Information card for entry 7123452

Structure parameters

• Formula: C46 H80 Bi7 Co3 K2 N4 O15
• Calculated formula: C46 H80 Bi7 Co3 K2 N4 O15
• Title of publication: [Bi7M3(CO)3]2- (M = Co, Rh): A New Prototype of 10-vertex Deltahedral Hybrids From Unprecedented Polycyclic η5−coordination addition of Bi73- and trimetallic fragments†
• Authors of publication: Li, Zhenyu; Dan, Ouyang; Xu, Li
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.123 ± 0.0005 Å
• b: 14.1602 ± 0.0006 Å
• c: 21.3908 ± 0.0009 Å
• α: 99.458 ± 0.002°
• β: 99.365 ± 0.001°
• γ: 117.512 ± 0.001°
• Cell volume: 3345.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1126
• Weighted residual factors for all reflections included in the refinement: 0.1204
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No