.050 Uiso 1 1 calc R U . . .
C11A C 0.5631(18) 0.5397(18) 0.2627(14) 0.045(3) Uiso 0.5 1 d D U P A 1
H11A H 0.5578 0.5457 0.3016 0.054 Uiso 0.5 1 calc R U P A 1
H11B H 0.6181 0.5201 0.2566 0.054 Uiso 0.5 1 calc R U P A 1
C12A C 0.553(3) 0.621(2) 0.2367(18) 0.063(4) Uiso 0.5 1 d D U P A 1
H12A H 0.5932 0.6575 0.2518 0.075 Uiso 0.5 1 calc R U P A 1
H12B H 0.5592 0.6156 0.1983 0.075 Uiso 0.5 1 calc R U P A 1
H12C H 0.4988 0.6412 0.2433 0.075 Uiso 0.5 1 calc R U P A 1
C13A C 0.515(2) 0.455(3) 0.1676(11) 0.045(3) Uiso 0.5 1 d D U P A 1
H13A H 0.4816 0.4106 0.1524 0.054 Uiso 0.5 1 calc R U P A 1
H13B H 0.4968 0.5043 0.1491 0.054 Uiso 0.5 1 calc R U P A 1
C14A C 0.601(2) 0.440(3) 0.153(2) 0.063(4) Uiso 0.5 1 d D U P A 1
H14A H 0.6039 0.4356 0.1145 0.075 Uiso 0.5 1 calc R U P A 1
H14B H 0.6349 0.4837 0.1664 0.075 Uiso 0.5 1 calc R U P A 1
H14C H 0.6196 0.3895 0.1697 0.075 Uiso 0.5 1 calc R U P A 1
C15A C 0.524(2) 0.3740(14) 0.2735(13) 0.045(3) Uiso 0.5 1 d D U P A 1
H15A H 0.5832 0.3705 0.2715 0.054 Uiso 0.5 1 calc R U P A 1
H15B H 0.5118 0.3805 0.3115 0.054 Uiso 0.5 1 calc R U P A 1
C16A C 0.489(3) 0.295(2) 0.2548(18) 0.063(4) Uiso 0.5 1 d D U P A 1
H16A H 0.5116 0.2520 0.2769 0.075 Uiso 0.5 1 calc R U P A 1
H16B H 0.4304 0.2964 0.2577 0.075 Uiso 0.5 1 calc R U P A 1
H16C H 0.5021 0.2863 0.2176 0.075 Uiso 0.5 1 calc R U P A 1
C11B C 0.5625(18) 0.4961(19) 0.2666(13) 0.045(3) Uiso 0.5 1 d D U P A 2
H11C H 0.5557 0.4930 0.3055 0.054 Uiso 0.5 1 calc R U P A 2
H11D H 0.6149 0.4714 0.2590 0.054 Uiso 0.5 1 calc R U P A 2
C12B C 0.565(3) 0.583(2) 0.2505(19) 0.063(4) Uiso 0.5 1 d D U P A 2
H12D H 0.6093 0.6099 0.2702 0.075 Uiso 0.5 1 calc R U P A 2
H12E H 0.5732 0.5871 0.2122 0.075 Uiso 0.5 1 calc R U P A 2
H12F H 0.5139 0.6088 0.2588 0.075 Uiso 0.5 1 calc R U P A 2
C13B C 0.503(2) 0.439(3) 0.1618(11) 0.045(3) Uiso 0.5 1 d D U P A 2
H13C H 0.4674 0.3989 0.1436 0.054 Uiso 0.5 1 calc R U P A 2
H13D H 0.4887 0.4918 0.1471 0.054 Uiso 0.5 1 calc R U P A 2
C14B C 0.589(2) 0.420(3) 0.149(2) 0.063(4) Uiso 0.5 1 d D U P A 2
H14D H 0.5948 0.4217 0.1103 0.075 Uiso 0.5 1 calc R U P A 2
H14E H 0.6249 0.4600 0.1660 0.075 Uiso 0.5 1 calc R U P A 2
H14F H 0.6035 0.3669 0.1624 0.075 Uiso 0.5 1 calc R U P A 2
C15B C 0.505(2) 0.3339(14) 0.2499(12) 0.045(3) Uiso 0.5 1 d D U P A 2
H15C H 0.4583 0.3007 0.2386 0.054 Uiso 0.5 1 calc R U P A 2
H15D H 0.5512 0.3166 0.2289 0.054 Uiso 0.5 1 calc R U P A 2
C16B C 0.525(3) 0.316(3) 0.3079(12) 0.063(4) Uiso 0.5 1 d D U P A 2
H16D H 0.5363 0.2594 0.3124 0.075 Uiso 0.5 1 calc R U P A 2
H16E H 0.5727 0.3473 0.3196 0.075 Uiso 0.5 1 calc R U P A 2
H16F H 0.4795 0.3315 0.3293 0.075 Uiso 0.5 1 calc R U P A 2
C21A C 0.157(2) 0.216(2) 0.3144(11) 0.067(5) Uiso 0.6 1 d D U P B 1
H21A H 0.1320 0.2466 0.3431 0.080 Uiso 0.6 1 calc R U P B 1
H21B H 0.1262 0.1654 0.3096 0.080 Uiso 0.6 1 calc R U P B 1
C22A C 0.243(2) 0.196(3) 0.3313(17) 0.068(5) Uiso 0.6 1 d D U P B 1
H22A H 0.2435 0.1653 0.3645 0.082 Uiso 0.6 1 calc R U P B 1
H22B H 0.2675 0.1644 0.3035 0.082 Uiso 0.6 1 calc R U P B 1
H22C H 0.2734 0.2456 0.3370 0.082 Uiso 0.6 1 calc R U P B 1
C23A C 0.194(2) 0.2007(18) 0.2076(10) 0.067(5) Uiso 0.6 1 d D U P B 1
H23A H 0.2531 0.2016 0.2140 0.080 Uiso 0.6 1 calc R U P B 1
H23B H 0.1748 0.1466 0.2168 0.080 Uiso 0.6 1 calc R U P B 1
C24A C 0.176(2) 0.215(2) 0.1491(12) 0.068(5) Uiso 0.6 1 d D U P B 1
H24A H 0.2020 0.1740 0.1282 0.082 Uiso 0.6 1 calc R U P B 1
H24B H 0.1173 0.2128 0.1420 0.082 Uiso 0.6 1 calc R U P B 1
H24C H 0.1957 0.2679 0.1393 0.082 Uiso 0.6 1 calc R U P B 1
C25A C 0.0411(12) 0.270(2) 0.2314(13) 0.067(5) Uiso 0.6 1 d D U P B 1
H25A H 0.0348 0.2946 0.1957 0.080 Uiso 0.6 1 calc R U P B 1
H25B H 0.0251 0.2131 0.2277 0.080 Uiso 0.6 1 calc R U P B 1
C26A C -0.016(3) 0.310(3) 0.2678(17) 0.068(5) Uiso 0.6 1 d D U P B 1
H26A H -0.0713 0.3049 0.2531 0.082 Uiso 0.6 1 calc R U P B 1
H26B H -0.0121 0.2853 0.3031 0.082 Uiso 0.6 1 calc R U P B 1
H26C H -0.0023 0.3671 0.2710 0.082 Uiso 0.6 1 calc R U P B 1
C21B C 0.240(3) 0.196(3) 0.2786(17) 0.067(5) Uiso 0.4 1 d D U P B 2
H21C H 0.2351 0.1443 0.2592 0.080 Uiso 0.4 1 calc R U P B 2
H21D H 0.2949 0.2159 0.2743 0.080 Uiso 0.4 1 calc R U P B 2
C22B C 0.229(4) 0.179(4) 0.3370(19) 0.068(5) Uiso 0.4 1 d D U P B 2
H22D H 0.2694 0.1407 0.3499 0.082 Uiso 0.4 1 calc R U P B 2
H22E H 0.2350 0.2292 0.3571 0.082 Uiso 0.4 1 calc R U P B 2
H22F H 0.1749 0.1573 0.3419 0.082 Uiso 0.4 1 calc R U P B 2
C23B C 0.122(3) 0.236(3) 0.1830(15) 0.067(5) Uiso 0.4 1 d D U P B 2
H23C H 0.0658 0.2200 0.1893 0.080 Uiso 0.4 1 calc R U P B 2
H23D H 0.1198 0.2832 0.1594 0.080 Uiso 0.4 1 calc R U P B 2
C24B C 0.162(3) 0.169(3) 0.154(2) 0.068(5) Uiso 0.4 1 d D U P B 2
H24D H 0.1312 0.1580 0.1203 0.082 Uiso 0.4 1 calc R U P B 2
H24E H 0.2168 0.1840 0.1459 0.082 Uiso 0.4 1 calc R U P B 2
H24F H 0.1626 0.1206 0.1759 0.082 Uiso 0.4 1 calc R U P B 2
C25B C 0.075(2) 0.253(3) 0.282(2) 0.067(5) Uiso 0.4 1 d D U P B 2
H25C H 0.0640 0.1950 0.2843 0.080 Uiso 0.4 1 calc R U P B 2
H25D H 0.0847 0.2720 0.3195 0.080 Uiso 0.4 1 calc R U P B 2
C26B C 0.000(3) 0.294(4) 0.260(3) 0.068(5) Uiso 0.4 1 d D U P B 2
H26D H -0.0452 0.2815 0.2827 0.082 Uiso 0.4 1 calc R U P B 2
H26E H 0.0086 0.3514 0.2592 0.082 Uiso 0.4 1 calc R U P B 2
H26F H -0.0121 0.2741 0.2239 0.082 Uiso 0.4 1 calc R U P B 2
C31 C 0.3266(10) 0.6096(11) 0.0643(6) 0.042(4) Uani 1 1 d . . . . .
C32 C 0.3401(10) 0.6903(11) 0.0746(6) 0.043(4) Uani 1 1 d . . . . .
C33 C 0.4189(11) 0.7168(12) 0.0741(7) 0.051(4) Uani 1 1 d . . . . .
H33 H 0.4301 0.7717 0.0806 0.061 Uiso 1 1 calc R U . . .
C34 C 0.4823(11) 0.6650(14) 0.0643(7) 0.054(5) Uani 1 1 d . . . . .
C35 C 0.4660(11) 0.5859(14) 0.0546(7) 0.054(5) Uani 1 1 d . . . . .
H35 H 0.5091 0.5505 0.0478 0.064 Uiso 1 1 calc R U . . .
C36 C 0.3877(10) 0.5564(11) 0.0544(6) 0.042(4) Uani 1 1 d . . . . .
C37 C 0.2734(12) 0.7448(12) 0.0886(9) 0.059(5) Uani 1 1 d . . . . .
H37A H 0.2412 0.7581 0.0564 0.071 Uiso 1 1 calc R U . . .
H37B H 0.2959 0.7938 0.1045 0.071 Uiso 1 1 calc R U . . .
H37C H 0.2393 0.7183 0.1142 0.071 Uiso 1 1 calc R U . . .
C38 C 0.5672(13) 0.6978(16) 0.0664(11) 0.077(7) Uani 1 1 d . . . . .
H38A H 0.5841 0.7085 0.1035 0.092 Uiso 1 1 calc R U . . .
H38B H 0.5688 0.7475 0.0459 0.092 Uiso 1 1 calc R U . . .
H38C H 0.6037 0.6587 0.0512 0.092 Uiso 1 1 calc R U . . .
C39 C 0.3705(14) 0.4683(14) 0.0426(8) 0.065(6) Uani 1 1 d . . . . .
H39A H 0.3529 0.4419 0.0750 0.078 Uiso 1 1 calc R U . . .
H39B H 0.4196 0.4425 0.0307 0.078 Uiso 1 1 calc R U . . .
H39C H 0.3281 0.4640 0.0146 0.078 Uiso 1 1 calc R U . . .
C41 C 0.0618(9) 0.4744(9) 0.0801(5) 0.033(3) Uani 1 1 d . . . . .
C42 C -0.0068(10) 0.5098(10) 0.0993(6) 0.037(3) Uani 1 1 d . . . . .
C43 C -0.0693(11) 0.4597(12) 0.1135(6) 0.047(4) Uani 1 1 d . . . . .
H43 H -0.1154 0.4830 0.1283 0.057 Uiso 1 1 calc R U . . .
C44 C -0.0677(15) 0.3786(14) 0.1071(8) 0.067(7) Uani 1 1 d . . . . .
C45 C 0.0003(16) 0.3464(12) 0.0839(8) 0.065(6) Uani 1 1 d . . . . .
H45 H 0.0015 0.2906 0.0772 0.078 Uiso 1 1 calc R U . . .
C46 C 0.0665(12) 0.3924(11) 0.0703(7) 0.049(4) Uani 1 1 d . . . . .
C47 C -0.0141(12) 0.5972(11) 0.1074(8) 0.054(5) Uani 1 1 d . . . . .
H47A H 0.0146 0.6124 0.1406 0.064 Uiso 1 1 calc R U . . .
H47B H -0.0710 0.6116 0.1093 0.064 Uiso 1 1 calc R U . . .
H47C H 0.0094 0.6253 0.0775 0.064 Uiso 1 1 calc R U . . .
C48 C -0.1352(17) 0.3259(17) 0.1226(10) 0.104(12) Uani 1 1 d . . . . .
H48A H -0.1265 0.3092 0.1598 0.125 Uiso 1 1 calc R U . . .
H48B H -0.1373 0.2786 0.0996 0.125 Uiso 1 1 calc R U . . .
H48C H -0.1861 0.3551 0.1187 0.125 Uiso 1 1 calc R U . . .
C49 C 0.1404(16) 0.3587(14) 0.0476(9) 0.075(7) Uani 1 1 d . . . . .
H49A H 0.1539 0.3891 0.0158 0.091 Uiso 1 1 calc R U . . .
H49B H 0.1311 0.3027 0.0379 0.091 Uiso 1 1 calc R U . . .
H49C H 0.1850 0.3621 0.0741 0.091 Uiso 1 1 calc R U . . .
C51 C 0.1364(10) 0.4504(10) 0.4449(5) 0.037(3) Uani 1 1 d . . . . .
C52 C 0.1441(10) 0.3677(10) 0.4493(6) 0.038(3) Uani 1 1 d . . . . .
C53 C 0.0748(12) 0.3230(11) 0.4420(7) 0.046(4) Uani 1 1 d . . . . .
H53 H 0.0784 0.2664 0.4437 0.056 Uiso 1 1 calc R U . . .
C54 C -0.0003(11) 0.3581(11) 0.4324(7) 0.046(4) Uani 1 1 d . . . . .
C55 C -0.0056(10) 0.4405(11) 0.4308(7) 0.043(4) Uani 1 1 d . . . . .
H55 H -0.0568 0.4649 0.4250 0.051 Uiso 1 1 calc R U . . .
C56 C 0.0624(10) 0.4884(9) 0.4373(6) 0.036(3) Uani 1 1 d . . . . .
C57 C 0.2251(12) 0.3285(12) 0.4578(8) 0.057(5) Uani 1 1 d . . . . .
H57A H 0.2179 0.2707 0.4617 0.068 Uiso 1 1 calc R U . . .
H57B H 0.2518 0.3500 0.4902 0.068 Uiso 1 1 calc R U . . .
H57C H 0.2582 0.3393 0.4272 0.068 Uiso 1 1 calc R U . . .
C58 C -0.0760(12) 0.3075(13) 0.4252(10) 0.066(6) Uani 1 1 d . . . . .
H58A H -0.0797 0.2708 0.4554 0.079 Uiso 1 1 calc R U . . .
H58B H -0.0736 0.2768 0.3921 0.079 Uiso 1 1 calc R U . . .
H58C H -0.1233 0.3424 0.4234 0.079 Uiso 1 1 calc R U . . .
C59 C 0.0542(11) 0.5780(11) 0.4331(7) 0.046(4) Uani 1 1 d . . . . .
H59A H 0.0073 0.5955 0.4524 0.055 Uiso 1 1 calc R U . . .
H59B H 0.0473 0.5933 0.3955 0.055 Uiso 1 1 calc R U . . .
H59C H 0.1028 0.6034 0.4486 0.055 Uiso 1 1 calc R U . . .
C61 C 0.3995(9) 0.5908(10) 0.4339(6) 0.037(3) Uani 1 1 d . . . . .
C62 C 0.4044(10) 0.6733(11) 0.4298(6) 0.042(4) Uani 1 1 d . . . . .
C63 C 0.4778(12) 0.7053(14) 0.4196(8) 0.058(5) Uani 1 1 d . . . . .
H63 H 0.4830 0.7617 0.4176 0.070 Uiso 1 1 calc R U . . .
C64 C 0.5455(12) 0.6581(15) 0.4120(8) 0.061(6) Uani 1 1 d . . . . .
C65 C 0.5379(11) 0.5764(15) 0.4174(7) 0.060(6) Uani 1 1 d . . . . .
H65 H 0.5839 0.5437 0.4131 0.072 Uiso 1 1 calc R U . . .
C66 C 0.4653(10) 0.5406(12) 0.4290(6) 0.043(4) Uani 1 1 d . . . . .
C67 C 0.3315(12) 0.7254(11) 0.4334(8) 0.053(4) Uani 1 1 d . . . . .
H67A H 0.2998 0.7229 0.3998 0.064 Uiso 1 1 calc R U . . .
H67B H 0.3483 0.7806 0.4403 0.064 Uiso 1 1 calc R U . . .
H67C H 0.2986 0.7066 0.4625 0.064 Uiso 1 1 calc R U . . .
C68 C 0.6249(14) 0.697(2) 0.3990(12) 0.104(11) Uani 1 1 d . . . . .
H68A H 0.6387 0.7376 0.4256 0.125 Uiso 1 1 calc R U . . .
H68B H 0.6202 0.7210 0.3636 0.125 Uiso 1 1 calc R U . . .
H68C H 0.6673 0.6558 0.3994 0.125 Uiso 1 1 calc R U . . .
C69 C 0.4579(12) 0.4513(12) 0.4339(8) 0.055(5) Uani 1 1 d . . . . .
H69A H 0.4213 0.4310 0.4056 0.066 Uiso 1 1 calc R U . . .
H69B H 0.4366 0.4379 0.4687 0.066 Uiso 1 1 calc R U . . .
H69C H 0.5110 0.4267 0.4307 0.066 Uiso 1 1 calc R U . . .
Cl1S Cl 0.2120(4) 0.5253(4) 0.7640(3) 0.0725(15) Uani 1 1 d . . . . .
Cl2S Cl 0.2352(5) 0.5332(5) 0.6505(3) 0.094(2) Uani 1 1 d . . . . .
C1S C 0.1800(14) 0.5686(13) 0.7046(11) 0.074(7) Uani 1 1 d . . . . .
H1SA H 0.1862 0.6272 0.7074 0.089 Uiso 1 1 calc R U . . .
H1SB H 0.1222 0.5568 0.6979 0.089 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
S2 Re1 S3 90.00(10) . .
S2 Re1 S4 173.41(12) . .
S3 Re1 S4 90.38(11) . .
S2 Re1 S1 90.00(11) . .
S3 Re1 S1 173.58(11) . .
S4 Re1 S1 88.89(11) . .
S2 Re1 Cl1 91.40(13) . .
S3 Re1 Cl1 90.28(12) . .
S4 Re1 Cl1 95.18(13) . .
S1 Re1 Cl1 96.15(12) . .
S2 Re1 Re4 57.04(8) . .
S3 Re1 Re4 57.15(8) . .
S4 Re1 Re4 118.08(9) . .
S1 Re1 Re4 117.87(8) . .
Cl1 Re1 Re4 130.97(10) . .
S2 Re1 Re2 116.98(8) . .
S3 Re1 Re2 117.34(8) . .
S4 Re1 Re2 57.23(8) . .
S1 Re1 Re2 57.19(8) . .
Cl1 Re1 Re2 138.60(10) . .
Re4 Re1 Re2 90.42(2) . .
S2 Re1 Re6 117.96(8) . .
S3 Re1 Re6 57.27(8) . .
S4 Re1 Re6 57.17(9) . .
S1 Re1 Re6 117.33(8) . .
Cl1 Re1 Re6 133.58(10) . .
Re4 Re1 Re6 60.97(2) . .
Re2 Re1 Re6 60.141(19) . .
S2 Re1 Re5 56.97(8) . .
S3 Re1 Re5 117.88(8) . .
S4 Re1 Re5 117.29(8) . .
S1 Re1 Re5 57.14(8) . .
Cl1 Re1 Re5 134.97(10) . .
Re4 Re1 Re5 60.775(19) . .
Re2 Re1 Re5 60.072(19) . .
Re6 Re1 Re5 91.27(2) . .
S8 Re2 S5 88.13(12) . .
S8 Re2 S4 90.87(12) . .
S5 Re2 S4 173.80(12) . .
S8 Re2 S1 173.78(13) . .
S5 Re2 S1 90.96(11) . .
S4 Re2 S1 89.38(11) . .
S8 Re2 Cl2 94.30(15) . .
S5 Re2 Cl2 94.49(13) . .
S4 Re2 Cl2 91.69(12) . .
S1 Re2 Cl2 91.91(13) . .
S8 Re2 Re1 117.53(9) . .
S5 Re2 Re1 117.81(9) . .
S4 Re2 Re1 57.50(8) . .
S1 Re2 Re1 57.71(7) . .
Cl2 Re2 Re1 133.61(11) . .
S8 Re2 Re3 56.93(10) . .
S5 Re2 Re3 57.03(8) . .
S4 Re2 Re3 117.54(8) . .
S1 Re2 Re3 117.66(8) . .
Cl2 Re2 Re3 136.80(11) . .
Re1 Re2 Re3 89.58(2) . .
S8 Re2 Re5 117.29(10) . .
S5 Re2 Re5 57.66(8) . .
S4 Re2 Re5 117.76(8) . .
S1 Re2 Re5 57.37(8) . .
Cl2 Re2 Re5 134.53(10) . .
Re1 Re2 Re5 60.271(18) . .
Re3 Re2 Re5 60.36(2) . .
S8 Re2 Re6 57.50(9) . .
S5 Re2 Re6 117.39(9) . .
S4 Re2 Re6 57.25(8) . .
S1 Re2 Re6 117.85(8) . .
Cl2 Re2 Re6 134.03(10) . .
Re1 Re2 Re6 60.149(19) . .
Re3 Re2 Re6 60.36(2) . .
Re5 Re2 Re6 91.40(2) . .
S8 Re3 S5 88.33(12) . .
S8 Re3 S7 90.25(14) . .
S5 Re3 S7 173.49(12) . .
S8 Re3 S6 173.64(13) . .
S5 Re3 S6 90.49(12) . .
S7 Re3 S6 90.23(13) . .
S8 Re3 P1A 90.2(4) . .
S5 Re3 P1A 89.8(4) . .
S7 Re3 P1A 96.6(4) . .
S6 Re3 P1A 96.0(4) . .
S8 Re3 P1B 100.0(4) . .
S5 Re3 P1B 95.6(4) . .
S7 Re3 P1B 90.9(4) . .
S6 Re3 P1B 86.4(4) . .
S8 Re3 Re4 117.94(9) . .
S5 Re3 Re4 117.95(8) . .
S7 Re3 Re4 57.44(10) . .
S6 Re3 Re4 57.40(9) . .
P1A Re3 Re4 139.2(3) . .
P1B Re3 Re4 128.2(3) . .
S8 Re3 Re2 57.13(10) . .
S5 Re3 Re2 57.15(8) . .
S7 Re3 Re2 116.98(9) . .
S6 Re3 Re2 117.21(9) . .
P1A Re3 Re2 130.9(3) . .
P1B Re3 Re2 141.7(3) . .
Re4 Re3 Re2 89.93(2) . .
S8 Re3 Re5 116.99(10) . .
S5 Re3 Re5 57.50(8) . .
S7 Re3 Re5 117.90(10) . .
S6 Re3 Re5 57.41(9) . .
P1A Re3 Re5 134.1(4) . .
P1B Re3 Re5 131.3(5) . .
Re4 Re3 Re5 60.50(2) . .
Re2 Re3 Re5 59.863(19) . .
S8 Re3 Re6 57.37(8) . .
S5 Re3 Re6 117.01(8) . .
S7 Re3 Re6 57.17(9) . .
S6 Re3 Re6 118.00(10) . .
P1A Re3 Re6 134.6(4) . .
P1B Re3 Re6 137.3(5) . .
Re4 Re3 Re6 60.63(2) . .
Re2 Re3 Re6 59.870(19) . .
Re5 Re3 Re6 90.82(2) . .
S2 Re4 S3 90.68(11) . .
S2 Re4 S7 173.50(13) . .
S3 Re4 S7 88.84(12) . .
S2 Re4 S6 89.12(12) . .
S3 Re4 S6 173.96(12) . .
S7 Re4 S6 90.67(13) . .
S2 Re4 P2B 89.3(6) . .
S3 Re4 P2B 93.7(5) . .
S7 Re4 P2B 97.2(6) . .
S6 Re4 P2B 92.3(5) . .
S2 Re4 P2A 84.7(4) . .
S3 Re4 P2A 86.0(3) . .
S7 Re4 P2A 101.8(4) . .
S6 Re4 P2A 100.0(3) . .
S2 Re4 Re1 57.62(8) . .
S3 Re4 Re1 57.60(7) . .
S7 Re4 Re1 117.02(10) . .
S6 Re4 Re1 117.57(9) . .
P2B Re4 Re1 132.4(5) . .
P2A Re4 Re1 123.7(2) . .
S2 Re4 Re3 117.09(8) . .
S3 Re4 Re3 117.15(8) . .
S7 Re4 Re3 57.69(10) . .
S6 Re4 Re3 57.85(10) . .
P2B Re4 Re3 137.3(5) . .
P2A Re4 Re3 146.2(2) . .
Re1 Re4 Re3 90.07(2) . .
S2 Re4 Re5 56.91(8) . .
S3 Re4 Re5 117.73(7) . .
S7 Re4 Re5 117.85(10) . .
S6 Re4 Re5 57.43(9) . .
P2B Re4 Re5 131.6(7) . .
P2A Re4 Re5 132.7(4) . .
Re1 Re4 Re5 60.169(19) . .
Re3 Re4 Re5 60.20(2) . .
S2 Re4 Re6 117.56(8) . .
S3 Re4 Re6 57.03(8) . .
S7 Re4 Re6 57.06(10) . .
S6 Re4 Re6 117.95(10) . .
P2B Re4 Re6 138.0(7) . .
P2A Re4 Re6 134.8(4) . .
Re1 Re4 Re6 59.983(19) . .
Re3 Re4 Re6 60.14(2) . .
Re5 Re4 Re6 90.36(2) . .
C1 Re5 S2 94.3(4) . .
C1 Re5 S1 87.9(4) . .
S2 Re5 S1 90.22(11) . .
C1 Re5 S5 94.5(4) . .
S2 Re5 S5 171.24(11) . .
S1 Re5 S5 90.27(11) . .
C1 Re5 S6 99.7(4) . .
S2 Re5 S6 88.50(13) . .
S1 Re5 S6 172.39(11) . .
S5 Re5 S6 89.86(13) . .
C1 Re5 Re2 130.9(4) . .
S2 Re5 Re2 116.65(8) . .
S1 Re5 Re2 57.12(8) . .
S5 Re5 Re2 56.84(8) . .
S6 Re5 Re2 117.08(10) . .
C1 Re5 Re1 131.3(4) . .
S2 Re5 Re1 57.05(8) . .
S1 Re5 Re1 57.40(7) . .
S5 Re5 Re1 116.39(8) . .
S6 Re5 Re1 115.98(9) . .
Re2 Re5 Re1 59.657(18) . .
C1 Re5 Re3 139.5(4) . .
S2 Re5 Re3 115.69(8) . .
S1 Re5 Re3 116.83(8) . .
S5 Re5 Re3 56.58(8) . .
S6 Re5 Re3 57.36(10) . .
Re2 Re5 Re3 59.78(2) . .
Re1 Re5 Re3 88.90(2) . .
C1 Re5 Re4 139.5(4) . .
S2 Re5 Re4 56.42(8) . .
S1 Re5 Re4 116.41(8) . .
S5 Re5 Re4 115.82(8) . .
S6 Re5 Re4 56.95(9) . .
Re2 Re5 Re4 89.19(2) . .
Re1 Re5 Re4 59.056(18) . .
Re3 Re5 Re4 59.30(2) . .
C4 Re6 S4 88.7(4) . .
C4 Re6 S3 94.8(4) . .
S4 Re6 S3 90.31(11) . .
C4 Re6 S8 94.1(4) . .
S4 Re6 S8 90.35(13) . .
S3 Re6 S8 171.13(11) . .
C4 Re6 S7 99.0(4) . .
S4 Re6 S7 172.28(12) . .
S3 Re6 S7 88.36(13) . .
S8 Re6 S7 89.81(15) . .
C4 Re6 Re2 131.2(4) . .
S4 Re6 Re2 57.10(8) . .
S3 Re6 Re2 116.68(7) . .
S8 Re6 Re2 56.85(9) . .
S7 Re6 Re2 117.03(9) . .
C4 Re6 Re1 132.1(4) . .
S4 Re6 Re1 57.29(8) . .
S3 Re6 Re1 57.05(7) . .
S8 Re6 Re1 116.44(9) . .
S7 Re6 Re1 115.99(10) . .
Re2 Re6 Re1 59.710(18) . .
C4 Re6 Re3 138.7(4) . .
S4 Re6 Re3 116.80(8) . .
S3 Re6 Re3 115.57(7) . .
S8 Re6 Re3 56.52(9) . .
S7 Re6 Re3 57.32(9) . .
Re2 Re6 Re3 59.77(2) . .
Re1 Re6 Re3 88.99(2) . .
C4 Re6 Re4 139.5(4) . .
S4 Re6 Re4 116.28(8) . .
S3 Re6 Re4 56.37(7) . .
S8 Re6 Re4 115.69(9) . .
S7 Re6 Re4 56.97(10) . .
Re2 Re6 Re4 89.06(2) . .
Re1 Re6 Re4 59.044(19) . .
Re3 Re6 Re4 59.23(2) . .
Re2 S1 Re5 65.52(8) . .
Re2 S1 Re1 65.10(8) . .
Re5 S1 Re1 65.45(8) . .
Re4 S2 Re5 66.67(9) . .
Re4 S2 Re1 65.34(8) . .
Re5 S2 Re1 65.97(8) . .
Re4 S3 Re1 65.25(8) . .
Re4 S3 Re6 66.60(8) . .
Re1 S3 Re6 65.68(8) . .
Re2 S4 Re6 65.65(9) . .
Re2 S4 Re1 65.28(8) . .
Re6 S4 Re1 65.55(8) . .
Re3 S5 Re2 65.82(8) . .
Re3 S5 Re5 65.91(9) . .
Re2 S5 Re5 65.50(8) . .
Re4 S6 Re3 64.75(9) . .
Re4 S6 Re5 65.63(9) . .
Re3 S6 Re5 65.23(9) . .
Re4 S7 Re6 65.98(9) . .
Re4 S7 Re3 64.87(9) . .
Re6 S7 Re3 65.51(10) . .
Re3 S8 Re2 65.94(9) . .
Re3 S8 Re6 66.11(10) . .
Re2 S8 Re6 65.66(9) . .
C11A P1A C13A 103.0(18) . .
C11A P1A C15A 102.8(16) . .
C13A P1A C15A 109(2) . .
C11A P1A Re3 119.1(14) . .
C13A P1A Re3 111.3(15) . .
C15A P1A Re3 111.4(14) . .
C11B P1B C15B 104.9(18) . .
C11B P1B C13B 106.7(19) . .
C15B P1B C13B 100.8(19) . .
C11B P1B Re3 113.8(14) . .
C15B P1B Re3 118.5(15) . .
C13B P1B Re3 110.7(15) . .
C21A P2A C25A 105.6(17) . .
C21A P2A C23A 98.6(16) . .
C25A P2A C23A 102.8(16) . .
C21A P2A Re4 116.3(14) . .
C25A P2A Re4 116.2(13) . .
C23A P2A Re4 115.1(13) . .
C21B P2B C23B 116(2) . .
C21B P2B C25B 105(3) . .
C23B P2B C25B 93(3) . .
C21B P2B Re4 114(2) . .
C23B P2B Re4 116(2) . .
C25B P2B Re4 109(2) . .
C1 N1 C2 111.9(14) . .
C1 N1 C31 129.4(13) . .
C2 N1 C31 118.2(13) . .
C1 N2 C3 111.7(13) . .
C1 N2 C41 128.9(12) . .
C3 N2 C41 119.0(12) . .
C5 N3 C4 111.3(13) . .
C5 N3 C51 120.4(13) . .
C4 N3 C51 128.1(12) . .
C6 N4 C4 112.8(13) . .
C6 N4 C61 118.8(12) . .
C4 N4 C61 128.4(12) . .
N1 C1 N2 102.3(12) . .
N1 C1 Re5 128.8(11) . .
N2 C1 Re5 127.6(10) . .
C3 C2 N1 106.6(15) . .
C2 C3 N2 107.4(15) . .
N4 C4 N3 101.3(12) . .
N4 C4 Re6 129.8(10) . .
N3 C4 Re6 128.1(10) . .
C6 C5 N3 108.7(15) . .
C5 C6 N4 105.9(14) . .
C12A C11A P1A 114(2) . .
C14A C13A P1A 119(3) . .
C16A C15A P1A 118(3) . .
C12B C11B P1B 115(3) . .
C14B C13B P1B 115(3) . .
C16B C15B P1B 116(3) . .
C22A C21A P2A 113(2) . .
C24A C23A P2A 115(2) . .
C26A C25A P2A 116(3) . .
C22B C21B P2B 116(4) . .
C24B C23B P2B 117(3) . .
C26B C25B P2B 118(4) . .
C36 C31 C32 123.0(16) . .
C36 C31 N1 118.6(17) . .
C32 C31 N1 118.2(16) . .
C33 C32 C31 117.2(17) . .
C33 C32 C37 121.3(18) . .
C31 C32 C37 121.5(16) . .
C32 C33 C34 121.5(19) . .
C35 C34 C33 119.2(18) . .
C35 C34 C38 122(2) . .
C33 C34 C38 119(2) . .
C34 C35 C36 121.4(19) . .
C31 C36 C35 117.7(18) . .
C31 C36 C39 121.7(17) . .
C35 C36 C39 120.6(17) . .
C42 C41 C46 122.2(15) . .
C42 C41 N2 119.5(14) . .
C46 C41 N2 118.1(16) . .
C41 C42 C43 117.6(16) . .
C41 C42 C47 122.7(15) . .
C43 C42 C47 119.6(17) . .
C44 C43 C42 123(2) . .
C43 C44 C45 116.9(18) . .
C43 C44 C48 123(3) . .
C45 C44 C48 121(2) . .
C46 C45 C44 123.1(19) . .
C45 C46 C41 116.6(19) . .
C45 C46 C49 123.8(19) . .
C41 C46 C49 119.5(19) . .
C56 C51 C52 122.9(15) . .
C56 C51 N3 120.2(14) . .
C52 C51 N3 116.7(15) . .
C53 C52 C51 117.0(16) . .
C53 C52 C57 121.3(16) . .
C51 C52 C57 121.5(15) . .
C52 C53 C54 122.2(16) . .
C55 C54 C53 118.8(16) . .
C55 C54 C58 120.0(18) . .
C53 C54 C58 121.2(17) . .
C54 C55 C56 121.3(16) . .
C55 C56 C51 117.6(15) . .
C55 C56 C59 119.6(16) . .
C51 C56 C59 122.7(15) . .
C66 C61 C62 123.2(15) . .
C66 C61 N4 118.1(15) . .
C62 C61 N4 118.4(15) . .
C63 C62 C61 117.3(17) . .
C63 C62 C67 120.9(18) . .
C61 C62 C67 121.7(16) . .
C62 C63 C64 122(2) . .
C65 C64 C63 118.2(18) . .
C65 C64 C68 122(2) . .
C63 C64 C68 120(2) . .
C64 C65 C66 122.1(19) . .
C61 C66 C65 116.9(18) . .
C61 C66 C69 121.8(16) . .
C65 C66 C69 121.3(17) . .
Cl1S C1S Cl2S 111.9(12) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 S2 2.399(3) .
Re1 S3 2.401(3) .
Re1 S4 2.410(3) .
Re1 S1 2.419(3) .
Re1 Cl1 2.420(3) .
Re1 Re4 2.5819(7) .
Re1 Re2 2.5954(7) .
Re1 Re6 2.6070(7) .
Re1 Re5 2.6115(7) .
Re2 S8 2.395(4) .
Re2 S5 2.398(3) .
Re2 S4 2.403(3) .
Re2 S1 2.405(3) .
Re2 Cl2 2.421(4) .
Re2 Re3 2.6040(7) .
Re2 Re5 2.6063(7) .
Re2 Re6 2.6068(7) .
Re3 S8 2.390(4) .
Re3 S5 2.395(3) .
Re3 S7 2.423(4) .
Re3 S6 2.429(4) .
Re3 P1A 2.477(19) .
Re3 P1B 2.48(2) .
Re3 Re4 2.5954(8) .
Re3 Re5 2.6194(7) .
Re3 Re6 2.6197(7) .
Re4 S2 2.384(3) .
Re4 S3 2.388(3) .
Re4 S7 2.416(4) .
Re4 S6 2.418(4) .
Re4 P2B 2.496(10) .
Re4 P2A 2.504(7) .
Re4 Re5 2.6272(7) .
Re4 Re6 2.6326(7) .
Re5 C1 2.213(15) .
Re5 S2 2.397(3) .
Re5 S1 2.412(3) .
Re5 S5 2.420(3) .
Re5 S6 2.431(4) .
Re6 C4 2.203(14) .
Re6 S4 2.406(3) .
Re6 S3 2.407(3) .
Re6 S8 2.413(4) .
Re6 S7 2.419(4) .
P1A C11A 1.829(17) .
P1A C13A 1.837(16) .
P1A C15A 1.839(17) .
P1B C11B 1.830(17) .
P1B C15B 1.832(17) .
P1B C13B 1.833(16) .
P2A C21A 1.835(17) .
P2A C25A 1.839(17) .
P2A C23A 1.841(17) .
P2B C21B 1.826(18) .
P2B C23B 1.836(18) .
P2B C25B 1.841(17) .
N1 C1 1.375(19) .
N1 C2 1.40(2) .
N1 C31 1.46(2) .
N2 C1 1.382(19) .
N2 C3 1.389(19) .
N2 C41 1.449(19) .
N3 C5 1.37(2) .
N3 C4 1.387(19) .
N3 C51 1.45(2) .
N4 C6 1.377(18) .
N4 C4 1.384(18) .
N4 C61 1.459(19) .
C2 C3 1.33(3) .
C5 C6 1.33(2) .
C11A C12A 1.51(2) .
C13A C14A 1.51(2) .
C15A C16A 1.51(2) .
C11B C12B 1.51(2) .
C13B C14B 1.51(2) .
C15B C16B 1.51(2) .
C21A C22A 1.51(2) .
C23A C24A 1.51(2) .
C25A C26A 1.51(2) .
C21B C22B 1.51(2) .
C23B C24B 1.51(2) .
C25B C26B 1.51(2) .
C31 C36 1.38(2) .
C31 C32 1.39(3) .
C32 C33 1.38(2) .
C32 C37 1.49(3) .
C33 C34 1.39(3) .
C34 C35 1.37(3) .
C34 C38 1.51(3) .
C35 C36 1.39(2) .
C36 C39 1.53(3) .
C41 C42 1.39(2) .
C41 C46 1.40(2) .
C42 C43 1.39(2) .
C42 C47 1.48(2) .
C43 C44 1.37(3) .
C44 C45 1.40(4) .
C44 C48 1.49(3) .
C45 C46 1.40(3) .
C46 C49 1.49(3) .
C51 C56 1.39(2) .
C51 C52 1.39(2) .
C52 C53 1.38(2) .
C52 C57 1.51(2) .
C53 C54 1.39(3) .
C54 C55 1.38(2) .
C54 C58 1.52(2) .
C55 C56 1.39(2) .
C56 C59 1.51(2) .
C61 C66 1.39(2) .
C61 C62 1.39(2) .
C62 C63 1.37(2) .
C62 C67 1.50(3) .
C63 C64 1.39(3) .
C64 C65 1.38(3) .
C64 C68 1.52(3) .
C65 C66 1.39(3) .
C66 C69 1.51(3) .
Cl1S C1S 1.72(3) .
Cl2S C1S 1.77(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
S2 Re1 Re2 S8 -104.54(14) . . . .
S3 Re1 Re2 S8 0.73(14) . . . .
S4 Re1 Re2 S8 71.82(15) . . . .
S1 Re1 Re2 S8 -175.37(14) . . . .
Cl1 Re1 Re2 S8 127.21(18) . . . .
Re4 Re1 Re2 S8 -51.90(11) . . . .
Re6 Re1 Re2 S8 3.78(11) . . . .
Re5 Re1 Re2 S8 -107.32(11) . . . .
S2 Re1 Re2 S5 -1.04(13) . . . .
S3 Re1 Re2 S5 104.22(12) . . . .
S4 Re1 Re2 S5 175.32(14) . . . .
S1 Re1 Re2 S5 -71.88(13) . . . .
Cl1 Re1 Re2 S5 -129.29(17) . . . .
Re4 Re1 Re2 S5 51.59(9) . . . .
Re6 Re1 Re2 S5 107.28(9) . . . .
Re5 Re1 Re2 S5 -3.82(9) . . . .
S2 Re1 Re2 S4 -176.36(13) . . . .
S3 Re1 Re2 S4 -71.09(13) . . . .
S1 Re1 Re2 S4 112.80(13) . . . .
Cl1 Re1 Re2 S4 55.39(18) . . . .
Re4 Re1 Re2 S4 -123.72(10) . . . .
Re6 Re1 Re2 S4 -68.04(10) . . . .
Re5 Re1 Re2 S4 -179.14(10) . . . .
S2 Re1 Re2 S1 70.84(13) . . . .
S3 Re1 Re2 S1 176.10(12) . . . .
S4 Re1 Re2 S1 -112.80(13) . . . .
Cl1 Re1 Re2 S1 -57.41(17) . . . .
Re4 Re1 Re2 S1 123.47(9) . . . .
Re6 Re1 Re2 S1 179.16(9) . . . .
Re5 Re1 Re2 S1 68.05(9) . . . .
S2 Re1 Re2 Cl2 127.62(17) . . . .
S3 Re1 Re2 Cl2 -127.11(16) . . . .
S4 Re1 Re2 Cl2 -56.02(17) . . . .
S1 Re1 Re2 Cl2 56.78(17) . . . .
Cl1 Re1 Re2 Cl2 -0.6(2) . . . .
Re4 Re1 Re2 Cl2 -179.74(14) . . . .
Re6 Re1 Re2 Cl2 -124.06(14) . . . .
Re5 Re1 Re2 Cl2 124.84(14) . . . .
S2 Re1 Re2 Re3 -52.79(9) . . . .
S3 Re1 Re2 Re3 52.47(9) . . . .
S4 Re1 Re2 Re3 123.57(10) . . . .
S1 Re1 Re2 Re3 -123.63(9) . . . .
Cl1 Re1 Re2 Re3 178.96(15) . . . .
Re4 Re1 Re2 Re3 -0.16(2) . . . .
Re6 Re1 Re2 Re3 55.53(2) . . . .
Re5 Re1 Re2 Re3 -55.57(2) . . . .
S2 Re1 Re2 Re5 2.78(9) . . . .
S3 Re1 Re2 Re5 108.05(9) . . . .
S4 Re1 Re2 Re5 179.14(10) . . . .
S1 Re1 Re2 Re5 -68.05(9) . . . .
Cl1 Re1 Re2 Re5 -125.47(15) . . . .
Re4 Re1 Re2 Re5 55.42(2) . . . .
Re6 Re1 Re2 Re5 111.10(2) . . . .
S2 Re1 Re2 Re6 -108.32(9) . . . .
S3 Re1 Re2 Re6 -3.06(8) . . . .
S4 Re1 Re2 Re6 68.04(10) . . . .
S1 Re1 Re2 Re6 -179.16(9) . . . .
Cl1 Re1 Re2 Re6 123.43(15) . . . .
Re4 Re1 Re2 Re6 -55.69(2) . . . .
Re5 Re1 Re2 Re6 -111.10(2) . . . .
S5 Re2 Re3 S8 112.08(14) . . . .
S4 Re2 Re3 S8 -71.39(14) . . . .
S1 Re2 Re3 S8 -176.43(13) . . . .
Cl2 Re2 Re3 S8 55.76(18) . . . .
Re1 Re2 Re3 S8 -123.81(10) . . . .
Re5 Re2 Re3 S8 -179.31(10) . . . .
Re6 Re2 Re3 S8 -68.45(10) . . . .
S8 Re2 Re3 S5 -112.08(14) . . . .
S4 Re2 Re3 S5 176.54(13) . . . .
S1 Re2 Re3 S5 71.49(13) . . . .
Cl2 Re2 Re3 S5 -56.32(18) . . . .
Re1 Re2 Re3 S5 124.12(10) . . . .
Re5 Re2 Re3 S5 68.62(10) . . . .
Re6 Re2 Re3 S5 179.47(10) . . . .
S8 Re2 Re3 S7 71.15(15) . . . .
S5 Re2 Re3 S7 -176.77(15) . . . .
S4 Re2 Re3 S7 -0.23(15) . . . .
S1 Re2 Re3 S7 -105.27(14) . . . .
Cl2 Re2 Re3 S7 126.91(19) . . . .
Re1 Re2 Re3 S7 -52.65(12) . . . .
Re5 Re2 Re3 S7 -108.15(12) . . . .
Re6 Re2 Re3 S7 2.70(11) . . . .
S8 Re2 Re3 S6 176.63(15) . . . .
S5 Re2 Re3 S6 -71.29(14) . . . .
S4 Re2 Re3 S6 105.25(14) . . . .
S1 Re2 Re3 S6 0.20(14) . . . .
Cl2 Re2 Re3 S6 -127.61(18) . . . .
Re1 Re2 Re3 S6 52.83(11) . . . .
Re5 Re2 Re3 S6 -2.67(11) . . . .
Re6 Re2 Re3 S6 108.18(11) . . . .
S8 Re2 Re3 P1A -56.5(6) . . . .
S5 Re2 Re3 P1A 55.6(6) . . . .
S4 Re2 Re3 P1A -127.8(6) . . . .
S1 Re2 Re3 P1A 127.1(6) . . . .
Cl2 Re2 Re3 P1A -0.7(6) . . . .
Re1 Re2 Re3 P1A 179.7(6) . . . .
Re5 Re2 Re3 P1A 124.2(6) . . . .
Re6 Re2 Re3 P1A -124.9(6) . . . .
S8 Re2 Re3 P1B -61.0(8) . . . .
S5 Re2 Re3 P1B 51.1(8) . . . .
S4 Re2 Re3 P1B -132.4(8) . . . .
S1 Re2 Re3 P1B 122.6(8) . . . .
Cl2 Re2 Re3 P1B -5.3(8) . . . .
Re1 Re2 Re3 P1B 175.2(8) . . . .
Re5 Re2 Re3 P1B 119.7(8) . . . .
Re6 Re2 Re3 P1B -129.5(8) . . . .
S8 Re2 Re3 Re4 123.96(10) . . . .
S5 Re2 Re3 Re4 -123.96(10) . . . .
S4 Re2 Re3 Re4 52.58(9) . . . .
S1 Re2 Re3 Re4 -52.47(9) . . . .
Cl2 Re2 Re3 Re4 179.72(15) . . . .
Re1 Re2 Re3 Re4 0.16(2) . . . .
Re5 Re2 Re3 Re4 -55.34(2) . . . .
Re6 Re2 Re3 Re4 55.51(2) . . . .
S8 Re2 Re3 Re5 179.31(10) . . . .
S5 Re2 Re3 Re5 -68.62(10) . . . .
S4 Re2 Re3 Re5 107.92(9) . . . .
S1 Re2 Re3 Re5 2.88(9) . . . .
Cl2 Re2 Re3 Re5 -124.94(15) . . . .
Re1 Re2 Re3 Re5 55.50(2) . . . .
Re6 Re2 Re3 Re5 110.85(2) . . . .
S8 Re2 Re3 Re6 68.45(10) . . . .
S5 Re2 Re3 Re6 -179.47(10) . . . .
S4 Re2 Re3 Re6 -2.93(9) . . . .
S1 Re2 Re3 Re6 -107.98(9) . . . .
Cl2 Re2 Re3 Re6 124.21(15) . . . .
Re1 Re2 Re3 Re6 -55.35(2) . . . .
Re5 Re2 Re3 Re6 -110.85(2) . . . .
S3 Re1 Re4 S2 114.76(13) . . . .
S4 Re1 Re4 S2 -174.85(13) . . . .
S1 Re1 Re4 S2 -69.94(13) . . . .
Cl1 Re1 Re4 S2 58.36(16) . . . .
Re2 Re1 Re4 S2 -122.42(9) . . . .
Re6 Re1 Re4 S2 -177.42(10) . . . .
Re5 Re1 Re4 S2 -67.57(9) . . . .
S2 Re1 Re4 S3 -114.76(13) . . . .
S4 Re1 Re4 S3 70.38(13) . . . .
S1 Re1 Re4 S3 175.30(13) . . . .
Cl1 Re1 Re4 S3 -56.41(16) . . . .
Re2 Re1 Re4 S3 122.82(9) . . . .
Re6 Re1 Re4 S3 67.81(9) . . . .
Re5 Re1 Re4 S3 177.66(9) . . . .
S2 Re1 Re4 S7 175.75(14) . . . .
S3 Re1 Re4 S7 -69.48(14) . . . .
S4 Re1 Re4 S7 0.90(14) . . . .
S1 Re1 Re4 S7 105.81(14) . . . .
Cl1 Re1 Re4 S7 -125.89(17) . . . .
Re2 Re1 Re4 S7 53.33(11) . . . .
Re6 Re1 Re4 S7 -1.67(11) . . . .
Re5 Re1 Re4 S7 108.18(11) . . . .
S2 Re1 Re4 S6 69.43(15) . . . .
S3 Re1 Re4 S6 -175.81(15) . . . .
S4 Re1 Re4 S6 -105.43(15) . . . .
S1 Re1 Re4 S6 -0.51(15) . . . .
Cl1 Re1 Re4 S6 127.78(17) . . . .
Re2 Re1 Re4 S6 -52.99(12) . . . .
Re6 Re1 Re4 S6 -108.00(12) . . . .
Re5 Re1 Re4 S6 1.85(12) . . . .
S2 Re1 Re4 P2B -53.2(9) . . . .
S3 Re1 Re4 P2B 61.6(9) . . . .
S4 Re1 Re4 P2B 131.9(9) . . . .
S1 Re1 Re4 P2B -123.2(9) . . . .
Cl1 Re1 Re4 P2B 5.1(9) . . . .
Re2 Re1 Re4 P2B -175.6(9) . . . .
Re6 Re1 Re4 P2B 129.4(9) . . . .
Re5 Re1 Re4 P2B -120.8(9) . . . .
S2 Re1 Re4 P2A -56.2(5) . . . .
S3 Re1 Re4 P2A 58.5(5) . . . .
S4 Re1 Re4 P2A 128.9(5) . . . .
S1 Re1 Re4 P2A -126.2(5) . . . .
Cl1 Re1 Re4 P2A 2.1(5) . . . .
Re2 Re1 Re4 P2A -178.7(5) . . . .
Re6 Re1 Re4 P2A 126.3(5) . . . .
Re5 Re1 Re4 P2A -123.8(5) . . . .
S2 Re1 Re4 Re3 122.57(9) . . . .
S3 Re1 Re4 Re3 -122.66(9) . . . .
S4 Re1 Re4 Re3 -52.28(9) . . . .
S1 Re1 Re4 Re3 52.64(9) . . . .
Cl1 Re1 Re4 Re3 -179.07(13) . . . .
Re2 Re1 Re4 Re3 0.16(2) . . . .
Re6 Re1 Re4 Re3 -54.85(2) . . . .
Re5 Re1 Re4 Re3 55.00(2) . . . .
S2 Re1 Re4 Re5 67.57(9) . . . .
S3 Re1 Re4 Re5 -177.66(9) . . . .
S4 Re1 Re4 Re5 -107.28(9) . . . .
S1 Re1 Re4 Re5 -2.37(9) . . . .
Cl1 Re1 Re4 Re5 125.93(13) . . . .
Re2 Re1 Re4 Re5 -54.84(2) . . . .
Re6 Re1 Re4 Re5 -109.85(2) . . . .
S2 Re1 Re4 Re6 177.42(10) . . . .
S3 Re1 Re4 Re6 -67.81(9) . . . .
S4 Re1 Re4 Re6 2.57(9) . . . .
S1 Re1 Re4 Re6 107.48(9) . . . .
Cl1 Re1 Re4 Re6 -124.22(13) . . . .
Re2 Re1 Re4 Re6 55.01(2) . . . .
Re5 Re1 Re4 Re6 109.85(2) . . . .
S8 Re3 Re4 S2 104.96(14) . . . .
S5 Re3 Re4 S2 0.85(13) . . . .
S7 Re3 Re4 S2 175.53(14) . . . .
S6 Re3 Re4 S2 -70.02(14) . . . .
P1A Re3 Re4 S2 -126.6(7) . . . .
P1B Re3 Re4 S2 -123.2(6) . . . .
Re2 Re3 Re4 S2 52.91(9) . . . .
Re5 Re3 Re4 S2 -1.91(9) . . . .
Re6 Re3 Re4 S2 107.79(9) . . . .
S8 Re3 Re4 S3 -1.13(14) . . . .
S5 Re3 Re4 S3 -105.25(13) . . . .
S7 Re3 Re4 S3 69.44(14) . . . .
S6 Re3 Re4 S3 -176.11(13) . . . .
P1A Re3 Re4 S3 127.3(7) . . . .
P1B Re3 Re4 S3 130.7(6) . . . .
Re2 Re3 Re4 S3 -53.18(9) . . . .
Re5 Re3 Re4 S3 -108.00(9) . . . .
Re6 Re3 Re4 S3 1.70(8) . . . .
S8 Re3 Re4 S7 -70.57(16) . . . .
S5 Re3 Re4 S7 -174.69(15) . . . .
S6 Re3 Re4 S7 114.45(15) . . . .
P1A Re3 Re4 S7 57.9(7) . . . .
P1B Re3 Re4 S7 61.3(6) . . . .
Re2 Re3 Re4 S7 -122.62(11) . . . .
Re5 Re3 Re4 S7 -177.44(11) . . . .
Re6 Re3 Re4 S7 -67.74(11) . . . .
S8 Re3 Re4 S6 174.98(15) . . . .
S5 Re3 Re4 S6 70.86(14) . . . .
S7 Re3 Re4 S6 -114.45(15) . . . .
P1A Re3 Re4 S6 -56.6(7) . . . .
P1B Re3 Re4 S6 -53.1(6) . . . .
Re2 Re3 Re4 S6 122.93(10) . . . .
Re5 Re3 Re4 S6 68.11(10) . . . .
Re6 Re3 Re4 S6 177.81(10) . . . .
S8 Re3 Re4 P2B -132.7(10) . . . .
S5 Re3 Re4 P2B 123.2(10) . . . .
S7 Re3 Re4 P2B -62.1(10) . . . .
S6 Re3 Re4 P2B 52.3(10) . . . .
P1B Re3 Re4 P2B -0.8(12) . . . .
Re2 Re3 Re4 P2B 175.3(10) . . . .
Re5 Re3 Re4 P2B 120.4(10) . . . .
Re6 Re3 Re4 P2B -129.9(10) . . . .
S8 Re3 Re4 P2A -129.9(7) . . . .
S5 Re3 Re4 P2A 126.0(7) . . . .
S7 Re3 Re4 P2A -59.3(7) . . . .
S6 Re3 Re4 P2A 55.1(7) . . . .
P1A Re3 Re4 P2A -1.5(10) . . . .
Re2 Re3 Re4 P2A 178.1(7) . . . .
Re5 Re3 Re4 P2A 123.3(7) . . . .
Re6 Re3 Re4 P2A -127.1(7) . . . .
S8 Re3 Re4 Re1 51.89(11) . . . .
S5 Re3 Re4 Re1 -52.22(9) . . . .
S7 Re3 Re4 Re1 122.46(11) . . . .
S6 Re3 Re4 Re1 -123.09(10) . . . .
P1A Re3 Re4 Re1 -179.7(7) . . . .
P1B Re3 Re4 Re1 -176.2(6) . . . .
Re2 Re3 Re4 Re1 -0.16(2) . . . .
Re5 Re3 Re4 Re1 -54.98(2) . . . .
Re6 Re3 Re4 Re1 54.72(2) . . . .
S8 Re3 Re4 Re5 106.87(11) . . . .
S5 Re3 Re4 Re5 2.75(9) . . . .
S7 Re3 Re4 Re5 177.44(11) . . . .
S6 Re3 Re4 Re5 -68.11(10) . . . .
P1A Re3 Re4 Re5 -124.7(7) . . . .
P1B Re3 Re4 Re5 -121.3(6) . . . .
Re2 Re3 Re4 Re5 54.82(2) . . . .
Re6 Re3 Re4 Re5 109.70(2) . . . .
S8 Re3 Re4 Re6 -2.83(11) . . . .
S5 Re3 Re4 Re6 -106.95(9) . . . .
S7 Re3 Re4 Re6 67.74(11) . . . .
S6 Re3 Re4 Re6 -177.81(10) . . . .
P1A Re3 Re4 Re6 125.6(7) . . . .
P1B Re3 Re4 Re6 129.0(6) . . . .
Re2 Re3 Re4 Re6 -54.88(2) . . . .
Re5 Re3 Re4 Re6 -109.70(2) . . . .
S8 Re2 Re5 C1 -131.9(5) . . . .
S5 Re2 Re5 C1 -63.7(5) . . . .
S4 Re2 Re5 C1 121.2(5) . . . .
S1 Re2 Re5 C1 51.7(5) . . . .
Cl2 Re2 Re5 C1 -3.2(5) . . . .
Re1 Re2 Re5 C1 120.3(5) . . . .
Re3 Re2 Re5 C1 -131.3(5) . . . .
Re6 Re2 Re5 C1 174.4(5) . . . .
S8 Re2 Re5 S2 104.94(13) . . . .
S5 Re2 Re5 S2 173.22(13) . . . .
S4 Re2 Re5 S2 -1.96(13) . . . .
S1 Re2 Re5 S2 -71.38(13) . . . .
Cl2 Re2 Re5 S2 -126.32(18) . . . .
Re1 Re2 Re5 S2 -2.78(9) . . . .
Re3 Re2 Re5 S2 105.60(9) . . . .
Re6 Re2 Re5 S2 51.26(9) . . . .
S8 Re2 Re5 S1 176.32(13) . . . .
S5 Re2 Re5 S1 -115.40(13) . . . .
S4 Re2 Re5 S1 69.42(13) . . . .
Cl2 Re2 Re5 S1 -54.94(18) . . . .
Re1 Re2 Re5 S1 68.60(9) . . . .
Re3 Re2 Re5 S1 176.97(9) . . . .
Re6 Re2 Re5 S1 122.64(9) . . . .
S8 Re2 Re5 S5 -68.28(13) . . . .
S4 Re2 Re5 S5 -175.18(14) . . . .
S1 Re2 Re5 S5 115.40(13) . . . .
Cl2 Re2 Re5 S5 60.46(18) . . . .
Re1 Re2 Re5 S5 -176.00(10) . . . .
Re3 Re2 Re5 S5 -67.62(10) . . . .
Re6 Re2 Re5 S5 -121.96(10) . . . .
S8 Re2 Re5 S6 2.02(14) . . . .
S5 Re2 Re5 S6 70.29(14) . . . .
S4 Re2 Re5 S6 -104.89(14) . . . .
S1 Re2 Re5 S6 -174.30(14) . . . .
Cl2 Re2 Re5 S6 130.76(18) . . . .
Re1 Re2 Re5 S6 -105.71(11) . . . .
Re3 Re2 Re5 S6 2.67(11) . . . .
Re6 Re2 Re5 S6 -51.67(11) . . . .
S8 Re2 Re5 Re1 107.72(10) . . . .
S5 Re2 Re5 Re1 176.00(10) . . . .
S4 Re2 Re5 Re1 0.82(10) . . . .
S1 Re2 Re5 Re1 -68.60(9) . . . .
Cl2 Re2 Re5 Re1 -123.54(15) . . . .
Re3 Re2 Re5 Re1 108.38(2) . . . .
Re6 Re2 Re5 Re1 54.04(2) . . . .
S8 Re2 Re5 Re3 -0.65(10) . . . .
S5 Re2 Re5 Re3 67.62(10) . . . .
S4 Re2 Re5 Re3 -107.56(10) . . . .
S1 Re2 Re5 Re3 -176.97(9) . . . .
Cl2 Re2 Re5 Re3 128.09(15) . . . .
Re1 Re2 Re5 Re3 -108.38(2) . . . .
Re6 Re2 Re5 Re3 -54.34(2) . . . .
S8 Re2 Re5 Re4 53.71(10) . . . .
S5 Re2 Re5 Re4 121.98(10) . . . .
S4 Re2 Re5 Re4 -53.20(10) . . . .
S1 Re2 Re5 Re4 -122.61(9) . . . .
Cl2 Re2 Re5 Re4 -177.55(15) . . . .
Re1 Re2 Re5 Re4 -54.02(2) . . . .
Re3 Re2 Re5 Re4 54.36(2) . . . .
Re6 Re2 Re5 Re4 0.02(2) . . . .
S2 Re1 Re5 C1 63.2(5) . . . .
S3 Re1 Re5 C1 133.1(5) . . . .
S4 Re1 Re5 C1 -120.6(5) . . . .
S1 Re1 Re5 C1 -51.6(5) . . . .
Cl1 Re1 Re5 C1 10.6(6) . . . .
Re4 Re1 Re5 C1 130.9(5) . . . .
Re2 Re1 Re5 C1 -119.8(5) . . . .
Re6 Re1 Re5 C1 -173.8(5) . . . .
S3 Re1 Re5 S2 69.89(13) . . . .
S4 Re1 Re5 S2 176.23(13) . . . .
S1 Re1 Re5 S2 -114.82(13) . . . .
Cl1 Re1 Re5 S2 -52.54(16) . . . .
Re4 Re1 Re5 S2 67.67(10) . . . .
Re2 Re1 Re5 S2 177.04(10) . . . .
Re6 Re1 Re5 S2 123.02(10) . . . .
S2 Re1 Re5 S1 114.82(13) . . . .
S3 Re1 Re5 S1 -175.29(13) . . . .
S4 Re1 Re5 S1 -68.95(13) . . . .
Cl1 Re1 Re5 S1 62.28(16) . . . .
Re4 Re1 Re5 S1 -177.51(9) . . . .
Re2 Re1 Re5 S1 -68.13(9) . . . .
Re6 Re1 Re5 S1 -122.16(9) . . . .
S2 Re1 Re5 S5 -173.30(13) . . . .
S3 Re1 Re5 S5 -103.41(13) . . . .
S4 Re1 Re5 S5 2.93(13) . . . .
S1 Re1 Re5 S5 71.88(13) . . . .
Cl1 Re1 Re5 S5 134.16(16) . . . .
Re4 Re1 Re5 S5 -105.63(9) . . . .
Re2 Re1 Re5 S5 3.74(9) . . . .
Re6 Re1 Re5 S5 -50.28(9) . . . .
S2 Re1 Re5 S6 -69.49(15) . . . .
S3 Re1 Re5 S6 0.40(15) . . . .
S4 Re1 Re5 S6 106.74(15) . . . .
S1 Re1 Re5 S6 175.69(14) . . . .
Cl1 Re1 Re5 S6 -122.03(17) . . . .
Re4 Re1 Re5 S6 -1.82(11) . . . .
Re2 Re1 Re5 S6 107.56(11) . . . .
Re6 Re1 Re5 S6 53.53(11) . . . .
S2 Re1 Re5 Re2 -177.04(10) . . . .
S3 Re1 Re5 Re2 -107.15(9) . . . .
S4 Re1 Re5 Re2 -0.81(10) . . . .
S1 Re1 Re5 Re2 68.13(9) . . . .
Cl1 Re1 Re5 Re2 130.42(13) . . . .
Re4 Re1 Re5 Re2 -109.37(2) . . . .
Re6 Re1 Re5 Re2 -54.03(2) . . . .
S2 Re1 Re5 Re3 -121.94(10) . . . .
S3 Re1 Re5 Re3 -52.05(9) . . . .
S4 Re1 Re5 Re3 54.29(10) . . . .
S1 Re1 Re5 Re3 123.23(9) . . . .
Cl1 Re1 Re5 Re3 -174.48(13) . . . .
Re4 Re1 Re5 Re3 -54.27(2) . . . .
Re2 Re1 Re5 Re3 55.10(2) . . . .
Re6 Re1 Re5 Re3 1.07(2) . . . .
S2 Re1 Re5 Re4 -67.67(10) . . . .
S3 Re1 Re5 Re4 2.22(9) . . . .
S4 Re1 Re5 Re4 108.56(10) . . . .
S1 Re1 Re5 Re4 177.51(9) . . . .
Cl1 Re1 Re5 Re4 -120.21(13) . . . .
Re2 Re1 Re5 Re4 109.37(2) . . . .
Re6 Re1 Re5 Re4 55.35(2) . . . .
S8 Re3 Re5 C1 119.7(6) . . . .
S5 Re3 Re5 C1 51.0(6) . . . .
S7 Re3 Re5 C1 -134.3(6) . . . .
S6 Re3 Re5 C1 -63.8(6) . . . .
P1A Re3 Re5 C1 -0.3(8) . . . .
P1B Re3 Re5 C1 -15.1(8) . . . .
Re4 Re3 Re5 C1 -131.9(6) . . . .
Re2 Re3 Re5 C1 119.1(6) . . . .
Re6 Re3 Re5 C1 173.0(6) . . . .
S8 Re3 Re5 S2 -106.55(13) . . . .
S5 Re3 Re5 S2 -175.25(13) . . . .
S7 Re3 Re5 S2 -0.57(14) . . . .
S6 Re3 Re5 S2 69.97(14) . . . .
P1A Re3 Re5 S2 133.4(5) . . . .
P1B Re3 Re5 S2 118.6(5) . . . .
Re4 Re3 Re5 S2 1.87(9) . . . .
Re2 Re3 Re5 S2 -107.20(9) . . . .
Re6 Re3 Re5 S2 -53.27(9) . . . .
S8 Re3 Re5 S1 -2.19(13) . . . .
S5 Re3 Re5 S1 -70.89(13) . . . .
S7 Re3 Re5 S1 103.79(14) . . . .
S6 Re3 Re5 S1 174.33(14) . . . .
P1A Re3 Re5 S1 -122.2(5) . . . .
P1B Re3 Re5 S1 -137.1(5) . . . .
Re4 Re3 Re5 S1 106.23(9) . . . .
Re2 Re3 Re5 S1 -2.85(9) . . . .
Re6 Re3 Re5 S1 51.09(9) . . . .
S8 Re3 Re5 S5 68.70(13) . . . .
S7 Re3 Re5 S5 174.67(15) . . . .
S6 Re3 Re5 S5 -114.78(15) . . . .
P1A Re3 Re5 S5 -51.3(5) . . . .
P1B Re3 Re5 S5 -66.2(5) . . . .
Re4 Re3 Re5 S5 177.12(10) . . . .
Re2 Re3 Re5 S5 68.04(10) . . . .
Re6 Re3 Re5 S5 121.97(10) . . . .
S8 Re3 Re5 S6 -176.52(15) . . . .
S5 Re3 Re5 S6 114.78(15) . . . .
S7 Re3 Re5 S6 -70.54(15) . . . .
P1A Re3 Re5 S6 63.4(5) . . . .
P1B Re3 Re5 S6 48.6(5) . . . .
Re4 Re3 Re5 S6 -68.10(11) . . . .
Re2 Re3 Re5 S6 -177.18(11) . . . .
Re6 Re3 Re5 S6 -123.24(11) . . . .
S8 Re3 Re5 Re2 0.65(10) . . . .
S5 Re3 Re5 Re2 -68.04(10) . . . .
S7 Re3 Re5 Re2 106.63(11) . . . .
S6 Re3 Re5 Re2 177.18(11) . . . .
P1A Re3 Re5 Re2 -119.4(5) . . . .
P1B Re3 Re5 Re2 -134.2(4) . . . .
Re4 Re3 Re5 Re2 109.08(2) . . . .
Re6 Re3 Re5 Re2 53.93(2) . . . .
S8 Re3 Re5 Re1 -54.35(10) . . . .
S5 Re3 Re5 Re1 -123.04(10) . . . .
S7 Re3 Re5 Re1 51.63(11) . . . .
S6 Re3 Re5 Re1 122.18(11) . . . .
P1A Re3 Re5 Re1 -174.4(5) . . . .
P1B Re3 Re5 Re1 170.8(4) . . . .
Re4 Re3 Re5 Re1 54.07(2) . . . .
Re2 Re3 Re5 Re1 -55.001(19) . . . .
Re6 Re3 Re5 Re1 -1.07(2) . . . .
S8 Re3 Re5 Re4 -108.42(10) . . . .
S5 Re3 Re5 Re4 -177.12(10) . . . .
S7 Re3 Re5 Re4 -2.44(11) . . . .
S6 Re3 Re5 Re4 68.10(11) . . . .
P1A Re3 Re5 Re4 131.5(5) . . . .
P1B Re3 Re5 Re4 116.7(4) . . . .
Re2 Re3 Re5 Re4 -109.08(2) . . . .
Re6 Re3 Re5 Re4 -55.14(2) . . . .
S2 Re4 Re5 C1 -50.2(6) . . . .
S3 Re4 Re5 C1 -121.1(6) . . . .
S7 Re4 Re5 C1 134.3(6) . . . .
S6 Re4 Re5 C1 63.0(6) . . . .
P2B Re4 Re5 C1 3.2(9) . . . .
P2A Re4 Re5 C1 -8.9(7) . . . .
Re1 Re4 Re5 C1 -118.9(6) . . . .
Re3 Re4 Re5 C1 131.8(6) . . . .
Re6 Re4 Re5 C1 -173.4(6) . . . .
S3 Re4 Re5 S2 -70.94(13) . . . .
S7 Re4 Re5 S2 -175.53(14) . . . .
S6 Re4 Re5 S2 113.24(15) . . . .
P2B Re4 Re5 S2 53.4(6) . . . .
P2A Re4 Re5 S2 41.3(3) . . . .
Re1 Re4 Re5 S2 -68.71(9) . . . .
Re3 Re4 Re5 S2 -177.98(10) . . . .
Re6 Re4 Re5 S2 -123.24(10) . . . .
S2 Re4 Re5 S1 71.05(13) . . . .
S3 Re4 Re5 S1 0.11(13) . . . .
S7 Re4 Re5 S1 -104.47(14) . . . .
S6 Re4 Re5 S1 -175.71(15) . . . .
P2B Re4 Re5 S1 124.4(6) . . . .
P2A Re4 Re5 S1 112.3(3) . . . .
Re1 Re4 Re5 S1 2.34(9) . . . .
Re3 Re4 Re5 S1 -106.92(9) . . . .
Re6 Re4 Re5 S1 -52.19(9) . . . .
S2 Re4 Re5 S5 175.30(13) . . . .
S3 Re4 Re5 S5 104.36(13) . . . .
S7 Re4 Re5 S5 -0.22(14) . . . .
S6 Re4 Re5 S5 -71.46(15) . . . .
P2B Re4 Re5 S5 -131.3(6) . . . .
P2A Re4 Re5 S5 -143.4(3) . . . .
Re1 Re4 Re5 S5 106.59(9) . . . .
Re3 Re4 Re5 S5 -2.67(9) . . . .
Re6 Re4 Re5 S5 52.06(9) . . . .
S2 Re4 Re5 S6 -113.24(15) . . . .
S3 Re4 Re5 S6 175.82(15) . . . .
S7 Re4 Re5 S6 71.23(16) . . . .
P2B Re4 Re5 S6 -59.9(6) . . . .
P2A Re4 Re5 S6 -72.0(3) . . . .
Re1 Re4 Re5 S6 178.05(12) . . . .
Re3 Re4 Re5 S6 68.78(12) . . . .
Re6 Re4 Re5 S6 123.52(12) . . . .
S2 Re4 Re5 Re2 123.22(10) . . . .
S3 Re4 Re5 Re2 52.28(9) . . . .
S7 Re4 Re5 Re2 -52.31(11) . . . .
S6 Re4 Re5 Re2 -123.54(12) . . . .
P2B Re4 Re5 Re2 176.6(6) . . . .
P2A Re4 Re5 Re2 164.5(3) . . . .
Re1 Re4 Re5 Re2 54.51(2) . . . .
Re3 Re4 Re5 Re2 -54.76(2) . . . .
Re6 Re4 Re5 Re2 -0.02(2) . . . .
S2 Re4 Re5 Re1 68.71(9) . . . .
S3 Re4 Re5 Re1 -2.23(9) . . . .
S7 Re4 Re5 Re1 -106.82(11) . . . .
S6 Re4 Re5 Re1 -178.05(12) . . . .
P2B Re4 Re5 Re1 122.1(6) . . . .
P2A Re4 Re5 Re1 110.0(3) . . . .
Re3 Re4 Re5 Re1 -109.27(2) . . . .
Re6 Re4 Re5 Re1 -54.53(2) . . . .
S2 Re4 Re5 Re3 177.98(10) . . . .
S3 Re4 Re5 Re3 107.04(9) . . . .
S7 Re4 Re5 Re3 2.45(11) . . . .
S6 Re4 Re5 Re3 -68.78(12) . . . .
P2B Re4 Re5 Re3 -128.7(6) . . . .
P2A Re4 Re5 Re3 -140.8(3) . . . .
Re1 Re4 Re5 Re3 109.27(2) . . . .
Re6 Re4 Re5 Re3 54.73(2) . . . .
S8 Re2 Re6 C4 62.7(5) . . . .
S5 Re2 Re6 C4 130.7(5) . . . .
S4 Re2 Re6 C4 -52.9(5) . . . .
S1 Re2 Re6 C4 -122.1(5) . . . .
Cl2 Re2 Re6 C4 2.2(5) . . . .
Re1 Re2 Re6 C4 -121.3(5) . . . .
Re3 Re2 Re6 C4 130.2(5) . . . .
Re5 Re2 Re6 C4 -175.4(5) . . . .
S8 Re2 Re6 S4 115.54(15) . . . .
S5 Re2 Re6 S4 -176.41(13) . . . .
S1 Re2 Re6 S4 -69.24(13) . . . .
Cl2 Re2 Re6 S4 55.03(18) . . . .
Re1 Re2 Re6 S4 -68.44(10) . . . .
Re3 Re2 Re6 S4 -176.91(10) . . . .
Re5 Re2 Re6 S4 -122.57(10) . . . .
S8 Re2 Re6 S3 -172.99(14) . . . .
S5 Re2 Re6 S3 -104.94(12) . . . .
S4 Re2 Re6 S3 71.47(13) . . . .
S1 Re2 Re6 S3 2.23(12) . . . .
Cl2 Re2 Re6 S3 126.49(17) . . . .
Re1 Re2 Re6 S3 3.03(8) . . . .
Re3 Re2 Re6 S3 -105.44(9) . . . .
Re5 Re2 Re6 S3 -51.10(9) . . . .
S5 Re2 Re6 S8 68.05(15) . . . .
S4 Re2 Re6 S8 -115.54(15) . . . .
S1 Re2 Re6 S8 175.22(14) . . . .
Cl2 Re2 Re6 S8 -60.52(19) . . . .
Re1 Re2 Re6 S8 176.02(12) . . . .
Re3 Re2 Re6 S8 67.55(12) . . . .
Re5 Re2 Re6 S8 121.89(12) . . . .
S8 Re2 Re6 S7 -70.26(16) . . . .
S5 Re2 Re6 S7 -2.21(15) . . . .
S4 Re2 Re6 S7 174.20(15) . . . .
S1 Re2 Re6 S7 104.96(14) . . . .
Cl2 Re2 Re6 S7 -130.77(19) . . . .
Re1 Re2 Re6 S7 105.76(12) . . . .
Re3 Re2 Re6 S7 -2.71(12) . . . .
Re5 Re2 Re6 S7 51.63(12) . . . .
S8 Re2 Re6 Re1 -176.02(12) . . . .
S5 Re2 Re6 Re1 -107.97(9) . . . .
S4 Re2 Re6 Re1 68.44(10) . . . .
S1 Re2 Re6 Re1 -0.80(9) . . . .
Cl2 Re2 Re6 Re1 123.46(15) . . . .
Re3 Re2 Re6 Re1 -108.47(2) . . . .
Re5 Re2 Re6 Re1 -54.13(2) . . . .
S8 Re2 Re6 Re3 -67.55(12) . . . .
S5 Re2 Re6 Re3 0.50(9) . . . .
S4 Re2 Re6 Re3 176.91(10) . . . .
S1 Re2 Re6 Re3 107.67(9) . . . .
Cl2 Re2 Re6 Re3 -128.07(15) . . . .
Re1 Re2 Re6 Re3 108.47(2) . . . .
Re5 Re2 Re6 Re3 54.34(2) . . . .
S8 Re2 Re6 Re4 -121.91(12) . . . .
S5 Re2 Re6 Re4 -53.86(9) . . . .
S4 Re2 Re6 Re4 122.55(10) . . . .
S1 Re2 Re6 Re4 53.31(9) . . . .
Cl2 Re2 Re6 Re4 177.58(15) . . . .
Re1 Re2 Re6 Re4 54.11(2) . . . .
Re3 Re2 Re6 Re4 -54.36(2) . . . .
Re5 Re2 Re6 Re4 -0.02(2) . . . .
S2 Re1 Re6 C4 -133.2(5) . . . .
S3 Re1 Re6 C4 -63.1(5) . . . .
S4 Re1 Re6 C4 51.9(5) . . . .
S1 Re1 Re6 C4 120.9(5) . . . .
Cl1 Re1 Re6 C4 -10.3(5) . . . .
Re4 Re1 Re6 C4 -130.8(5) . . . .
Re2 Re1 Re6 C4 120.1(5) . . . .
Re5 Re1 Re6 C4 174.1(5) . . . .
S2 Re1 Re6 S4 174.85(13) . . . .
S3 Re1 Re6 S4 -115.09(13) . . . .
S1 Re1 Re6 S4 68.93(12) . . . .
Cl1 Re1 Re6 S4 -62.23(16) . . . .
Re4 Re1 Re6 S4 177.30(9) . . . .
Re2 Re1 Re6 S4 68.14(9) . . . .
Re5 Re1 Re6 S4 122.11(9) . . . .
S2 Re1 Re6 S3 -70.06(12) . . . .
S4 Re1 Re6 S3 115.09(13) . . . .
S1 Re1 Re6 S3 -175.98(12) . . . .
Cl1 Re1 Re6 S3 52.86(16) . . . .
Re4 Re1 Re6 S3 -67.61(9) . . . .
Re2 Re1 Re6 S3 -176.77(9) . . . .
Re5 Re1 Re6 S3 -122.80(9) . . . .
S2 Re1 Re6 S8 102.99(14) . . . .
S3 Re1 Re6 S8 173.05(14) . . . .
S4 Re1 Re6 S8 -71.86(14) . . . .
S1 Re1 Re6 S8 -2.92(14) . . . .
Cl1 Re1 Re6 S8 -134.09(17) . . . .
Re4 Re1 Re6 S8 105.44(11) . . . .
Re2 Re1 Re6 S8 -3.72(11) . . . .
Re5 Re1 Re6 S8 50.25(11) . . . .
S2 Re1 Re6 S7 -0.79(14) . . . .
S3 Re1 Re6 S7 69.27(14) . . . .
S4 Re1 Re6 S7 -175.64(14) . . . .
S1 Re1 Re6 S7 -106.71(14) . . . .
Cl1 Re1 Re6 S7 122.13(17) . . . .
Re4 Re1 Re6 S7 1.66(11) . . . .
Re2 Re1 Re6 S7 -107.51(11) . . . .
Re5 Re1 Re6 S7 -53.53(11) . . . .
S2 Re1 Re6 Re2 106.71(9) . . . .
S3 Re1 Re6 Re2 176.77(9) . . . .
S4 Re1 Re6 Re2 -68.14(9) . . . .
S1 Re1 Re6 Re2 0.80(9) . . . .
Cl1 Re1 Re6 Re2 -130.37(13) . . . .
Re4 Re1 Re6 Re2 109.16(2) . . . .
Re5 Re1 Re6 Re2 53.97(2) . . . .
S2 Re1 Re6 Re3 51.67(9) . . . .
S3 Re1 Re6 Re3 121.73(9) . . . .
S4 Re1 Re6 Re3 -123.18(9) . . . .
S1 Re1 Re6 Re3 -54.25(9) . . . .
Cl1 Re1 Re6 Re3 174.59(13) . . . .
Re4 Re1 Re6 Re3 54.12(2) . . . .
Re2 Re1 Re6 Re3 -55.05(2) . . . .
Re5 Re1 Re6 Re3 -1.07(2) . . . .
S2 Re1 Re6 Re4 -2.45(9) . . . .
S3 Re1 Re6 Re4 67.61(9) . . . .
S4 Re1 Re6 Re4 -177.30(9) . . . .
S1 Re1 Re6 Re4 -108.37(9) . . . .
Cl1 Re1 Re6 Re4 120.47(13) . . . .
Re2 Re1 Re6 Re4 -109.16(2) . . . .
Re5 Re1 Re6 Re4 -55.19(2) . . . .
S8 Re3 Re6 C4 -51.4(6) . . . .
S5 Re3 Re6 C4 -120.0(6) . . . .
S7 Re3 Re6 C4 63.3(6) . . . .
S6 Re3 Re6 C4 133.6(6) . . . .
P1A Re3 Re6 C4 -0.2(8) . . . .
P1B Re3 Re6 C4 15.6(7) . . . .
Re4 Re3 Re6 C4 131.5(6) . . . .
Re2 Re3 Re6 C4 -119.5(6) . . . .
Re5 Re3 Re6 C4 -173.4(6) . . . .
S8 Re3 Re6 S4 70.98(15) . . . .
S5 Re3 Re6 S4 2.41(13) . . . .
S7 Re3 Re6 S4 -174.23(15) . . . .
S6 Re3 Re6 S4 -103.97(13) . . . .
P1A Re3 Re6 S4 122.2(5) . . . .
P1B Re3 Re6 S4 138.0(5) . . . .
Re4 Re3 Re6 S4 -106.05(9) . . . .
Re2 Re3 Re6 S4 2.91(9) . . . .
Re5 Re3 Re6 S4 -51.02(9) . . . .
S8 Re3 Re6 S3 175.37(14) . . . .
S5 Re3 Re6 S3 106.80(12) . . . .
S7 Re3 Re6 S3 -69.84(14) . . . .
S6 Re3 Re6 S3 0.42(13) . . . .
P1A Re3 Re6 S3 -133.4(5) . . . .
P1B Re3 Re6 S3 -117.6(5) . . . .
Re4 Re3 Re6 S3 -1.66(8) . . . .
Re2 Re3 Re6 S3 107.30(8) . . . .
Re5 Re3 Re6 S3 53.37(8) . . . .
S5 Re3 Re6 S8 -68.57(14) . . . .
S7 Re3 Re6 S8 114.80(16) . . . .
S6 Re3 Re6 S8 -174.94(15) . . . .
P1A Re3 Re6 S8 51.3(5) . . . .
P1B Re3 Re6 S8 67.0(5) . . . .
Re4 Re3 Re6 S8 -177.03(11) . . . .
Re2 Re3 Re6 S8 -68.07(11) . . . .
Re5 Re3 Re6 S8 -122.00(11) . . . .
S8 Re3 Re6 S7 -114.80(17) . . . .
S5 Re3 Re6 S7 176.64(15) . . . .
S6 Re3 Re6 S7 70.26(15) . . . .
P1A Re3 Re6 S7 -63.5(5) . . . .
P1B Re3 Re6 S7 -47.8(5) . . . .
Re4 Re3 Re6 S7 68.17(12) . . . .
Re2 Re3 Re6 S7 177.13(12) . . . .
Re5 Re3 Re6 S7 123.21(12) . . . .
S8 Re3 Re6 Re2 68.07(11) . . . .
S5 Re3 Re6 Re2 -0.50(9) . . . .
S7 Re3 Re6 Re2 -177.13(12) . . . .
S6 Re3 Re6 Re2 -106.87(10) . . . .
P1A Re3 Re6 Re2 119.3(5) . . . .
P1B Re3 Re6 Re2 135.1(5) . . . .
Re4 Re3 Re6 Re2 -108.96(2) . . . .
Re5 Re3 Re6 Re2 -53.93(2) . . . .
S8 Re3 Re6 Re1 123.07(11) . . . .
S5 Re3 Re6 Re1 54.50(9) . . . .
S7 Re3 Re6 Re1 -122.14(12) . . . .
S6 Re3 Re6 Re1 -51.88(10) . . . .
P1A Re3 Re6 Re1 174.3(5) . . . .
P1B Re3 Re6 Re1 -169.9(5) . . . .
Re4 Re3 Re6 Re1 -53.97(2) . . . .
Re2 Re3 Re6 Re1 55.00(2) . . . .
Re5 Re3 Re6 Re1 1.07(2) . . . .
S8 Re3 Re6 Re4 177.03(11) . . . .
S5 Re3 Re6 Re4 108.46(9) . . . .
S7 Re3 Re6 Re4 -68.17(12) . . . .
S6 Re3 Re6 Re4 2.09(10) . . . .
P1A Re3 Re6 Re4 -131.7(5) . . . .
P1B Re3 Re6 Re4 -115.9(5) . . . .
Re2 Re3 Re6 Re4 108.96(2) . . . .
Re5 Re3 Re6 Re4 55.04(2) . . . .
S2 Re4 Re6 C4 122.5(6) . . . .
S3 Re4 Re6 C4 51.3(6) . . . .
S7 Re4 Re6 C4 -61.7(6) . . . .
S6 Re4 Re6 C4 -132.6(6) . . . .
P2B Re4 Re6 C4 -1.5(9) . . . .
P2A Re4 Re6 C4 10.8(7) . . . .
Re1 Re4 Re6 C4 120.0(6) . . . .
Re3 Re4 Re6 C4 -130.5(6) . . . .
Re5 Re4 Re6 C4 174.7(6) . . . .
S2 Re4 Re6 S4 -0.08(13) . . . .
S3 Re4 Re6 S4 -71.26(12) . . . .
S7 Re4 Re6 S4 175.69(14) . . . .
S6 Re4 Re6 S4 104.84(13) . . . .
P2B Re4 Re6 S4 -124.1(7) . . . .
P2A Re4 Re6 S4 -111.8(4) . . . .
Re1 Re4 Re6 S4 -2.53(9) . . . .
Re3 Re4 Re6 S4 106.93(9) . . . .
Re5 Re4 Re6 S4 52.15(9) . . . .
S2 Re4 Re6 S3 71.18(13) . . . .
S7 Re4 Re6 S3 -113.05(14) . . . .
S6 Re4 Re6 S3 176.10(13) . . . .
P2B Re4 Re6 S3 -52.8(7) . . . .
P2A Re4 Re6 S3 -40.5(4) . . . .
Re1 Re4 Re6 S3 68.73(9) . . . .
Re3 Re4 Re6 S3 178.20(9) . . . .
Re5 Re4 Re6 S3 123.41(9) . . . .
S2 Re4 Re6 S8 -104.27(14) . . . .
S3 Re4 Re6 S8 -175.45(14) . . . .
S7 Re4 Re6 S8 71.50(15) . . . .
S6 Re4 Re6 S8 0.65(15) . . . .
P2B Re4 Re6 S8 131.7(7) . . . .
P2A Re4 Re6 S8 144.0(4) . . . .
Re1 Re4 Re6 S8 -106.72(11) . . . .
Re3 Re4 Re6 S8 2.75(11) . . . .
Re5 Re4 Re6 S8 -52.04(11) . . . .
S2 Re4 Re6 S7 -175.77(15) . . . .
S3 Re4 Re6 S7 113.05(14) . . . .
S6 Re4 Re6 S7 -70.85(15) . . . .
P2B Re4 Re6 S7 60.2(7) . . . .
P2A Re4 Re6 S7 72.5(4) . . . .
Re1 Re4 Re6 S7 -178.22(11) . . . .
Re3 Re4 Re6 S7 -68.76(11) . . . .
Re5 Re4 Re6 S7 -123.54(11) . . . .
S2 Re4 Re6 Re2 -52.21(9) . . . .
S3 Re4 Re6 Re2 -123.39(9) . . . .
S7 Re4 Re6 Re2 123.56(11) . . . .
S6 Re4 Re6 Re2 52.71(10) . . . .
P2B Re4 Re6 Re2 -176.2(7) . . . .
P2A Re4 Re6 Re2 -163.9(4) . . . .
Re1 Re4 Re6 Re2 -54.66(2) . . . .
Re3 Re4 Re6 Re2 54.81(2) . . . .
Re5 Re4 Re6 Re2 0.02(2) . . . .
S2 Re4 Re6 Re1 2.45(9) . . . .
S3 Re4 Re6 Re1 -68.73(9) . . . .
S7 Re4 Re6 Re1 178.22(11) . . . .
S6 Re4 Re6 Re1 107.37(10) . . . .
P2B Re4 Re6 Re1 -121.5(7) . . . .
P2A Re4 Re6 Re1 -109.3(4) . . . .
Re3 Re4 Re6 Re1 109.47(2) . . . .
Re5 Re4 Re6 Re1 54.68(2) . . . .
S2 Re4 Re6 Re3 -107.01(9) . . . .
S3 Re4 Re6 Re3 -178.20(9) . . . .
S7 Re4 Re6 Re3 68.76(11) . . . .
S6 Re4 Re6 Re3 -2.10(10) . . . .
P2B Re4 Re6 Re3 129.0(7) . . . .
P2A Re4 Re6 Re3 141.3(4) . . . .
Re1 Re4 Re6 Re3 -109.47(2) . . . .
Re5 Re4 Re6 Re3 -54.79(2) . . . .
S5 Re2 S1 Re5 49.75(10) . . . .
S4 Re2 S1 Re5 -124.06(9) . . . .
Cl2 Re2 S1 Re5 144.27(11) . . . .
Re1 Re2 S1 Re5 -73.03(6) . . . .
Re3 Re2 S1 Re5 -2.97(9) . . . .
Re6 Re2 S1 Re5 -72.20(8) . . . .
S5 Re2 S1 Re1 122.78(10) . . . .
S4 Re2 S1 Re1 -51.03(9) . . . .
Cl2 Re2 S1 Re1 -142.70(11) . . . .
Re3 Re2 S1 Re1 70.06(8) . . . .
Re5 Re2 S1 Re1 73.03(6) . . . .
Re6 Re2 S1 Re1 0.83(9) . . . .
C1 Re5 S1 Re2 -143.6(4) . . . .
S2 Re5 S1 Re2 122.12(9) . . . .
S5 Re5 S1 Re2 -49.13(9) . . . .
Re1 Re5 S1 Re2 72.51(6) . . . .
Re3 Re5 S1 Re2 2.93(9) . . . .
Re4 Re5 S1 Re2 70.12(7) . . . .
C1 Re5 S1 Re1 143.9(4) . . . .
S2 Re5 S1 Re1 49.61(9) . . . .
S5 Re5 S1 Re1 -121.64(9) . . . .
Re2 Re5 S1 Re1 -72.51(6) . . . .
Re3 Re5 S1 Re1 -69.58(7) . . . .
Re4 Re5 S1 Re1 -2.39(9) . . . .
S2 Re1 S1 Re2 -122.67(10) . . . .
S4 Re1 S1 Re2 50.83(10) . . . .
Cl1 Re1 S1 Re2 145.92(11) . . . .
Re4 Re1 S1 Re2 -70.67(8) . . . .
Re6 Re1 S1 Re2 -0.82(9) . . . .
Re5 Re1 S1 Re2 -73.13(6) . . . .
S2 Re1 S1 Re5 -49.55(10) . . . .
S4 Re1 S1 Re5 123.95(10) . . . .
Cl1 Re1 S1 Re5 -140.96(11) . . . .
Re4 Re1 S1 Re5 2.46(9) . . . .
Re2 Re1 S1 Re5 73.13(6) . . . .
Re6 Re1 S1 Re5 72.30(7) . . . .
S3 Re4 S2 Re5 123.21(9) . . . .
S6 Re4 S2 Re5 -50.75(11) . . . .
P2B Re4 S2 Re5 -143.1(5) . . . .
P2A Re4 S2 Re5 -150.8(3) . . . .
Re1 Re4 S2 Re5 73.15(6) . . . .
Re3 Re4 S2 Re5 1.97(9) . . . .
Re6 Re4 S2 Re5 70.63(8) . . . .
S3 Re4 S2 Re1 50.06(9) . . . .
S6 Re4 S2 Re1 -123.90(11) . . . .
P2B Re4 S2 Re1 143.8(5) . . . .
P2A Re4 S2 Re1 136.0(3) . . . .
Re3 Re4 S2 Re1 -71.17(8) . . . .
Re5 Re4 S2 Re1 -73.15(6) . . . .
Re6 Re4 S2 Re1 -2.52(9) . . . .
C1 Re5 S2 Re4 150.0(4) . . . .
S1 Re5 S2 Re4 -122.11(9) . . . .
S6 Re5 S2 Re4 50.39(10) . . . .
Re2 Re5 S2 Re4 -69.37(8) . . . .
Re1 Re5 S2 Re4 -72.23(6) . . . .
Re3 Re5 S2 Re4 -1.93(9) . . . .
C1 Re5 S2 Re1 -137.8(4) . . . .
S1 Re5 S2 Re1 -49.88(9) . . . .
S6 Re5 S2 Re1 122.62(10) . . . .
Re2 Re5 S2 Re1 2.86(9) . . . .
Re3 Re5 S2 Re1 70.30(8) . . . .
Re4 Re5 S2 Re1 72.23(6) . . . .
S3 Re1 S2 Re4 -49.71(9) . . . .
S1 Re1 S2 Re4 123.86(9) . . . .
Cl1 Re1 S2 Re4 -139.99(10) . . . .
Re2 Re1 S2 Re4 71.31(8) . . . .
Re6 Re1 S2 Re4 2.55(9) . . . .
Re5 Re1 S2 Re4 74.19(7) . . . .
S3 Re1 S2 Re5 -123.90(10) . . . .
S1 Re1 S2 Re5 49.68(9) . . . .
Cl1 Re1 S2 Re5 145.83(10) . . . .
Re4 Re1 S2 Re5 -74.19(7) . . . .
Re2 Re1 S2 Re5 -2.88(9) . . . .
Re6 Re1 S2 Re5 -71.64(8) . . . .
S2 Re4 S3 Re1 -50.08(9) . . . .
S7 Re4 S3 Re1 123.43(11) . . . .
P2B Re4 S3 Re1 -139.4(6) . . . .
P2A Re4 S3 Re1 -134.7(4) . . . .
Re3 Re4 S3 Re1 71.11(8) . . . .
Re5 Re4 S3 Re1 2.29(9) . . . .
Re6 Re4 S3 Re1 72.86(6) . . . .
S2 Re4 S3 Re6 -122.94(9) . . . .
S7 Re4 S3 Re6 50.57(11) . . . .
P2B Re4 S3 Re6 147.7(6) . . . .
P2A Re4 S3 Re6 152.5(4) . . . .
Re1 Re4 S3 Re6 -72.86(6) . . . .
Re3 Re4 S3 Re6 -1.76(9) . . . .
Re5 Re4 S3 Re6 -70.57(8) . . . .
S2 Re1 S3 Re4 49.63(10) . . . .
S4 Re1 S3 Re4 -123.79(10) . . . .
Cl1 Re1 S3 Re4 141.03(11) . . . .
Re2 Re1 S3 Re4 -71.09(7) . . . .
Re6 Re1 S3 Re4 -74.24(6) . . . .
Re5 Re1 S3 Re4 -2.31(9) . . . .
S2 Re1 S3 Re6 123.87(10) . . . .
S4 Re1 S3 Re6 -49.55(9) . . . .
Cl1 Re1 S3 Re6 -144.73(11) . . . .
Re4 Re1 S3 Re6 74.24(6) . . . .
Re2 Re1 S3 Re6 3.15(9) . . . .
Re5 Re1 S3 Re6 71.93(7) . . . .
C4 Re6 S3 Re4 -149.4(4) . . . .
S4 Re6 S3 Re4 121.89(9) . . . .
S7 Re6 S3 Re4 -50.51(10) . . . .
Re2 Re6 S3 Re4 69.12(8) . . . .
Re1 Re6 S3 Re4 72.24(6) . . . .
Re3 Re6 S3 Re4 1.72(8) . . . .
C4 Re6 S3 Re1 138.3(4) . . . .
S4 Re6 S3 Re1 49.64(9) . . . .
S7 Re6 S3 Re1 -122.75(10) . . . .
Re2 Re6 S3 Re1 -3.12(9) . . . .
Re3 Re6 S3 Re1 -70.52(7) . . . .
Re4 Re6 S3 Re1 -72.24(6) . . . .
S8 Re2 S4 Re6 -49.56(11) . . . .
S1 Re2 S4 Re6 124.23(9) . . . .
Cl2 Re2 S4 Re6 -143.88(12) . . . .
Re1 Re2 S4 Re6 73.03(6) . . . .
Re3 Re2 S4 Re6 3.03(10) . . . .
Re5 Re2 S4 Re6 72.19(8) . . . .
S8 Re2 S4 Re1 -122.59(11) . . . .
S1 Re2 S4 Re1 51.20(9) . . . .
Cl2 Re2 S4 Re1 143.09(12) . . . .
Re3 Re2 S4 Re1 -70.00(9) . . . .
Re5 Re2 S4 Re1 -0.84(10) . . . .
Re6 Re2 S4 Re1 -73.03(6) . . . .
C4 Re6 S4 Re2 143.2(4) . . . .
S3 Re6 S4 Re2 -122.09(9) . . . .
S8 Re6 S4 Re2 49.06(10) . . . .
Re1 Re6 S4 Re2 -72.63(6) . . . .
Re3 Re6 S4 Re2 -2.99(9) . . . .
Re4 Re6 S4 Re2 -70.05(8) . . . .
C4 Re6 S4 Re1 -144.2(4) . . . .
S3 Re6 S4 Re1 -49.46(9) . . . .
S8 Re6 S4 Re1 121.69(10) . . . .
Re2 Re6 S4 Re1 72.63(6) . . . .
Re3 Re6 S4 Re1 69.64(8) . . . .
Re4 Re6 S4 Re1 2.58(9) . . . .
S3 Re1 S4 Re2 122.82(10) . . . .
S1 Re1 S4 Re2 -50.80(9) . . . .
Cl1 Re1 S4 Re2 -146.87(10) . . . .
Re4 Re1 S4 Re2 70.51(8) . . . .
Re6 Re1 S4 Re2 73.19(7) . . . .
Re5 Re1 S4 Re2 0.84(10) . . . .
S3 Re1 S4 Re6 49.63(9) . . . .
S1 Re1 S4 Re6 -123.99(9) . . . .
Cl1 Re1 S4 Re6 139.94(10) . . . .
Re4 Re1 S4 Re6 -2.68(9) . . . .
Re2 Re1 S4 Re6 -73.19(7) . . . .
Re5 Re1 S4 Re6 -72.35(8) . . . .
S8 Re3 S5 Re2 -51.14(10) . . . .
S6 Re3 S5 Re2 122.61(11) . . . .
P1A Re3 S5 Re2 -141.4(4) . . . .
P1B Re3 S5 Re2 -151.0(4) . . . .
Re4 Re3 S5 Re2 69.87(8) . . . .
Re5 Re3 S5 Re2 72.71(6) . . . .
Re6 Re3 S5 Re2 0.51(9) . . . .
S8 Re3 S5 Re5 -123.85(10) . . . .
S6 Re3 S5 Re5 49.90(11) . . . .
P1A Re3 S5 Re5 145.9(4) . . . .
P1B Re3 S5 Re5 136.3(4) . . . .
Re4 Re3 S5 Re5 -2.84(10) . . . .
Re2 Re3 S5 Re5 -72.71(6) . . . .
Re6 Re3 S5 Re5 -72.19(8) . . . .
S8 Re2 S5 Re3 50.99(11) . . . .
S1 Re2 S5 Re3 -122.86(9) . . . .
Cl2 Re2 S5 Re3 145.15(12) . . . .
Re1 Re2 S5 Re3 -69.39(8) . . . .
Re5 Re2 S5 Re3 -73.32(7) . . . .
Re6 Re2 S5 Re3 -0.52(10) . . . .
S8 Re2 S5 Re5 124.31(11) . . . .
S1 Re2 S5 Re5 -49.53(9) . . . .
Cl2 Re2 S5 Re5 -141.52(12) . . . .
Re1 Re2 S5 Re5 3.93(10) . . . .
Re3 Re2 S5 Re5 73.32(7) . . . .
Re6 Re2 S5 Re5 72.80(8) . . . .
C1 Re5 S5 Re3 -149.6(4) . . . .
S1 Re5 S5 Re3 122.52(9) . . . .
S6 Re5 S5 Re3 -49.87(10) . . . .
Re2 Re5 S5 Re3 73.18(6) . . . .
Re1 Re5 S5 Re3 69.33(8) . . . .
Re4 Re5 S5 Re3 2.75(9) . . . .
C1 Re5 S5 Re2 137.2(4) . . . .
S1 Re5 S5 Re2 49.34(9) . . . .
S6 Re5 S5 Re2 -123.05(10) . . . .
Re1 Re5 S5 Re2 -3.86(9) . . . .
Re3 Re5 S5 Re2 -73.18(6) . . . .
Re4 Re5 S5 Re2 -70.43(8) . . . .
S2 Re4 S6 Re3 123.20(10) . . . .
S7 Re4 S6 Re3 -50.30(11) . . . .
P2B Re4 S6 Re3 -147.5(6) . . . .
P2A Re4 S6 Re3 -152.4(4) . . . .
Re1 Re4 S6 Re3 70.94(9) . . . .
Re5 Re4 S6 Re3 72.85(7) . . . .
Re6 Re4 S6 Re3 2.15(10) . . . .
S2 Re4 S6 Re5 50.35(10) . . . .
S7 Re4 S6 Re5 -123.15(12) . . . .
P2B Re4 S6 Re5 139.6(6) . . . .
P2A Re4 S6 Re5 134.8(4) . . . .
Re1 Re4 S6 Re5 -1.91(12) . . . .
Re3 Re4 S6 Re5 -72.85(7) . . . .
Re6 Re4 S6 Re5 -70.70(9) . . . .
S5 Re3 S6 Re4 -123.42(10) . . . .
S7 Re3 S6 Re4 50.11(10) . . . .
P1A Re3 S6 Re4 146.7(4) . . . .
P1B Re3 S6 Re4 141.0(4) . . . .
Re2 Re3 S6 Re4 -70.70(9) . . . .
Re5 Re3 S6 Re4 -73.45(7) . . . .
Re6 Re3 S6 Re4 -2.16(10) . . . .
S5 Re3 S6 Re5 -49.98(10) . . . .
S7 Re3 S6 Re5 123.56(11) . . . .
P1A Re3 S6 Re5 -139.8(4) . . . .
P1B Re3 S6 Re5 -145.6(4) . . . .
Re4 Re3 S6 Re5 73.45(7) . . . .
Re2 Re3 S6 Re5 2.75(11) . . . .
Re6 Re3 S6 Re5 71.29(9) . . . .
C1 Re5 S6 Re4 -144.1(4) . . . .
S2 Re5 S6 Re4 -49.97(10) . . . .
S5 Re5 S6 Re4 121.41(10) . . . .
Re2 Re5 S6 Re4 69.40(10) . . . .
Re1 Re5 S6 Re4 1.86(12) . . . .
Re3 Re5 S6 Re4 72.14(7) . . . .
C1 Re5 S6 Re3 143.8(4) . . . .
S2 Re5 S6 Re3 -122.12(10) . . . .
S5 Re5 S6 Re3 49.27(10) . . . .
Re2 Re5 S6 Re3 -2.74(11) . . . .
Re1 Re5 S6 Re3 -70.28(10) . . . .
Re4 Re5 S6 Re3 -72.14(7) . . . .
S3 Re4 S7 Re6 -50.55(9) . . . .
S6 Re4 S7 Re6 123.43(11) . . . .
P2B Re4 S7 Re6 -144.1(5) . . . .
P2A Re4 S7 Re6 -136.2(3) . . . .
Re1 Re4 S7 Re6 1.73(11) . . . .
Re3 Re4 S7 Re6 73.01(8) . . . .
Re5 Re4 S7 Re6 70.49(9) . . . .
S3 Re4 S7 Re3 -123.56(10) . . . .
S6 Re4 S7 Re3 50.42(11) . . . .
P2B Re4 S7 Re3 142.8(5) . . . .
P2A Re4 S7 Re3 150.7(3) . . . .
Re1 Re4 S7 Re3 -71.28(9) . . . .
Re5 Re4 S7 Re3 -2.51(11) . . . .
Re6 Re4 S7 Re3 -73.01(8) . . . .
C4 Re6 S7 Re4 144.6(4) . . . .
S3 Re6 S7 Re4 50.04(9) . . . .
S8 Re6 S7 Re4 -121.28(10) . . . .
Re2 Re6 S7 Re4 -69.28(10) . . . .
Re1 Re6 S7 Re4 -1.69(11) . . . .
Re3 Re6 S7 Re4 -72.06(7) . . . .
C4 Re6 S7 Re3 -143.3(4) . . . .
S3 Re6 S7 Re3 122.10(10) . . . .
S8 Re6 S7 Re3 -49.22(10) . . . .
Re2 Re6 S7 Re3 2.78(12) . . . .
Re1 Re6 S7 Re3 70.37(10) . . . .
Re4 Re6 S7 Re3 72.06(7) . . . .
S8 Re3 S7 Re4 123.58(11) . . . .
S6 Re3 S7 Re4 -50.08(11) . . . .
P1A Re3 S7 Re4 -146.2(4) . . . .
P1B Re3 S7 Re4 -136.4(4) . . . .
Re2 Re3 S7 Re4 70.93(10) . . . .
Re5 Re3 S7 Re4 2.52(11) . . . .
Re6 Re3 S7 Re4 73.71(7) . . . .
S8 Re3 S7 Re6 49.87(11) . . . .
S6 Re3 S7 Re6 -123.79(11) . . . .
P1A Re3 S7 Re6 140.1(4) . . . .
P1B Re3 S7 Re6 149.8(4) . . . .
Re4 Re3 S7 Re6 -73.71(7) . . . .
Re2 Re3 S7 Re6 -2.78(12) . . . .
Re5 Re3 S7 Re6 -71.19(10) . . . .
S5 Re3 S8 Re2 51.15(10) . . . .
S7 Re3 S8 Re2 -122.50(10) . . . .
P1A Re3 S8 Re2 140.9(4) . . . .
P1B Re3 S8 Re2 146.6(4) . . . .
Re4 Re3 S8 Re2 -69.86(9) . . . .
Re5 Re3 S8 Re2 -0.67(10) . . . .
Re6 Re3 S8 Re2 -72.79(7) . . . .
S5 Re3 S8 Re6 123.94(10) . . . .
S7 Re3 S8 Re6 -49.71(11) . . . .
P1A Re3 S8 Re6 -146.3(4) . . . .
P1B Re3 S8 Re6 -140.6(4) . . . .
Re4 Re3 S8 Re6 2.93(11) . . . .
Re2 Re3 S8 Re6 72.79(7) . . . .
Re5 Re3 S8 Re6 72.11(9) . . . .
S5 Re2 S8 Re3 -51.07(10) . . . .
S4 Re2 S8 Re3 122.82(9) . . . .
Cl2 Re2 S8 Re3 -145.43(11) . . . .
Re1 Re2 S8 Re3 69.56(8) . . . .
Re5 Re2 S8 Re3 0.68(10) . . . .
Re6 Re2 S8 Re3 73.45(8) . . . .
S5 Re2 S8 Re6 -124.52(11) . . . .
S4 Re2 S8 Re6 49.37(10) . . . .
Cl2 Re2 S8 Re6 141.12(12) . . . .
Re1 Re2 S8 Re6 -3.89(11) . . . .
Re3 Re2 S8 Re6 -73.45(8) . . . .
Re5 Re2 S8 Re6 -72.77(8) . . . .
C4 Re6 S8 Re3 148.9(4) . . . .
S4 Re6 S8 Re3 -122.45(10) . . . .
S7 Re6 S8 Re3 49.83(11) . . . .
Re2 Re6 S8 Re3 -73.20(7) . . . .
Re1 Re6 S8 Re3 -69.36(10) . . . .
Re4 Re6 S8 Re3 -2.83(11) . . . .
C4 Re6 S8 Re2 -137.9(4) . . . .
S4 Re6 S8 Re2 -49.25(10) . . . .
S7 Re6 S8 Re2 123.03(11) . . . .
Re1 Re6 S8 Re2 3.84(11) . . . .
Re3 Re6 S8 Re2 73.20(7) . . . .
Re4 Re6 S8 Re2 70.37(10) . . . .
S8 Re3 P1A C11A -19.1(15) . . . .
S5 Re3 P1A C11A 69.2(15) . . . .
S7 Re3 P1A C11A -109.4(15) . . . .
S6 Re3 P1A C11A 159.7(15) . . . .
Re4 Re3 P1A C11A -155.3(13) . . . .
Re2 Re3 P1A C11A 25.3(18) . . . .
Re5 Re3 P1A C11A 110.4(15) . . . .
Re6 Re3 P1A C11A -60.1(16) . . . .
S8 Re3 P1A C13A -138.6(15) . . . .
S5 Re3 P1A C13A -50.3(15) . . . .
S7 Re3 P1A C13A 131.1(15) . . . .
S6 Re3 P1A C13A 40.2(15) . . . .
Re4 Re3 P1A C13A 85.2(16) . . . .
Re2 Re3 P1A C13A -94.2(16) . . . .
Re5 Re3 P1A C13A -9.1(17) . . . .
Re6 Re3 P1A C13A -179.7(14) . . . .
S8 Re3 P1A C15A 100.2(13) . . . .
S5 Re3 P1A C15A -171.5(13) . . . .
S7 Re3 P1A C15A 9.9(13) . . . .
S6 Re3 P1A C15A -81.0(13) . . . .
Re4 Re3 P1A C15A -36.0(16) . . . .
Re2 Re3 P1A C15A 144.6(12) . . . .
Re5 Re3 P1A C15A -130.3(12) . . . .
Re6 Re3 P1A C15A 59.1(14) . . . .
S8 Re3 P1B C11B -9.4(15) . . . .
S5 Re3 P1B C11B 79.9(15) . . . .
S7 Re3 P1B C11B -99.8(15) . . . .
S6 Re3 P1B C11B 170.0(15) . . . .
Re4 Re3 P1B C11B -147.5(13) . . . .
Re2 Re3 P1B C11B 38.9(19) . . . .
Re5 Re3 P1B C11B 130.7(14) . . . .
Re6 Re3 P1B C11B -61.3(16) . . . .
S8 Re3 P1B C15B 114.7(14) . . . .
S5 Re3 P1B C15B -156.0(14) . . . .
S7 Re3 P1B C15B 24.3(15) . . . .
S6 Re3 P1B C15B -65.9(14) . . . .
Re4 Re3 P1B C15B -23.4(17) . . . .
Re2 Re3 P1B C15B 163.0(12) . . . .
Re5 Re3 P1B C15B -105.2(15) . . . .
Re6 Re3 P1B C15B 62.8(15) . . . .
S8 Re3 P1B C13B -129.6(15) . . . .
S5 Re3 P1B C13B -40.3(15) . . . .
S7 Re3 P1B C13B 140.0(15) . . . .
S6 Re3 P1B C13B 49.8(15) . . . .
Re4 Re3 P1B C13B 92.3(15) . . . .
Re2 Re3 P1B C13B -81.3(16) . . . .
Re5 Re3 P1B C13B 10.5(16) . . . .
Re6 Re3 P1B C13B 178.5(14) . . . .
S2 Re4 P2A C21A -146.8(13) . . . .
S3 Re4 P2A C21A -55.8(13) . . . .
S7 Re4 P2A C21A 32.2(13) . . . .
S6 Re4 P2A C21A 125.0(13) . . . .
Re1 Re4 P2A C21A -102.0(13) . . . .
Re3 Re4 P2A C21A 80.1(14) . . . .
Re5 Re4 P2A C21A 179.5(12) . . . .
Re6 Re4 P2A C21A -22.6(14) . . . .
S2 Re4 P2A C25A -21.6(13) . . . .
S3 Re4 P2A C25A 69.5(13) . . . .
S7 Re4 P2A C25A 157.4(13) . . . .
S6 Re4 P2A C25A -109.8(13) . . . .
Re1 Re4 P2A C25A 23.2(15) . . . .
Re3 Re4 P2A C25A -154.6(12) . . . .
Re5 Re4 P2A C25A -55.3(14) . . . .
Re6 Re4 P2A C25A 102.6(14) . . . .
S2 Re4 P2A C23A 98.6(14) . . . .
S3 Re4 P2A C23A -170.3(14) . . . .
S7 Re4 P2A C23A -82.4(14) . . . .
S6 Re4 P2A C23A 10.4(14) . . . .
Re1 Re4 P2A C23A 143.5(12) . . . .
Re3 Re4 P2A C23A -34.4(18) . . . .
Re5 Re4 P2A C23A 64.9(14) . . . .
Re6 Re4 P2A C23A -137.2(13) . . . .
S2 Re4 P2B C21B 171(2) . . . .
S3 Re4 P2B C21B -98(2) . . . .
S7 Re4 P2B C21B -9(2) . . . .
S6 Re4 P2B C21B 82(2) . . . .
Re1 Re4 P2B C21B -146.5(17) . . . .
Re3 Re4 P2B C21B 40(2) . . . .
Re5 Re4 P2B C21B 129(2) . . . .
Re6 Re4 P2B C21B -56(2) . . . .
S2 Re4 P2B C23B 31(2) . . . .
S3 Re4 P2B C23B 122(2) . . . .
S7 Re4 P2B C23B -149(2) . . . .
S6 Re4 P2B C23B -58(2) . . . .
Re1 Re4 P2B C23B 74(2) . . . .
Re3 Re4 P2B C23B -100(2) . . . .
Re5 Re4 P2B C23B -11(2) . . . .
Re6 Re4 P2B C23B 163.7(19) . . . .
S2 Re4 P2B C25B -72(2) . . . .
S3 Re4 P2B C25B 19(2) . . . .
S7 Re4 P2B C25B 108(2) . . . .
S6 Re4 P2B C25B -161(2) . . . .
Re1 Re4 P2B C25B -29(2) . . . .
Re3 Re4 P2B C25B 156.8(18) . . . .
Re5 Re4 P2B C25B -114(2) . . . .
Re6 Re4 P2B C25B 61(2) . . . .
C2 N1 C1 N2 -3(2) . . . .
C31 N1 C1 N2 -174.4(17) . . . .
C2 N1 C1 Re5 -170.0(14) . . . .
C31 N1 C1 Re5 18(3) . . . .
C3 N2 C1 N1 1.1(19) . . . .
C41 N2 C1 N1 173.3(15) . . . .
C3 N2 C1 Re5 168.8(13) . . . .
C41 N2 C1 Re5 -19(2) . . . .
S2 Re5 C1 N1 177.1(14) . . . .
S1 Re5 C1 N1 87.1(14) . . . .
S5 Re5 C1 N1 -3.0(14) . . . .
S6 Re5 C1 N1 -93.7(14) . . . .
Re2 Re5 C1 N1 45.8(16) . . . .
Re1 Re5 C1 N1 128.4(13) . . . .
Re3 Re5 C1 N1 -43.6(17) . . . .
Re4 Re5 C1 N1 -142.9(12) . . . .
S2 Re5 C1 N2 12.6(13) . . . .
S1 Re5 C1 N2 -77.4(13) . . . .
S5 Re5 C1 N2 -167.5(13) . . . .
S6 Re5 C1 N2 101.9(13) . . . .
Re2 Re5 C1 N2 -118.7(12) . . . .
Re1 Re5 C1 N2 -36.0(16) . . . .
Re3 Re5 C1 N2 151.9(10) . . . .
Re4 Re5 C1 N2 52.6(16) . . . .
C1 N1 C2 C3 3(3) . . . .
C31 N1 C2 C3 175.9(18) . . . .
N1 C2 C3 N2 -2(3) . . . .
C1 N2 C3 C2 1(2) . . . .
C41 N2 C3 C2 -172.4(18) . . . .
C6 N4 C4 N3 0.0(17) . . . .
C61 N4 C4 N3 179.3(15) . . . .
C6 N4 C4 Re6 170.7(12) . . . .
C61 N4 C4 Re6 -10(2) . . . .
C5 N3 C4 N4 0.4(17) . . . .
C51 N3 C4 N4 -174.9(15) . . . .
C5 N3 C4 Re6 -170.5(12) . . . .
C51 N3 C4 Re6 14(2) . . . .
S4 Re6 C4 N4 -88.6(13) . . . .
S3 Re6 C4 N4 -178.8(13) . . . .
S8 Re6 C4 N4 1.7(14) . . . .
S7 Re6 C4 N4 92.1(13) . . . .
Re2 Re6 C4 N4 -46.6(16) . . . .
Re1 Re6 C4 N4 -130.1(12) . . . .
Re3 Re6 C4 N4 42.5(17) . . . .
Re4 Re6 C4 N4 140.5(11) . . . .
S4 Re6 C4 N3 79.8(13) . . . .
S3 Re6 C4 N3 -10.4(14) . . . .
S8 Re6 C4 N3 170.0(13) . . . .
S7 Re6 C4 N3 -99.5(13) . . . .
Re2 Re6 C4 N3 121.8(12) . . . .
Re1 Re6 C4 N3 38.3(16) . . . .
Re3 Re6 C4 N3 -149.1(11) . . . .
Re4 Re6 C4 N3 -51.1(16) . . . .
C4 N3 C5 C6 -1(2) . . . .
C51 N3 C5 C6 175.0(15) . . . .
N3 C5 C6 N4 1(2) . . . .
C4 N4 C6 C5 0(2) . . . .
C61 N4 C6 C5 -179.8(15) . . . .
C13A P1A C11A C12A 63(3) . . . .
C15A P1A C11A C12A 176(3) . . . .
Re3 P1A C11A C12A -60(3) . . . .
C11A P1A C13A C14A 51(4) . . . .
C15A P1A C13A C14A -57(4) . . . .
Re3 P1A C13A C14A -180(3) . . . .
C11A P1A C15A C16A -167(3) . . . .
C13A P1A C15A C16A -59(3) . . . .
Re3 P1A C15A C16A 64(3) . . . .
C15B P1B C11B C12B 170(3) . . . .
C13B P1B C11B C12B 63(3) . . . .
Re3 P1B C11B C12B -59(3) . . . .
C11B P1B C13B C14B 47(4) . . . .
C15B P1B C13B C14B -62(3) . . . .
Re3 P1B C13B C14B 171(3) . . . .
C11B P1B C15B C16B 47(4) . . . .
C13B P1B C15B C16B 158(3) . . . .
Re3 P1B C15B C16B -81(3) . . . .
C25A P2A C21A C22A 167(3) . . . .
C23A P2A C21A C22A 61(3) . . . .
Re4 P2A C21A C22A -63(3) . . . .
C21A P2A C23A C24A 162(3) . . . .
C25A P2A C23A C24A 54(3) . . . .
Re4 P2A C23A C24A -73(3) . . . .
C21A P2A C25A C26A 65(3) . . . .
C23A P2A C25A C26A 168(3) . . . .
Re4 P2A C25A C26A -66(3) . . . .
C23B P2B C21B C22B -133(5) . . . .
C25B P2B C21B C22B -32(5) . . . .
Re4 P2B C21B C22B 88(5) . . . .
C21B P2B C23B C24B -18(6) . . . .
C25B P2B C23B C24B -126(5) . . . .
Re4 P2B C23B C24B 121(4) . . . .
C21B P2B C25B C26B -170(5) . . . .
C23B P2B C25B C26B -52(5) . . . .
Re4 P2B C25B C26B 67(5) . . . .
C1 N1 C31 C36 80(2) . . . .
C2 N1 C31 C36 -91(2) . . . .
C1 N1 C31 C32 -105(2) . . . .
C2 N1 C31 C32 84(2) . . . .
C36 C31 C32 C33 1(2) . . . .
N1 C31 C32 C33 -174.3(14) . . . .
C36 C31 C32 C37 -175.8(15) . . . .
N1 C31 C32 C37 9(2) . . . .
C31 C32 C33 C34 -1(3) . . . .
C37 C32 C33 C34 175.9(17) . . . .
C32 C33 C34 C35 0(3) . . . .
C32 C33 C34 C38 -177.8(18) . . . .
C33 C34 C35 C36 0(3) . . . .
C38 C34 C35 C36 177.9(18) . . . .
C32 C31 C36 C35 0(2) . . . .
N1 C31 C36 C35 174.4(14) . . . .
C32 C31 C36 C39 -179.2(15) . . . .
N1 C31 C36 C39 -4(2) . . . .
C34 C35 C36 C31 0(3) . . . .
C34 C35 C36 C39 179.0(17) . . . .
C1 N2 C41 C42 101.0(19) . . . .
C3 N2 C41 C42 -87.3(19) . . . .
C1 N2 C41 C46 -83.1(19) . . . .
C3 N2 C41 C46 89(2) . . . .
C46 C41 C42 C43 6(2) . . . .
N2 C41 C42 C43 -178.4(13) . . . .
C46 C41 C42 C47 -176.9(15) . . . .
N2 C41 C42 C47 -1(2) . . . .
C41 C42 C43 C44 -3(2) . . . .
C47 C42 C43 C44 179.6(16) . . . .
C42 C43 C44 C45 -1(3) . . . .
C42 C43 C44 C48 179.8(17) . . . .
C43 C44 C45 C46 4(3) . . . .
C48 C44 C45 C46 -177.7(18) . . . .
C44 C45 C46 C41 -1(3) . . . .
C44 C45 C46 C49 177.6(19) . . . .
C42 C41 C46 C45 -4(2) . . . .
N2 C41 C46 C45 -179.7(14) . . . .
C42 C41 C46 C49 177.5(16) . . . .
N2 C41 C46 C49 2(2) . . . .
C5 N3 C51 C56 87.1(19) . . . .
C4 N3 C51 C56 -98.0(19) . . . .
C5 N3 C51 C52 -87.6(19) . . . .
C4 N3 C51 C52 87.4(19) . . . .
C56 C51 C52 C53 4(2) . . . .
N3 C51 C52 C53 178.8(13) . . . .
C56 C51 C52 C57 -179.6(15) . . . .
N3 C51 C52 C57 -5(2) . . . .
C51 C52 C53 C54 -2(2) . . . .
C57 C52 C53 C54 -178.0(16) . . . .
C52 C53 C54 C55 -1(3) . . . .
C52 C53 C54 C58 -179.3(17) . . . .
C53 C54 C55 C56 1(3) . . . .
C58 C54 C55 C56 179.9(16) . . . .
C54 C55 C56 C51 1(2) . . . .
C54 C55 C56 C59 177.6(15) . . . .
C52 C51 C56 C55 -4(2) . . . .
N3 C51 C56 C55 -178.1(13) . . . .
C52 C51 C56 C59 179.5(14) . . . .
N3 C51 C56 C59 5(2) . . . .
C6 N4 C61 C66 96.1(18) . . . .
C4 N4 C61 C66 -83.2(19) . . . .
C6 N4 C61 C62 -78.2(18) . . . .
C4 N4 C61 C62 102.5(18) . . . .
C66 C61 C62 C63 1(2) . . . .
N4 C61 C62 C63 175.1(14) . . . .
C66 C61 C62 C67 177.8(15) . . . .
N4 C61 C62 C67 -8(2) . . . .
C61 C62 C63 C64 2(3) . . . .
C67 C62 C63 C64 -175.0(17) . . . .
C62 C63 C64 C65 -3(3) . . . .
C62 C63 C64 C68 178(2) . . . .
C63 C64 C65 C66 1(3) . . . .
C68 C64 C65 C66 -180(2) . . . .
C62 C61 C66 C65 -3(2) . . . .
N4 C61 C66 C65 -176.6(14) . . . .
C62 C61 C66 C69 179.6(14) . . . .
N4 C61 C66 C69 6(2) . . . .
C64 C65 C66 C61 1(3) . . . .
C64 C65 C66 C69 179.1(17) . . . .
